Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00155A, Paper

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Sharon E. Ashbrook
This Faraday Discussion explored the field of NMR crystallography, considering recent developments in experimental and theoretical approaches, new advances in machine learning and applications to disordered, amorphous and dynamic materials.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00111G, Paper

Ying Yang, Yuanqing Ma, J. Justin Gooding
We demonstrate how to effectively modulate the fluorescence intensity of organic dye-labelled cell samples on an indium tin oxide surface using electrochemistry with redox-active mediators present in an oxygen scavenger buffer.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00135D, Paper

Tianyi Xiong, Wenjie Ma, Ping Yu
Ion current oscillation of polyelectrolyte modified micropipettes in pH gradients was discovered and regulated. The periodic switch between the protonated/deprotonated state of modified micropipettes contributed to the spontaneous ICO observation.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00146J, Paper

Lebing Wang, Shuo Zhou, Yunjiao Wang, Yan Wang, Jing Li, Xiaohan Chen, Daming Zhou, Liyuan Liang, Bohua Yin, Youwen Zhang, Liang Wang
A molecular sandwich-based DNAzyme catalytic reaction is capable of transducing detectable nucleic acids as a substitute for difficult to yield protein detection in complicated biological matrices, in a nanopore.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00122B, Paper

Ancheng Wang, Rong Jin, Dechen Jiang
An integrated SECCM with LEIS is established by combining the preamplifier based EIS measurement with scanning electrochemical cell microscopy.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00126E, Paper

Wandong Zhao, Jin Lu
Imaging the single molecule electrocatalytic (EC') process and correlating it with the conventional ensemble EC' mechanism.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00137K, Paper

Kaoru Hiramoto, Kosuke Ino, Ibuki Takahashi, Ayumi Hirano-Iwata, Hitoshi Shiku
We propose the use of electrochemiluminescence microscopy in a solution of [Ru(bpy)₃]²⁺ and tri-n-propylamine to monitor alterations in lipid membranes due to peptide action.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00148F, Paper

DaVante Cain, Ethan Cao, Ivan Vlassiouk, Tilman E. Schäffer, Zuzanna S. Siwy
The conductance and selectivity of low-aspect-ratio nanopores are almost independent of the length due to polarization effects controlled by the geometric and electrochemical properties of the whole (pore + reservoir) system.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00117F, Paper

Yuanhao Wang, Nan An, Bintong Huang, Yueming Zhai
Denaturation of individual ovalbumin induced by guanidine hydrochloride and lead ions was investigated by using non-sticky SiN_x nanonets.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00115J, Paper

Lachlan F. Gaudin, Cameron L. Bentley
Through presenting and discussing these findings, this article seeks to highlight complications in single-NP SECCM experiments, particularly those arising from issues with sample preparation.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00132J, Paper

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Nikan Afsahi, Zhu Zhang, Sanli Faez, Jean-Marc Noël, Manas Ranjan Panda, Mainak Majumder, Naimeh Naseri, Jean-François Lemineur, Frédéric Kanoufi
Interferometric scattering microscopy (iSCAT) allows visualizing individual petal-like MoS₂ sub-microparticles and monitoring operando their activity towards oxygen reduction reaction.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00136B, Paper

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Giada Caniglia, Sarah Horn, Christine Kranz
The feasibility of fabricating micro- and sub-micro-sized AFM probes based on Pt-B electrodeposition for the electrochemical detection of H₂ evolution is demonstrated.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00149D, Paper

Zhiwei Shang, Jing Zhao, Mengyu Yang, Yuling Xiao, Wenjing Chu, Yilin Cai, Xiaoqing Yi, Meihua Lin, Fan Xia
A biomimetic lipid membrane was developed by integrating DNA nanowires with a two-dimensional nanofluid membrane. By manipulating the DNA content, the composition of the membrane can be controlled, thereby adjusting ion transport.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00130C, Paper

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Ziwen Zhao, Arunava Naha, Nikolaos Kostopoulos, Alina Sekretareva
In this study, two approaches for step detection in single-entity electrochemistry data are developed and compared: discrete wavelet transforms and convolutional neural networks.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00138A, Paper

Peibo Xu, Henry David Jetmore, Ran Chen, Mei Shen
Glutamate detection on a glutamate oxidase-modified Pt nanoelectrode with the smallest area to date.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00080C, Paper

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Samuel F. Wenzel, Heekwon Lee, Hang Ren
The contributions of migration and electroosmotic flow induced by electrochemical redox molecules in dual-barrel SECCM were characterised.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00124A, Paper

Jaimy Monteiro, Harry Dunne, Kim McKelvey
A new scanning probe approach for the delivery of a gas-phase reactant to the surface of an electrocatalyst through a self-replenishing bubble located at the end of a scanning probe has been developed.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00116H, Paper

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Junichi Usuda, Kenshin Yagyu, Hiromasa Tanaka, Masaru Hori, Kenji Ishikawa, Yasufumi Takahashi
To characterize the anti-tumor effect of plasma-activated Ringer's lactate solutions, we used scanning ion conductance microscopy, using glass nanopipettes as probes, to visualize the structural changes of the cell surface.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00147H, Paper

Liang Liu
Deformation of liquid and gel electrolytes before touching the sample in SECCM and SGECM: equilibrium does not always exist.
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Faraday Discuss., 2024, Accepted Manuscript
DOI: 10.1039/D4FD00165F, Paper

Rawan AbouHaidar, Sana Bougueroua, Denis DUFLOT, Marie-Pierre Gaigeot, Barbara E Wyslouzil, Celine Toubin
Ice clouds in the upper troposphere are crucial for regulating Earth’s climate by affecting stratospheric humidity and the global radiative balance. A key aspect of cloud formation is heterogeneous ice...
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Faraday Discuss., 2024, 253,343-364
DOI: 10.1039/D4FD00012A, Paper

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Anne Hockmann, Florian Ackermann, Diddo Diddens, Isidora Cekic-Laskovic, Monika Schönhoff
Unusually high Li transference numbers (t⁺ > 0.7) in a bisolvent-in-salt electrolyte are explained by a heterogeneous Li solvation structure, which yields two distinctly different Li species with different transport behavior.
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Faraday Discuss., 2024, 253,329-342
DOI: 10.1039/D4FD00030G, Paper

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Evangelia Daskalopoulou, Philip Hunt, Christopher E. Elgar, Minjun Yang, Andrew P. Abbott, Jennifer M. Hartley
Formation of metal passivation layers during electrochemical dissolution is prevented by the use of ultrasound. Migration becomes the main method of mass transport across the electrical double layer.
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Faraday Discuss., 2024, 253,458-477
DOI: 10.1039/D4FD00031E, Paper

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Ben Jacobson, Shida Li, Paul Daly, Christopher E. Elgar, Andrew P. Abbott, Andrew Feeney, Paul Prentice
We characterise the development of cavitation structure in three deep eutectic solvents of increasing viscosity, and water, via high-speed imaging and parallel acoustic detection..
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Faraday Discuss., 2024, 253,100-117
DOI: 10.1039/D4FD00034J, Paper

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Tabita Pothmann, Maleen Middendorf, Christian Gerken, Pinchas Nürnberg, Monika Schönhoff, Bernhard Roling
An experimental overdetermination method and a Reverse Monte Carlo-based approach lead to strongly reduced uncertainties of transport parameters for highly concentrated electrolytes and to accurate information about ion correlations and transport limitations in batteries.
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Faraday Discuss., 2024, 253,478-492
DOI: 10.1039/D4FD00027G, Paper

Kateryna Goloviznina, Alessandra Serva, Mathieu Salanne
In 21 m LiTFSI water-in-salt electrolyte, the proton forms species existing in bulk water (H₃O⁺, H₅O₂⁺, etc.) as well as the HTFSI acid, known to be a superacid in water.
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Faraday Discuss., 2024, 253,273-288
DOI: 10.1039/D4FD00048J, Paper

Adriaan van den Bruinhorst, Chiara Corsini, Guillaume Depraetère, Nithavong Cam, Agílio Pádua, Margarida Costa Gomes
We quantified the balance between excess enthalpy (interactions) and excess entropy (structure/disorder) of mixing that determines large melting point depressions in deep eutectic solvents (DESs), reformulating the role of hydrogen bonding in DESs.
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Faraday Discuss., 2024, 253,26-41
DOI: 10.1039/D4FD00045E, Paper

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Iva Manasi, Stephen M. King, Karen J. Edler
The size of cationic micelles in a pTSA based deep eutectic solvent can be tuned by changing the solvent composition, which alters the surfactant–solvent interactions.
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Faraday Discuss., 2024, 253,129-145
DOI: 10.1039/D4FD00025K, Paper

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Fabian Zills, Moritz René Schäfer, Samuel Tovey, Johannes Kästner, Christian Holm
We demonstrate a learning-on-the-fly procedure to train machine-learned potentials from single-point density functional theory calculations before performing production molecular dynamics simulations.
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Faraday Discuss., 2024, 253,193-211
DOI: 10.1039/D4FD00040D, Paper

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Timothy S. Groves, Susan Perkin
We present measurements and analysis of the interactions between macroscopic bodies across a fluid mixture of two ionic liquids of widely diverging ionic size.
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Faraday Discuss., 2024, 253,365-384
DOI: 10.1039/D4FD00021H, Paper

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Daniel M. Markiewitz, Zachary A. H. Goodwin, Michael McEldrew, J. Pedro de Souza, Xuhui Zhang, Rosa M. Espinosa-Marzal, Martin Z. Bazant
We have developed a theory for the electrical double layer of salt-in-ionic liquids accounting for the thermoreversible association of ions into Cayley tree aggregates. We find that the solution becomes more aggregated at moderate positive voltages.
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Faraday Discuss., 2024, 253,385-406
DOI: 10.1039/D4FD00024B, Paper

Toru Ishikawa, Shohei Haga, Keisuke Shigenobu, Taku Sudoh, Seiji Tsuzuki, Wataru Shinoda, Kaoru Dokko, Masayoshi Watanabe, Kazuhide Ueno
Linear ether-based electrolytes show low solubility of the sulfur species, stability towards Li metal and polysulfide nucleophiles. Li–S cells using the lightweight electrolyte demonstrated an energy density exceeding 300 W h kg⁻¹.
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Faraday Discuss., 2024, 253,181-192
DOI: 10.1039/D4FD00058G, Paper

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Sophie Bonnassieux, Raj Pandya, Dhyllan Adan Skiba, Damien Degoulange, Dorothée Petit, Peter Seem, Russel P. Cowburn, Betar M. Gallant, Alexis Grimaud
We reinvestigated the PEG/K₂HPO₄/H₂O systems using a combination of liquid-phase nuclear magnetic resonance and high-resolution Raman spectroscopies, coupled with injection microcalorimetry.
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Faraday Discuss., 2024, 253,233-250
DOI: 10.1039/D4FD00052H, Paper

Nicolas Scaglione, Jocasta Avila, Agilio Padua, Margarida Costa Gomes
Tetraalkylphosphonium carboxylate ionic liquids absorb large quantities of carbon dioxide and are easily regenerated.
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Faraday Discuss., 2024, 253,426-440
DOI: 10.1039/D4FD00070F, Paper

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Javad Jeddi, Jukka Niskanen, Benoît H. Lessard, Joshua Sangoro
Four model 1,2,3-triazole-based polyILs with polycation or polyanion backbones, are investigated to understand the impact of mobile ion types and backbone chemical structure.
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Faraday Discuss., 2024, 253,79-99
DOI: 10.1039/D4FD00084F, Paper

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J.-F. Dufrêche, B. Siboulet, M. Duvail
Here we examine the question of the chemical models widely used to describe dense solutions, particularly ionic solutions.
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Faraday Discuss., 2024, 253,118-128
DOI: 10.1039/D4FD00083H, Paper

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Matteo Boventi, Michele Mauri, Franca Castiglione, Roberto Simonutti
Type V deep eutectic solvents thymol : camphor, menthol : thymol and eutectic mixtures based on menthol : carboxylic acids with variable chain length, are investigated to clarify the peculiar nanostructure of these materials..
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Faraday Discuss., 2024, 253,11-25
DOI: 10.1039/D4FD00086B, Paper

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Matthew S. Emerson, Raphael Ogbodo, Claudio J. Margulis
This article presents a perspective on what we think are key topics related to the structure and structural dynamics of ILs and to some extent high-temperature molten salts.
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Faraday Discuss., 2024, 253,42-54
DOI: 10.1039/D4FD00050A, Paper

Yasuhiro Umebayashi, Erika Otani, Hikari Watanabe, Jihae Han
Li[(CF₃SO₂)₂N] mixtures with propane sultone or sulfolane, newly termed as glass-forming liquid electrolytes, exhibited large-size aggregate (AGG) formation via speciation and dipole reorientation. The AGGs may be crucial for the unique Li⁺ conduction.
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Faraday Discuss., 2024, 253,510-523
DOI: 10.1039/D4FD00150H, Paper

Rob Atkin
A DIF is a electrolyte where the ion–ion distance is smaller than the Bjerrum length, causing strong electrostatic coupling in correlated domains. Ionic domains may be interspersed with non-polar or immiscible regions.
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Faraday Discuss., 2024, 253,289-313
DOI: 10.1039/D4FD90035A, Discussion

Andrew P. Abbott, Rob Atkin, Duncan W. Bruce, Paola Carbone, Giacomo Damilano, Robert A. W. Dryfe, Jean-Francois Dufrêche, Karen J. Edler, Y. K. Catherine Fung, Kateryna Goloviznina, Margarida Costa Gomes, Alexis Grimaud, Timothy S. Groves, Jennifer M. Hartley, John D. Holbrey, Christian Holm, Pierre Illien, Roland Kjellander, Alexei Kornyshev, Kevin R. J. Lovelock, Daniel M. Markiewitz, Joshua Maurer, Shurui Miao, Naoya Nishi, Beatriz Rocha de Moraes, Bernhard Roling, Benjamin Rotenberg, Joshua Sangoro, Nicolas Schaeffer, Monika Schönhoff, David J. Sconyers, John M. Slattery, Małgorzata Swadźba-Kwaśny, Adriaan van den Bruinhorst, Tom Welton
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Faraday Discuss., 2024, 253,493-509
DOI: 10.1039/D4FD90037E, Discussion

Rob Atkin, Duncan W. Bruce, Robert A. W. Dryfe, Emmanuelle Dubois, Karen J. Edler, Christopher E. Elgar, Andrew Feeney, Kateryna Goloviznina, Timothy S. Groves, Benworth Hansen, John D. Holbrey, Christian Holm, Alexei Kornyshev, Claudio J. Margulis, Daniel M. Markiewitz, Richard P. Matthews, Joshua Maurer, Shurui Miao, Frederik Philippi, Elixabete Rezabal, Bernhard Roling, Benjamin Rotenberg, Joshua Sangoro, Monika Schönhoff, John M. Slattery, Małgorzata Swadźba-Kwaśny, Neave Taylor, Masayoshi Watanabe, Jake Yang
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Faraday Discuss., 2024, 253,407-425
DOI: 10.1039/D4FD90036G, Discussion

Andrew P. Abbott, Rob Atkin, Margarida Costa Gomes, Jean-François Dufrêche, Christopher E. Elgar, Y. K. Catherine Fung, Kateryna Goloviznina, Alexis Grimaud, Benworth Hansen, Jennifer M. Hartley, Christian Holm, Alexei Kornyshev, Kevin R. J. Lovelock, Daniel M. Markiewitz, Joshua Maurer, Shurui Miao, Susan Perkin, Frederik Philippi, Bernhard Roling, Nicolas Schaeffer, Monika Schönhoff, David J. Sconyers, Neave Taylor, Kazuhide Ueno, Adriaan van den Bruinhorst, Masayoshi Watanabe, Yuki Yamada
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Faraday Discuss., 2024, 253,146-180
DOI: 10.1039/D4FD90034K, Discussion

Andrew P. Abbott, Rob Atkin, Muhammad Dabai Bala, Stuart J. Brown, Duncan W. Bruce, Paola Carbone, Franca Castiglione, Margarida Costa Gomes, Jean-François Dufrêche, Karen J. Edler, Andrew Feeney, Kateryna Goloviznina, Juan Luis Gómez-Estévez, Timothy S. Groves, Benworth Hansen, Rachel Hendrikse, Christian Holm, Pierre Illien, Roland Kjellander, Alexei Kornyshev, Claudio J. Margulis, Joshua Maurer, Shurui Miao, Susan Perkin, Elixabete Rezabal, Beatriz Rocha de Moraes, Bernhard Roling, Benjamin Rotenberg, Joshua Sangoro, Nicolas Schaeffer, Monika Schönhoff, Karina Shimizu, John M. Slattery, Neave Taylor, Yasuhiro Umebayashi, Adriaan van den Bruinhorst, Masayoshi Watanabe, Fabian Zills
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Faraday Discuss., 2024, 253,9-10
DOI: 10.1039/D4FD90045F, Editorial

Susan Perkin, Tom Welton
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00093E, Paper

Krzysztof Maziarz, Austin Tripp, Guoqing Liu, Megan Stanley, Shufang Xie, Piotr Gaiński, Philipp Seidl, Marwin H. S. Segler
Syntheseus provides reference models and search algorithms as well as metrics to evaluate and improve synthesis planning tools.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00159A, Paper

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Oluwasegun Wahab, Lane A. Baker
This introductory lecture prefaces the 2024 New Horizons in Nanoelectrochemistry Faraday Discussion.
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Faraday Discuss., 2024, Advance Article
DOI: 10.1039/D4FD00144C, Paper

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Grayson F. Huldin, Junming Huang, Julius Reitemeier, Kaiyu X. Fu
Nafion blocks the aptamer's active sites from planar gold, while the aptamer retains its redox activity from nanoporous gold.
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