To provide a solution conveying and cooling apparatus that enables removal of a deposit of solid material, or a fouling deposit, inside the apparatus with extremely simple work equipment by fewer on-site workers in a short tune without any dangerous work such as hydroblasting. The solution conveying and cooling apparatus has a rigid outer tube for a cooling medium and a plurality of rigid outer tubes for solution arranged parallel to each other inside the rigid outer tube for a cooling medium. A thin inner tube is disposed inside each of the rigid outer tubes for solution, this thin inner tube having an outer diameter smaller than an inner diameter of the rigid outer tube for solution at normal temperature and pressure, and expanding by an increase in at least one of temperature and pressure of a solution conveyed and as a result contacting with an inner surface of the rigid outer tube for solution that is cooled by the cooling medium.

A heat transfer system includes a substrate having a heat exchange region including a surface having an enhancement region including alternating regions of selectively placed plurality of nucleation sites and regions lacking selectively placed nucleation sites, such that bubble formation and departure during boiling of a liquid in contact with the enhancement region induces liquid motion over the surface of the regions lacking selectively placed nucleation sites sufficient to enhance both critical heat flux and heat transfer coefficient at the critical heat flux in the enhancement region of the system.

Coatings for enhancing performance of materials surfaces, methods of producing the coating and coated substrates, and coated condensers are disclosed herein. More particularly, exemplary embodiments provide chemical coating materials useful for coating condenser components.

A heat dissipation module adapted to perform heat dissipation on a heat generating component is provided. The heat dissipation module includes a graphite sheet and an insulating and heat conducting layer. The graphite sheet includes a plurality of through holes, an attaching surface and a heat dissipating surface opposite to the attaching surface, wherein the attaching surface is configured to be attached to the heat generating component. Each of the through holes penetrates the graphite sheet, so the attaching surface and the heat dissipating surface are connected via the through holes. The insulating and heat conducting layer covers the graphite sheet. The insulating and heat conducting layer least covers the attaching surface, the heat dissipating surface and inner walls of the through holes.

A Rack Information Handling System (RIHS) has a liquid cooling subsystem that provides cooling liquid to liquid cooled (LC) nodes received in chassis-receiving bays of a rack. Leak collection structures are positioned to receive cooling liquid that leaks from the liquid cooling subsystem. Liquid sensors detect a presence of leaked cooling liquid in the leak collection structures. A leak detection subsystem responds to a detected presence of liquid by providing a leak indication. In one or more embodiments, the liquid cooling subsystem has a liquid rail formed by more than one rack interconnections vertically aligned in a rear section of the rack that are connected by modular rail conduits for node-to-node fluid transfer. The leak collection structures include a pipe cover received over at least one modular rail conduit. A liquid cavity of each pipe cover spills over into another lower pipe cover at a rate that can be correlated to severity of the leak.

There is disclosed a vehicle air conditioner which is capable of enlarging an effective range of a dehumidifying and heating mode to environmental conditions and smoothly dehumidifying and heating a vehicle interior. A vehicle air conditioner 1 executes a dehumidifying and heating mode in which a controller lets a refrigerant discharged from a compressor 2 radiate heat in a radiator 4, and decompresses the refrigerant by which heat has been radiated and then lets the refrigerant absorb heat in a heat absorber 9 and an outdoor heat exchanger 7, the controller decreases an outdoor blower voltage FANVout of an outdoor blower 15 and decreases an air volume into the outdoor blower 15 in a case where a temperature Te of the heat absorber 9 is high even when the controller adjusts a valve position of an outdoor expansion valve 6 into a lower limit of controlling in a situation in which a temperature TCI of the radiator 4 is satisfactory.

An air conditioning system of a motor vehicle with a refrigerant circuit for operation in a refrigerator mode and a heat pump mode. The refrigerant circuit includes a primary circuit with a compressor, a heat exchanger for heat transfer between the refrigerant and the surroundings, an expansion element and a heat exchanger for heat transfer from the intake air being conditioned for the passenger compartment to the refrigerant, and a first flow path. The flow path extends from a branching point between the compressor and the heat exchanger to an opening and includes a heat exchanger for heat transfer from the refrigerant to the intake air being conditioned for the passenger compartment. The heat exchanger is situated in a flow direction of intake air of the passenger compartment after the heat exchanger.

An automobile interior temperature stabilizer includes a holder adapted for placing within a vehicle cabin and a temperature stabilizing member which is made of latent heat material that absorbs and releases heat without rising in its temperature and is disposed in the holder, wherein the temperature stabilizing member has a threshold temperature range that the temperature stabilizing member is arranged for absorbing cabin heat within the vehicle cabin to cool down the vehicle cabin when an interior temperature of the vehicle is higher than the threshold temperature range, and the temperature stabilizing member is arranged for releasing stored heat to the vehicle cabin to warm the vehicle cabin when an interior temperature of the vehicle is lower than the threshold temperature range. Therefore, the automobile interior temperature stabilizer is able to maintain the cabin temperature of the vehicle without using any power from the vehicle.

An adjustable refrigerant distribution device and a heat exchanger having same. The heat exchanger comprises: first and second collecting pipes; a heat exchanger core body; and a refrigerant distribution device, the refrigerant distribution device comprises a first distribution pipe, a first inlet pipe and a first drive assembly. The pipe wall of the first distribution pipe is provided with a first distribution hole. The first distribution pipe is inserted into at least one of the first and the second collecting pipes. The first inlet pipe is located outside at least one collecting pipe and is in communication with the first distribution pipe, and the first drive assembly drives the first distribution pipe to move relative to at least one collecting pipe. The distribution pipe of the refrigerant distribution device and the heat exchanger can translate along the axial direction, thereby adjusting refrigerant distribution so as to satisfy different distribution requirements.

A digital down converter with an equalizer translates an ADC output signal to a low frequency spectral region, followed by decimation. All operations of correction of the processed signal are carried out with a reduced sampling rate compared with sampling rates of the prior art. Equalization is performed only in a frequency pass band of the down converter. The achieved reduction of the required computation resources is sufficient to enable the down converter with equalization to operate in a real time mode.

Methods and apparatus to parallelize data decompression are disclosed. An example method adjusting a first one of initial starting positions to determine a first adjusted starting position by decoding the bitstream starting at a training position in the bitstream, the decoding including traversing the bitstream from the training position as though first data located at the training position is a valid token; and merging, by executing an instruction with the processor, first decoded data generated by decoding a first segment of the compressed data bitstream starting from the first adjusted starting position with second decoded data generated by decoding a second segment of the compressed data bitstream, the decoding of the second segment starting from a second position in the compressed data bitstream and being performed in parallel with the decoding of the first segment, and the second segment preceding the first segment in the compressed data bitstream.

A circuit includes a time delta detector configured to receive an input clock signal and a reference clock signal and generate a delta pulse signal and a reference pulse signal. A comparison circuit is configured to receive the delta pulse signal and the reference pulse signal. The comparison circuit generates an output indicative of a bit of a time difference between the input clock signal and the reference clock signal. A control circuit is configured to receive the output from the comparison circuit. The control circuit maintains a count of the time difference between the input clock signal and the reference clock signal.

A method for adaptively regulating a coding mode and a digital correction circuit thereof are provided. The method is for a successive-approximation-register analog-to-digital converter (SAR ADC). In the method, whether to regulate a binary weight corresponding to each of digital bits is determined according to the number of completed comparison cycles to provide a first coding sequence. The first coding sequence is directly compensated according to uncompleted comparison cycles to provide a correct digital output code.

An analog to digital converter (ADC) system that includes a first amplifier configured to amplify an analog input signal to produce an amplified direct current (DC) signal, an ADC configured to receive the amplified DC signal and convert the amplified DC signal into a digital DC signal, a digital to analog converter configured to receive the digital DC signal and convert the digital DC signal into an analog DC signal, and a second amplifier configured to receive an analog alternating current (AC) signal comprising the analog DC signal subtracted from the analog input signal and amplify the analog AC signal to produce an amplified AC signal. The ADC is further configured to receive the amplified AC signal and produce a digital AC signal. The second amplifier has a gain greater than a gain of the first amplifier.

Disclosed are methods and systems for significantly compressing sparse multidimensional ordered series data comprised of indexed data sets, wherein each data set comprises an index, a first variable and a second variable. The methods and systems are particularly suited for compression of data recorded in double precision floating point format.

An ultrasound device including an asynchronous successive approximation analog-to-digital converter and method are provided. The device includes at least one ultrasonic transducer, a plurality of asynchronous successive-approximation-register (SAR) analog-to-digital converters (ADC) coupled to the at least one ultrasonic transducer, at least one asynchronous SAR in the plurality having a sample and hold stage, a digital-to-analog converter (DAC), a comparator, and control circuitry, wherein a DAC update event following at least one bit conversion is synchronized to a corresponding DAC update event of at least one other ADC in the plurality of ADCs.

Methods and systems for time interleaved analog-to-digital converter timing mismatch calibration and compensation may include receiving an analog signal on a chip, converting the analog signal to a digital signal utilizing a time interleaved analog-to-digital-converter (ADC), and reducing a blocker signal that is generated by timing offsets in the time interleaved ADC by estimating complex coupling coefficients between a desired digital output signal and the blocker signal utilizing a decorrelation algorithm on frequencies within a desired frequency bandwidth. The decorrelation algorithm may comprise a symmetric adaptive decorrelation algorithm. The received analog signal may be generated by a calibration tone generator on the chip. An aliased signal may be summed with an output signal from a multiplier. The complex coupling coefficients may be determined utilizing the decorrelation algorithm on the summed signals. A multiplier may be configured to cancel the blocker signal utilizing the determined complex coupling coefficients.

A converter includes: a terminal that receives code-modulated power that has been generated with a modulation code; and a circuit that intermittently converts the code-modulated power with a conversion code based on the modulation code. The code-modulated power is alternating-current power.

Aspects of dynamic data compression selection are presented. In an example method, as uncompressed data chunks of a data stream are compressed, at least one performance factor affecting selection of one of multiple compression algorithms for the uncompressed data chunks of the data stream may be determined. Each of the multiple compression algorithms may facilitate a different expected compression ratio. One of the multiple compression algorithms may be selected separately for each uncompressed data chunk of the data stream based on the at least one performance factor. Each uncompressed data chunk may be compressed using the selected one of the multiple compression algorithms for the uncompressed data chunk.

Typically, complex systems require a separate and expensive equalizer at the output of an analog-to-digital converter (ADC). Rather than providing a separate equalizer, the effective Signal Transfer Function (STF) of a Multi-stAge noise SHaping (MASH) ADC can be modified by leveraging available digital filtering hardware necessary for quantization noise cancellation. The modification can involves adding calculations in the software previously provided for computing digital quantization noise cancellation filter coefficients, where the calculations are added to take into account equalization as well. As a result, the signal transfer function can be modified to meet ADC or system-level signal-chain specifications without additional equalization hardware. The method is especially attractive for high-speed applications where magnitude and phase responses are more challenging to meet.

Continuous-time analog-to-digital converters (ADCs) such as continuous-time delta-sigma ADCs and continuous-time pipeline ADCs, has input resistor structure at the input. The input resistor structure is typically tunable, and the tunability is usually provided by metal-oxide semiconductor field effect transistor (MOSFET) switches. Core MOSFETs, which has a terminal-to-terminal voltage

For continuous-time multi-stage noise shaping analog-to-digital converters (CT MASH ADCs), quantization noise cancellation often requires accurate estimation of transfer functions, e.g., a noise transfer function of the front end modulator and a signal transfer function of the back end modulator. To provide quantization noise cancellation, digital quantization noise cancellation filters adaptively tracks transfer function variations due to integrator gain errors, flash-to-DAC timing errors, as well as the inter-stage gain and timing errors. Tracking the transfer functions is performed through the direct cross-correlation between the injected maximum length linear feedback shift registers (LFSR) sequence and modulator outputs and then corrects these non-ideal effects by accurately modeling the transfer functions with programmable finite impulse response (PFIR) filters.

An analog-to-digital converter (ADC) is a device that can include a reference shuffler and a loop filter. An ADC can achieve better performance with incremental adjustment of a pointer of the reference shuffler, changing coefficients of the loop filter, and storing calibration codes of the ADC in a non-volatile memory. By incrementally adjusting a pointer of the reference shuffler, a calibration can be performed more efficiently than with a random adjustment of the pointer. By temporarily changing the loop filter coefficients, a greater amount of activity can be introduced into the loop filter. This activity can allow the calibration to proceed more efficiently. By storing the calibration codes in a non-volatile memory, a search space for calibration codes can be reduced. Thus, a calibration can occur more quickly, and the calibration itself can be improved.

A flash analog-to-digital converter (ADC) includes comparators that convert an analog input signal to a digital output signal. Offsets of these comparators introduce noise and can hurt the performance of the ADC. Thus, these comparators are calibrated using calibration codes. Conventional calibration methods determine these calibration codes by removing the ADC from an input signal. Otherwise, it is difficult to distinguish the noise from the signal in the calibration measurement. In contrast, an embodiment can determine the calibration codes while the ADC converts the input signal to a digital signal. Such an embodiment can be achieved by a frequency-domain technique. In an embodiment employing a frequency-domain power meter, an input signal can be removed from the power measurement. This removal enables accurate measurement of in-band noise without having the measurement be corrupted by input signal power.

For continuous-time multi-stage noise shaping analog to digital converters (CT MASH ADCs), quantization noise cancellation often requires estimation of transfer functions, e.g., a noise transfer function of the front end modulator. To estimate the noise transfer function, a dither signal can be injected in the front end modulator. However, it is not trivial how the dither signal can be injected, since the dither signal can potentially leak to the back end modulator and cause overall noise degradation. To address some of these issues, the dither signal is injected post the flash analog to digital converter (ADC) of the front end modulator. Furthermore, dummy comparator structures can be used to synchronize the dither with the quantization noise of the targeted flash ADC.

A circuit and a method for converting an analog signal to a digital value representation is disclosed. In one aspect, the circuit includes an incremental sigma-delta analog-to-digital converter (ADC). The circuit further includes a first input line for providing a primary analog signal representing a sensor measurement to the incremental sigma-delta ADC. The circuit further includes a second input line for providing a secondary analog signal to the incremental sigma-delta ADC. The incremental sigma-delta ADC receives the primary and secondary analog signals during a first period (TADC1) and a second period (TADC2), respectively. The circuit further includes a filter configured to weight the digital values in a sequence of digital values output by the incremental sigma-delta ADC, and to output a single digital value representing the sensor measurement.

The present disclosure pertains to systems and methods for monitoring a plurality of analog-to-digital converters. In one embodiment, a plurality of input channels may each be in communication with a different phase of a three-phase electric power delivery system. The input channels may be configured to receive analog signals from the different phases. A composite signal subsystem may be configured to generate a composite signal based on the plurality of input channels. An analog-to-digital converter subsystem may be configured to produce a digitized representation of each of the plurality of input channels and a digitized representation of the composite signal. An analog-to-digital converter monitor subsystem may identify an error in the analog-to-digital conversion based on the digitized representation of the composite signal and the digitized representations of the plurality of input channels.

A liquid separator system having a gas phase zone, an aqueous phase zone and a denser liquid zone is used to separate mixtures of fluids. The separator can be used for separating molten sulfur from liquid redox solution or reslurry water. The system includes a vessel with a top part and a bottom part. The vessel has a larger diameter at the top part than at the bottom part. The system also includes an inlet for introducing a redox solution or reslurry water and molten sulfur, which is denser than redox solution or reslurry water, into the vessel. An outlet near the bottom part of the vessel allows a flow of the molten sulfur from the vessel. An interface control structure senses an interface level between the redox solution or reslurry water and the molten sulfur, and the interface control structure controls the flow of molten sulfur from the outlet. The interface control structure is adjusted to optimally alter the vertical height of the interface level within the vessel so that the residence time of the molten sulfur in the vessel does not decrease as the sulfur production throughput decreases, and so that the interface area of the molten sulfur and the redox solution is reduced as the sulfur throughput decreases. A pressure controller monitors the pressure in the vessel and adds or removes gas from a gas phase zone in the vessel to maintain a predetermined pressure regardless of the vertical height of the interface.

Method for producing a uranium concentrate in the form of solid particles, by precipitation from a uranium-containing solution using a precipitating agent, in a vertical reactor comprising a base, a top, a central part, an upper part, and a lower part, the solid particles of the uranium concentrate forming a fluidized bed under the action of a rising liquid current which circulates from the base towards the top of the reactor successively passing through the lower part, the central part and the upper part of the reactor, and which is created by introducing a liquid recycling current (flow) at the base of the reactor, said liquid recycling current being tapped at a first determined level (A) in the upper part of the reactor and sent back without settling to the base of the reactor, excess liquid being also evacuated via an overflow located at a second determined level (B) in the upper part of the reactor; a method in which the upper limit (C) of the fluidized bed of solid particles is controlled so that it is positioned at a level below the first and second determined levels.

The present invention relates to a process for the wet production of granules from powdered materials, in particular raw materials for the production of glass. The process of the invention comprises the following successive steps: (i) the powdered materials to be granulated are divided into at least two portions: a first portion and a second portion; (ii) a binder liquid is added to the first portion of powdered materials; (iii) the first mixture thus obtained is agglomerated in the granulator in order to obtain granules (a); (iv) the second portion of powdered materials is added to the granulator; and (v) the new mixture obtained is agglomerated in the granulator in order to obtain granules (b). This sequenced granulation process allows granules to be obtained that have a degree of moisture that assures their stability and their ease of handling eliminating the drying step.

Method for the production of a coarse-grained ammonium sulphate product by crystallization and installation for carrying out the method from an ammonium sulphate solution in a DTB type crystallizer having an internal suspension circuit and a clarifying zone, from which a clarified partial flow of solution is constantly drawn off into an external circuit, is heated in a heat exchanger to dissolve the solids contained therein and is guided back as a clear solution into the lower region of the crystallizer. A fine crystal suspension flow is drawn off from the clarifying zone as a further partial flow and guided back into the internal circuit of the crystallization stage without any previous dissolution of the solid proportion contained therein.

The invention provides a process comprising: a crystallization step of concentrating and crystallizing the ammonium salt of sulfuric acid from an aqueous solution that contains the ammonium salt of sulfuric acid; a solid-liquid separation step of solid-liquid separating the ammonium salt of sulfuric acid obtained in the crystallization step, and a crystallization mother liquid recycling step of recycling a crystallization mother liquid obtained in the solid-liquid separation step to at least one step selected from the crystallization step and one or more steps that precede the crystallization step, in which not all of the crystallization mother liquid is recycled.

A method of producing a titanium dioxide pigment is provided. Also provided is a method of improving the processability of titanium dioxide particles without adversely affecting the rheological properties of the titanium dioxide particles.

A method of processing bundles of carbon nanotubes (CNTs). Bundles of CNTs are put into a solution and unbundled using sonication and one or more surfactants that break apart and disperse at least some of the bundles into the solution such that it contains individual semiconducting CNTs, individual metallic CNTs, and remaining CNT bundles. The individual CNTs are separated from each other using agarose bead column separation using sodium dodecyl sulfate as a surfactant. Remaining CNT bundles are then separated out by performing density-gradient ultracentrifugation.

Mineral, cosmetic, pharmaceutical, agricultural, nutraceutical, and other compositions are produced using a mineral composition containing minimal concentrations of cadmium, lead, arsenic, and mercury and containing relatively high concentrations of micro and macro mineral elements, of rare earth elements, of calcium, and of silica. The mineral concentrations are produced by processing naturally occurring clay soil to concentrate mineral elements naturally occurring in the soil.

Highly compactable granulations and methods for preparing highly compactable granulations are disclosed. More particularly, highly compactable calcium carbonate granulations are disclosed. The granulations comprise powdered materials such as calcium carbonate that have small median particle sizes. The disclosed granulations are useful in pharmaceutical and nutraceutical tableting and provide smaller tablet sizes upon compression than previously available.

A method of producing a surface-treated carbon black powder dispersion includes subjecting carbon black fine particles having a volume average particle size of 100 nm to 20 μm to wet granulation and drying by heating to obtain granulated carbon black having a hardness of 12 cN or less and a pH of less than 7, grinding the granulated carbon black to obtain a ground product having a volume average particle size of 20 nm to 20 μm, and subjecting the ground product to wet oxidization in an aqueous medium. The resulting surface-treated carbon black powder dispersion exhibits excellent print density, print quality, discharge stability, and storage stability when used as an inkjet printer aqueous black ink.

This invention relates to novel methods for affecting, controlling and/or directing various crystal formation, structure formation or phase formation/phase change reaction pathways or systems by exposing one or more components in a holoreaction system to at least one spectral energy pattern. In a first aspect of the invention, at least one spectral energy pattern can be applied to a crystallization reaction system. In a second aspect of the invention, at least one spectral energy conditioning pattern can be applied to a conditioning reaction system. The spectral energy conditioning pattern can, for example, be applied at a separate location from the reaction vessel (e.g., in a conditioning reaction vessel) or can be applied in (or to) the reaction vessel, but prior to other (or all) crystallization reaction system participants being introduced into the reaction vessel.

A method for growing crystals in solution is suitable for the rapid, controlled and effective preparation of crystals of large dimensions from a solution supersaturated with a compound. The crystal growth is carried out under static conditions. To do this: the growth is performed in a crystallization chamber kept at a constant temperature Tc, which chamber is in fluid communication with a saturation chamber at a temperature Ts, similarly constant and different from Tc, with solubility of the compound at the temperature Ts greater than the solubility of the compound at the temperature Tc. A continuous circulation of the solution between the crystallization and saturation chambers is established, thus maintaining a constant supersaturation rate within the crystallization chamber. Furthermore, the circulating solution is subjected to a treatment for eliminating and inhibiting the formation of aggregates, enabling the nucleation of parasitic crystallites to be inhibited.

The present invention pertains to a process for producing sodium chloride comprising the steps of (i) preparing a brine comprising at least 150 g/l of sodium chloride by dissolving a sodium chloride source in water, (ii) subjecting the resulting brine to a eutectic freeze crystallization step by indirect cooling of said brine, resulting in the formation of ice, sodium chloride dihydrate, and a mother liquor, (iii) separating the sodium chloride dihydrate formed in step (ii) from the ice and optionally mother liquor at the eutectic temperature, such that a sodium chloride dihydrate-rich stream is formed, and (iv) feeding said sodium chloride dihydrate-rich stream to a recrystallizer to form sodium chloride and a mother liquor.

The invention provides a process for increasing the crystallinity of at least one solid material which is less than 100% crystalline, comprising applying ultrasound to the substantially dry solid material.

The present invention relates to compositions and methods to increase the output of a high quality product from the precipitation liquor crystallization process exemplified through the aluminum hydroxide recovery processes such as the Bayer process. The invention is a method of increasing the size of precipitates from a liquor. The invention in one embodiment relates to the use of a crystal growth modifier compositions added to the precipitation process to increase the particle size distribution of the precipitated alumina trihydrate.

A reaction-crystallization apparatus for carrying out reaction and/or solvent extraction and/or crystallization of soluble salts has an upper section having a top and a decanter. The decanter has a vertical vessel having a horizontal weir at the top of the upper section. The top of the upper section has an outlet for removing a light phase at the top of the decanter. The apparatus has a lower section, including a crystallizer. The crystallizer includes: a coaxial draft tube; a feed pipe; an agitator inside the draft tube; and at least one outlet at the bottom for crystal slurry removal. The apparatus has an intermediate section sandwiched between the lower section and the upper section such that the sections are in fluid communication and includes at least one coaxial vertical baffle with a gap between the draft tube and the coaxial vertical baffle and is adjustable by moving the baffle.

A process for the production of sodium carbonate and sodium bicarbonate out of trona, comprising crushing trona ore and dissolving it in a leaching tank containing a solution comprising sodium carbonate and sodium bicarbonate, and an additive selected from the group consisting of: phosphates, phospholipids, carboxylates, carboxilic acids, and combinations thereof, saturated in sodium bicarbonate, in order to produce solid particles suspended in a production solution comprising sodium carbonate, the solid particles containing insoluble impurities and at least 65% by weight of sodium bicarbonate. The solid particles are separated from the production solution containing sodium carbonate. At least part of the production solution containing sodium carbonate is taken out of the leaching tank.

The present invention pertains to a process for producing sodium chloride comprising the steps of: (i) preparing a brine having a sodium chloride concentration which is higher than the sodium chloride concentration of the eutectic point but lower than the sodium chloride concentration of a saturated brine by dissolving a sodium chloride source in water; (ii) cooling the resulting brine by indirect cooling in a self-cleaning fluidized bed heat exchanger/crystallizer to a temperature lower than 0° C. but higher than the eutectic temperature of the resulting brine, thereby forming a slurry comprising sodium chloride dihydrate and a mother liquor; (iii) feeding the sodium chloride dihydrate to a recrystallizer to form sodium chloride and a mother liquor, and (iv) recycling at least part of the mother liquor obtained in step (ii) and/or step (iii) to step (i).

The present invention relates to a process for the preparation of articles of manufacture made of or based on sulphur, which comprises cooling of liquid sulphur in a volume of containment until the sulphur mass solidifies and forming of the product, characterized in that elastic pressure waves are applied to the cooling mass of liquid sulphur to produce a crystalline suspension of solid sulphur in liquid sulphur.

Process for the combined regeneration of at least two soluble salts contained in a residue of an industrial process comprising heavy metals, comprising: adding an amount of reactive aqueous solution needed to completely dissolve the salts which are desired to be regenerated to the residue; subjecting the resulting aqueous suspension to a separation to obtain an aqueous production solution on the one hand and insoluble impurities on the other hand, which are removed; successively subjected the aqueous production solution to at least two selective crystallization steps intended to crystallize, separately, the at least two soluble salts which are desired to be regenerated, which are washed, dried and regenerated separately; and adjusting the concentration of at least one of the soluble salts to be regenerated in the aqueous production solution, at the moment when such solution is subjected to the step of crystallization of this salt, to give rise to the selective crystallization of this salt, by addition of a controlled amount of this salt to the aqueous production solution upstream of the crystallization step.

Titanium dioxide which includes particles having a large major-axis length in a large proportion and comprises columnar particles having a satisfactory particle size distribution. A titanium compound, an alkali metal compound, and an oxyphosphorus compound are heated/fired in the presence of titanium dioxide nucleus crystals having an aspect ratio of 2 or higher to grow the titanium dioxide nucleus crystals. Subsequently, a titanium compound, an alkali metal compound, and an oxyphosphorus compound are further added and heated/fired in the presence of the grown titanium dioxide nucleus crystals. Thus, titanium dioxide is produced which comprises columnar particles having a weight-average major-axis length of 7.0-15.0 μm and in which particles having a major-axis length of 10 μm or longer account for 15 wt. % or more of all the particles.

Provided is a method and an apparatus for purifying potassium nitrate from the solid waste produced by a chemical glass-strengthening process. In the method, the solid waste is melted into a liquid waste at first. Potassium nitrate of various purity grades can be obtained by batch processing the liquid waste through stepwise cooling processes of cooling the liquid waste to a first temperature facilitating the potassium nitrate contained in the liquid waste to be crystallized at a first rate and then cooling the liquid waste to a second temperature close to the freezing point of the potassium nitrate at a second rate that is slower than the first rate. The recovered potassium nitrate from the solid waste can be recycled and reused.

The invention provides a method of agglomeration (10) which has the steps of mixing a feedstock (12) of small particles which have an average particle size of 3 mm or less with a binder (14) which is in the form of a polyvinyl alcohol in the form of an aqueous polyvinyl alcohol solution in a first blender (16) to form a binder mixture (18), reacting a gelling agent (20) with the feedstock and the binder and processing the binder mixture to deliver an agglomerate (22).