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Detection of prostate-specific antigen in semen using DNA aptamers: an application of nucleic acid aptamers in forensic body fluid identification

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00371A, Paper
Tetsuya Satoh, Seiya Kouroki, Yusuke Kitamura, Toshihiro Ihara, Kazutoshi Matsumura, Susumu Iwase
In forensics, body fluid identification plays an important role because it aids in reconstructing the crime scene. Therefore, it is essential to develop simple and reliable techniques for body fluid...
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A dual-functional PDMS-assisted paper-based SERS platform for reliable detection of thiram residue both on fruit surface and in juice

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00483A, Paper
Shuang Lin, Wuliji Hasi, Siqingaowa Han, Xiang Lin, Li Wang
In this work, a dual-functional SERS platform was developed via a paper-based SERS substrate with the aid of hydrophobic Polydimethylsiloxane (PDMS) for effective and reliable measurements of thiram on fruit...
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A novel microfluidic paper-based analytical device based on chemiluminescence for the determination of β-agonists in swine hair

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02754H, Paper
Wei Li, Yong Luo, Xiqing Yue, Junrui Wu, Rina Wu, Yu Qiao, Qing Peng, Bo Shi, Bingcheng Lin, Xu Chen
β-Agonists are illegal feed additives in the feed industries of many countries, especially China.
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A simple and rapid method for blood plasma separation driven by capillary force with an application on protein detection

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00240B, Paper
Qingxue Gao, Yongjia Chang, Qingmei Deng, Hui You
Blood plasma separation is a vital sample pre-treatment procedure for microfluidic devices of blood diagnostic, which requires reliability and speediness. In this work, we propose a novel and simple method...
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Effective methods for the determination of triphenyltin residues in surface water and soil samples by high-performance liquid chromatography with tandem mass spectrometry

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00329H, Paper
Gabriel C. dos Santos, Állisson A. da S. Avellar, Rômulo de O. Schwaickhardt, Nelson M. G. Bandeira, Filipe F. Donato, Osmar D. Prestes, Renato Zanella
Monitoring of triphenyltin (TPhT) in the environment, particularly to control its misuse in agriculture, is of great importance because of its high toxicity.
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Development of a magnetic dispersive micro-solid-phase extraction method based on a deep eutectic solvent as a carrier for the rapid determination of meloxicam in biological samples

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00095G, Paper
Samira Rastbood, Mohammad Reza Hadjmohammadi, Seyedeh Maedeh Majidi
An environmentally friendly magnetic dispersive micro solid phase extraction based on a deep eutectic solvent as a carrier and disperser of adsorbents.
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Rapid detection of quality of Japanese fermented soy sauce using near-infrared spectroscopy

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00521E, Paper
Shuo Wang, Takehiro Tamura, Nobuyuki Kyouno, Xiaofang Liu, Han Zhang, Yoshinobu Akiyama, Jie Yu Chen
The application of NIR spectroscopy has great potential as an alternative quality control method, which provides a robust model for routinely estimating the final quality of soy sauce production rapidly and economically.
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Dopamine-modified magnetic graphene oxide as a recoverable sorbent for the preconcentration of metal ions by an effervescence-assisted dispersive micro solid-phase extraction procedure

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00522C, Paper
Basira Karbalaie, Maryam Rajabi, Bahareh Fahimirad
Nanomagnetic graphene oxide modified with dopamine (GO–Fe3O4–DA) was synthesized via a very simple procedure.
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Chiral separations with crosslinked cellulose derivatives attached onto hybrid silica monolith particles via thiol-ene click reaction

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00772B, Paper
Yuhong Zhou, Qian Liang, Zhilun Zhang, Zhaodi Wang, Mingxian Huang
Hybrid silica monolith containing vinyl groups was synthesized by a sol-gel method and then ground and treated, yielding silica particles with 3-5 μm in particles size and 10-20 nm in...
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A novel hybrid micro extraction for sensitive determination of 17β-Estradiol in water samples

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00581A, Paper
Shivender Singh Saini
A novel and green hybrid of pipette tip micro solid phase extraction (PT-µSPE) and supported liquid extraction (SLE) has been tailored and established for efficient and sensitive determination of 17β-Estradiol...
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Targeted profiling of amino acid metabolome in serum by a liquid chromatography-mass spectrometry method: application to identify potential markers for diet-induced hyperlipidemia

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00305K, Paper
Xiao-fan Wang, You-xi Zhang, Hai-ying Ma
Targeted profiling of amino acid metabolome in serum by LC-MS: application to identify potential markers for diet-induced hyperlipidemia.
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Fast magnetic solid-phase extraction using Fe3O4-NH2@MOF material for monohydroxy polycyclic aromatic hydrocarbons in urine of coke-oven workers

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00449A, Paper
Yahui Wang, Meng Yan, Qianqian Ji, Manman Wang, Qian Wang, Xue-Sheng Wang, Yulan Hao
In this work, magnetic material (Fe3O4-NH2@MIL-101) was successfully prepared, and the material was used as a sorbent for the magnetic solid-phase extraction (MSPE) of trace level monohydroxy polycyclic aromatic hydrocarbons...
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Derivatization and rapid GC—MS screening of chlorides relevant to the Chemical Weapons Convention in organic liquid samples

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00263A, Paper
Open Access
Marja-Leena Kuitunen, Jorgelina Cecilia Altamirano, Peter Siegenthaler, Terhi Hannele Taure, Vesa Mauri Antero Häkkinen, Paula Vanninen
A simple derivatization technique was developed for the analysis of seven Schedule 3 chemicals and one Schedule 2 chemical listed in the Chemical Weapons Conventions (CWC). Phosgene, phosphorus oxychloride, phosphorus...
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Improving the determination of celecoxib in body fluids and pharmaceuticals using a new selective and thermosensitive molecularly imprinted poly(vinylidene fluoride) membrane

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Anal. Methods, 2020, 12,2185-2195
DOI: 10.1039/D0AY00237B, Paper
Negin Yazdanian, Behrouz Akbari-Adergani, Maryam Kazemipour, Homayon Ahmad Panahi, Mehran Javanbakht
Molecularly imprinted membranes that demonstrated high selectivity for celecoxib were synthesized using N-vinylcaprolactam and 2-hydroxyethyl methacrylate.
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Versatile additively manufactured (3D printed) wall-jet flow cell for high performance liquid chromatography-amperometric analysis: application to the detection and quantification of new psychoactive substances (NBOMes)

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Anal. Methods, 2020, 12,2152-2165
DOI: 10.1039/D0AY00500B, Paper
Open Access
Hadil M. Elbardisy, Eduardo M. Richter, Robert D. Crapnell, Michael P. Down, Peter G. Gough, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks
Additive manufacturing is an emerging technology of vast applicability, receiving significant interest in a plethora of industrial and research domains as it allows the translation of designs produced via computer software, into 3D printed objects.
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Quality by Design (QbD) approach for the development of a rapid UHPLC method for simultaneous determination of aglycone and glycoside forms of isoflavones in dietary supplements

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Anal. Methods, 2020, 12,2082-2092
DOI: 10.1039/C9AY02778E, Paper
Kornelija Lasić, Ana Mornar, Biljana Nigović
Systematic development of a UHPLC method by QbD approach as performed for simultaneous determination of aglycone (genistein, daidzein, biochanin A and formononetin) and glycoside (genistin, daidzin, sissotrin, ononin) forms of isoflavones.
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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

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Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
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Aptamer-based fluorometric determination of chloramphenicol by controlling the activity of hemin as a peroxidase mimetic

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00389A, Paper
Ling-Chen Wang, Cheng-Yi Hong, Zheng-Zhong Lin, Xiao-Mei Chen, Zhi-Yong Huang
A method for the aptamer-based determination of chloramphenicol (CAP) was developed by exploiting the peroxidase mimicking activity of hemin.
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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
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Confirmation of brand identification in infant formulas by using near-infrared spectroscopy fingerprints

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00375A, Paper
Shuyi Chang, Chengcheng Yin, Sha Liang, Mei Lu, Ping Wang, Zhicheng Li
The NIR spectra of 12 batches of each stage of Brand A infant formulas.
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Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
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The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00334D, Paper
Hong-Lin Ding, Yan-Qing Pu, Da-Ying Ye, Zi-Yue Dong, Man Yang, Cheng-Wei Lü, Yue An
The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications are shown.
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Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
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Solid-phase microextraction using a β-ketoenamine-linked covalent organic framework coating for efficient enrichment of synthetic musks in water samples

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02755F, Paper
Lian Wen, Peng Wu, Lei-Lei Wang, Li-Zong Chen, Ming-Lin Wang, Xia Wang, Jin-Ming Lin, Ru-Song Zhao
This study indicated the promising applicability of the TpPa-1 as a solid-phase microextraction fiber coating for reliably detecting synthetic musks at trace levels from environmental samples.
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Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
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Facile dispersive solid-phase extraction based on humic acid for the determination of aflatoxins in various edible oils

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00534G, Paper
Ping Liu, Yan-Hua Liao, Hao-Bo Zheng, Yang Tang
Aflatoxins (AFs), as the secondary metabolites produced by some toxigenic fungi of Aspergillus species, are well known to be extremely harmful to humans and animals because of their high toxicity, mutagenicity, carcinogenicity, and teratogenicity.
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Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
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A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

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Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
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Adsorptive removal of Hg2+ from environmental water samples using thioglycerol-intercalated magnetic layered double hydroxides

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Anal. Methods, 2020, 12,2279-2286
DOI: 10.1039/D0AY00448K, Paper
Ali Esrafili, Mahnaz Ghambarian, Mohammad Tajik, Mahroo Baharfar
Herein, the removal of Hg2+ from environmental water samples was carried out using a novel nanoadsorbent based on magnetite nanoparticles coated by a thioglycerol-intercalated layered double hydroxide.
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LC-MS in combination with DMBA derivatization for sialic acid speciation and distribution analysis in fish tissues

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Anal. Methods, 2020, 12,2221-2227
DOI: 10.1039/D0AY00100G, Paper
Junjie Du, Qiwei Zhang, Jianjun Li, Qi Zheng
For sialic acid speciation analysis, DMBA provides superior chromatographic separation efficiency and comparable MS/MS spectra with DMB.
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Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

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Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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What’s novel in the new Eurachem guide on uncertainty from sampling?

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Anal. Methods, 2020, 12,2295-2297
DOI: 10.1039/D0AY90051F, AMC Technical Brief
Analytical Methods Committee, AMCTB No. 96
This Technical Brief aims to explain how the new second edition of the Eurachem guide, Measurement uncertainty arising from sampling, differs significantly from the first edition that was published in 2007.
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Development and validation of a real-time microelectrochemical sensor for clinical monitoring of tissue oxygenation/perfusion

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00206B, Paper
Gama Theophile Gnahoré, Jack L. Kelly, Saidhbhe L. O'Riordan, Fiachra B. Bolger, Michelle M. Doran, Michelle Sands, John P. Lowry
Oxygen is critically important to tissue viability and there is increasing demand for its reliable real-time clinical monitoring in order to prevent, diagnose and treat several pathological disorders, including hypoxia, stroke and reperfusion injury.
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A simple paper-based approach for arsenic determination in water using hydride generation coupled with mercaptosuccinic-acid capped CdTe quantum dots

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00273A, Paper
Oraphan Thepmanee, Kanlaya Prapainop Katewongsa, Obnithi Nooppha, Nuanlaor Ratanawimarnwong, Weena Siangproh, Orawon Chailapakul, Kriangsak Songsrirote
This research aims to develop a simple paper-based device for arsenic detection in water samples where a hydride generation technique coupled with mercaptosuccinic acid-capped CdTe quantum dots (MSA-CdTe QDs) as...
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Dispersive micro-solid phase extraction based on graphene/polydopamine composite for the extraction of pyrethroids in water samples

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00562B, Paper
Qinqin Xu, Kexin Qiao, Chen Yan, Zikai Liu, Runhua Lu, Wenfeng Zhou
In this study, a simple, rapid, precise, and environmentally friendly microextraction named dispersive micro-solid phase extraction based on graphene/polydopamine composite as sorbent was investigated for the analysis of four pyrethroids...
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The application of antibody – aptamer hybrid biosensors in the clinical diagnostics and environmental analysis

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00678E, Critical Review
Marta Jarczewska, Elzbieta Malinowska
The growing number of various diseases and the increase of environmental contamination are the causes for elaboration of novel methods for their detection. The possibility of application of affinity-based biosensors...
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A flower-like Ag coated with molecularly imprinted polymers as surface-enhanced Raman scattering substrate for sensitive and selective detection of glibenclamide

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00575D, Paper
Xiaohui Ren, Xin Li
The flower-like Ag, was formed by nanosheets self-assembly, as SERS active substrate was utilized for preparation of flower-like Ag@molecularly imprinted polymers (MIPs) surface-enhanced Raman scattering (SERS) sensor. Based on the...
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Rapid and colorimetric detection of nucleic acids based on entropy-driven circuit and DNAzyme mediated autocatalytic reaction

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00341G, Paper
Hongli Shi, Jianyuan Dai, fang Wang, Yushun Xia, Dan Xiao, Cuisong Zhou
In this work, a novel, rapid and enzyme-free colorimetric biosensor for nucleic acids detection has been developed based on entropy-driven circuit (EDC) and DNAzyme mediated autocatalytic reaction. Upon sensing of...
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Between Rome and Persia [electronic resource] : the middle Euphrates, Mesopotamia, and Palmyra under Roman control / Peter M. Edwell

By darius.uleth.ca
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London ; New York : Routledge, 2008


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The Oxford handbook of Anglo-Saxon archaeology [electronic resource] / edited by Helena Hamerow, David A. Hinton and Sally Crawford.

By darius.uleth.ca
Published On ::

Oxford : Oxford University Press, 2011.


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Egyptian mummies and modern science [electronic resource] / edited by Rosalie David

By darius.uleth.ca
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Cambridge ; New York : Cambridge University Press, 2008


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Covid-19 Factoid: France and Iran face similar fight, Germany stands out

By www.business-standard.com
Published On :: Tue, 31 Mar 2020 06:35:00 +0530

Around 20 cases are being registered and at least two people are losing their lives almost every minute due to coronavirus across the globe.


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Covid-19 Factoid: Over 3,000 dying daily, and three other data trends

By www.business-standard.com
Published On :: Thu, 02 Apr 2020 06:47:00 +0530

The US, Italy and Spain together share almost half the total Covid-19 cases across the globe


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Covid-19 Factoid: Gap between daily new cases and recoveries widening

By www.business-standard.com
Published On :: Fri, 03 Apr 2020 07:02:00 +0530

The world is adding over 70,000 cases everyday while the daily recoveries are still sub-15,000 on an average in the last three days.


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Covid-19 Factoid: Counting the dead - from the US to Punjab and Iran

By www.business-standard.com
Published On :: Wed, 08 Apr 2020 07:06:00 +0530

The US remains the most affected country with over 340,000 cases and the death toll at over 11,000


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Covid-19 Factoid: Pain and recovery as cases set to cross 1.5 mn mark

By www.business-standard.com
Published On :: Fri, 10 Apr 2020 07:12:00 +0530

Germany, where 40 per cent of all infected persons are recovering, is doing the best by that metric among the five worst-affected nations


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Covid-19 Factoid: Just 3 states account for half of new India cases in Apr

By www.business-standard.com
Published On :: Sat, 11 Apr 2020 06:34:00 +0530

While North America and Europe account for the bulk of all coronavirus cases globally, half of new cases reported in India have come from Delhi, Maharashtra and Tamil Nadu alone


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Covid-19 factoid: Alarm bells ring as India adds 1,500 cases in a day

By www.business-standard.com
Published On :: Sun, 12 Apr 2020 06:34:00 +0530

Country's death toll consistently rising too, taking just two days to add the last 50 fatalities to the total.


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View: What happens if the Covid tax on super-rich becomes a reality

By economictimes.indiatimes.com
Published On :: 2020-05-07T11:04:15+05:30

International instances back higher tax liabilities for the rich at times of exigencies.


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