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Pd-Promoted cross coupling of iodobenzene with vinylgold via an unprecedented phenyl transmetalation from Pd to Au

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC02645J, Communication
Jiwei Wang, Licheng Zhan, Gendi Wang, Yin Wei, Min Shi, Jun Zhang
Oxidative addition of Pd/Au vinylene species with iodobenzene reveals the effect of a strong metallophilic Pd⋯Au interaction on phenyl transmetalation from PdIV to AuI, which allows subsequent reductive elimination of LAuI at Pd and Au.
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A convenient reagent for the conversion of aldoximes into nitriles and isonitriles

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC00188K, Communication
Wei Zhang, Jin-Hong Lin, Pengfei Zhang, Ji-Chang Xiao
Described herein is the convenient transformation of aldoximes into nitriles or isonitriles by slightly modifying reaction conditions.
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Construction of Nanocage-Structured Heterogeneous Binary Metal Sulfides via Step-by-Step Confined Growth for Boosted Lithium Storage Properties

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC00962H, Communication
Rongfang Zhao, Yue Han, Wenlong Li, Jinhua Li, Ming Chen, Lingxin Chen
Nanocage-structured materials-heterogeneous binary metal sulfides (MoS2 and Co9S8) in carbon nanocages (Co9S8/MoS2@CNCs) via step-by-step confined growth display superior Li-storage performance, profiting from the synergistic effect of bimetallic sulfides, high filling...
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Surfactant-free synthesis of ultralong silver nanowires for endurable transparent conducting electrodes

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC01915A, Communication
Sian-Hong Tseng, Lian-Ming Lyu, Kai-Yuan Hsiao, Wan-Hua Ho, Ming-Yen Lu
The present study employed the surfactant-free growth of ultralong (~50 μm) silver nanowires (AgNWs) with high aspect ratio (up to 500) by galvanic replacement. AgNW conducting film were fabricated as...
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Bimolecular Vinylation of Arenes by Vinyl Cations

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02300K, Communication
ZHILONG LI, Vincent Gandon, Christophe Bour
Styrene derivatives can be easily synthesized from vinyl triflates and arenes under mild reaction conditions, using [Li][Al(OC(CF3)3)4] as a catalyst and LiHMDS as a base. This transformation is likely to...
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Fluorescent Molecular Logic Gates based on Photoinduced Electron Transfer (PET) Driven by a Combination of Atomic and Biomolecular Inputs

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC00478B, Communication
Open Access
Glenn Wright, Chaoyi Yao, Tom Moody, A. P. De Silva
Molecular AND logic gates 1, 3, 5 and 7, which are designed according to principles of photoinduced electron transfer (PET) switching, respond to co-existing Candida antarctica lipase B and H+...
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A DNA logic gate with dual-anchored proximity aptamers for accurate identification of circulating tumor cells

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC00564A, Communication
Tianshu Chen, Xin Fu, Qianqian Zhang, Dongsheng Mao, Yuchen Song, Chang Feng, Xiaoli Zhu
We have designed a DNA logic gate that can integrate multiple biomarkers recognition with signal amplification to perform accurate and and sensitive analysis of circulating tumor cells (CTCs). It also...
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Intra-mitochondrial self-assembly to overcome the intracellular enzymatic degradation of L-peptides

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC02029J, Communication
M. T. Jeena, Seokyoung Lee, Ayan Kumar Barui, Seongeon Jin, Yuri Cho, Suk-Won Hwang, Sehoon Kim, Ja-Hyoung Ryu
The design of peptide-based therapeutics is generally based on the replacement of L-amino acids with D-isomers to obtain improved therapeutic efficiency.
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Harnessing chemical exchange: 19F magnetic resonance OFF/ON zinc sensing with a Tm(III) complex

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01876G, Communication
Meng Yu, Da Xie, Rahul T. Kadakia, Weiran Wang, Emily L. Que
A Tm(III) complex displays an “off–on” 19F NMR/MRI response to Zn(II) upon tuning the chemical exchange rate.
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3D spongy nanofiber structure Fe–NC catalysts built by a graphene regulated electrospinning method

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01517B, Communication
Weiyuan Ding, Hongquan Yu, Yu Tang, Zhuxin Li, Bijiao Liu, Dechong Liu, Yuyu Wang, Shu hong Liu, Hong Zhao, Daniel Mandler
A Fe–NC catalyst containing carbon nanotubes, mesopores and macropores with a measurable 3D framework structure was prepared by electrospinning.
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A radical-mediated 1,3,4-trifunctionalization cascade of 1,3-enynes with sulfinates and tert-butyl nitrite: facile access to sulfonyl isoxazoles

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01659D, Communication
Xin Yue, Ming Hu, Xingyi He, Shuang Wu, Jin-Heng Li
An unprecedented indium-promoted three-component 1,3,4-trifunctionalization cascade of 1,3-enynes with sulfinates and tert-butyl nitrite for producing 5-sulfonylisoxazoles via [3+2] annulation is reported.
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Enhancing the catalytic properties of well-defined electrophilic platinum complexes

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01438A, Feature Article
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Pablo Ríos, Amor Rodríguez, Salvador Conejero
Well-defined electrophilic or low-electron count platinum complexes are very versatile catalysts for a variety of chemical transformations.
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Catalytic cycle of carbohydrate dehydration by Lewis acids: structures and rates from synergism of conventional and DNP NMR

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01756F, Communication
Pernille Rose Jensen, Sebastian Meier
Structures and rates in the catalytic cycle of carbohydrate dehydration by Lewis acidic salt are determined through the systematic use of complementary NMR approaches.
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Three component hydroxyletherification and hydroxylazidation of (trifluoromethyl)alkenes: access to α-trifluoromethyl β-heteroatom substituted tertiary alcohols

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC02550J, Communication
Hao Zeng, Chuanle Zhu, Chi Liu, Yingying Cai, Fulin Chen, Huanfeng Jiang
The three component hydroxyletherification and hydroxylazidation reactions of (trifluoromethyl)alkenes are reported, providing various useful α-trifluoromethyl β-heteroatom substituted tertiary alcohols in high yields.
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Enzyme-mimicking accelerated signal enhancement for visually multiplexed quantitation of telomerase activity

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC01951H, Communication
Lu Sun, Qiao Zhao, Xinli Liu, Yongchun Pan, Yanfeng Gao, Jingjing Yang, Yuzhen Wang, Yujun Song
Here, we propose an amplification strategy of enzyme-mimicking accelerated signal enhancement integrated with triple-channel volumetric bar-chart chip for visually multiplexed quantitation of telomerase activity. This platform was used for evaluating...
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Liquid metal exfoliation of two dimensional polydopamine nanosheets for templated assembly of noble metal nanoparticles

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC02108C, Communication
Yong Liu, Juanjuan Li, Wei Zhang
A liquid metal-assisted exfoliation strategy is developed for synthesizing two-dimensional polydopamine nanosheets.
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Correction: Colloidal synthesis of porous red phosphorus nanoparticles as a metal-free electrocatalyst for the hydrogen evolution reaction

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC90201B, Correction
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Cheng-Ying Chan, Chao-Hung Chang, Hsing-Yu Tuan
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Self-assembly of an organometallic Fe9O6 cluster from aerobic oxidation of (tmeda)Fe(CH2tBu)2

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Chem. Commun., 2020, 56,4994-4997
DOI: 10.1039/D0CC00011F, Communication
Jonathan A. Kephart, Zachary Hecht, Brooke N. Livesay, Indrani Bhowmick, Matthew P. Shores, V. Codrina Popescu, Navamoney Arulsamy, Elliott B. Hulley
Aerobic oxidation of (tmeda)Fe(CH2tBu)2 in toluene or THF solution leads to the self-assembly of a magic-sized all-ferrous oxide cluster containing the Fe9O6 subunit and bearing organometallic and diamine ligands.
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Investigation of the cathodic interfacial stability of a nitrile electrolyte and its performance with a high-voltage LiCoO2 cathode

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Chem. Commun., 2020, 56,4998-5001
DOI: 10.1039/D0CC00049C, Communication
Fang Xian, Jiedong Li, Zhenglin Hu, Qian Zhou, Chen Wang, Chenglong Lu, Zhongyi Zhang, Shanmu Dong, Chunbo Mou, Guanglei Cui
We adopted a SN based deep eutectic electrolyte with the SN as the only solvent and found that the high-state Co ion could be reduced by the SN solvent on the interface of the LiCoO2 electrode, causing a reverse phase change of the LiCoO2.
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para-Selective arylation and alkenylation of monosubstituted arenes using thianthrene S-oxide as a transient mediator

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Chem. Commun., 2020, 56,5058-5061
DOI: 10.1039/D0CC00641F, Communication
Xiao-Yue Chen, Xiao-Xue Nie, Yichen Wu, Peng Wang
Using thianthrene S-oxide (TTSO) as a transient mediator, para-arylation and alkenylation of mono-substituted arenes have been demonstrated via a para-selective thianthrenation/Pd-catalyzed thio-Suzuki–Miyaura coupling sequence under mild conditions.
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Electrochemically generated N-iodoaminium species as key intermediates for selective methyl sulphonylimination of tertiary amines

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Chem. Commun., 2020, 56,5010-5013
DOI: 10.1039/C9CC09869K, Communication
Binbin Huang, Chao Yang, Jia Zhou, Wujiong Xia
This study presents a straightforward protocol for approaching N-sulphonylamidines via an electricity-driven, iodine-mediated cross dehydrogenative condensation (CDC) between sulphonamides and tertiary amines.
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1,6-Conjugate addition initiated formal [4+2] annulation of p-quinone methides with sulfonyl allenols: a unique access to spiro[5.5]undeca-1,4-dien-3-one scaffolds

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Chem. Commun., 2020, 56,5022-5025
DOI: 10.1039/D0CC01005G, Communication
Ganesh S. Ghotekar, Sachin R. Shirsath, Aslam C. Shaikh, M. Muthukrishnan
An expedient one-pot synthesis of carbocyclic spiro[5.5]undeca-1,4-dien-3-ones via 1,6-conjugate addition initiated formal [4+2] annulation sequences by employing p-quinone methides and sulfonyl allenols.
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Synthetic method, growth mechanism and electrochemical properties of PbSnS2 nanosheets for supercapacitors

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Chem. Commun., 2020, 56,5062-5065
DOI: 10.1039/D0CC01011A, Communication
Yuhan Zeng, Hehe Huang, Shenhu Huang, Tongtong Jiang, Zekai Fang, Lin Li, Yuming Dai
Facile hydrothermally synthesized PbSnS2 nanosheets with various morphologies were developed to obtain high performance electrode materials for supercapacitors.
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Solvent-driven migration of highly polar monomers into hydrophobic PDMS produces a thick graft layer via subsurface initiated ATRP for efficient antibiofouling

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Chem. Commun., 2020, 56,5030-5033
DOI: 10.1039/D0CC00768D, Communication
Xin Yu, Yang Yang, Wufang Yang, Xungai Wang, Xin Liu, Feng Zhou, Yan Zhao
Organic solvents that possess affinity towards both polar monomers and hydrophobic PDMS play a “driving” role in the diffusion of polar monomers into the subsurface of the PDMS substrate.
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Live cell fluorescent stain of bacterial curli and biofilm through supramolecular recognition between bromophenol blue and CsgA

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Chem. Commun., 2020, 56,5014-5017
DOI: 10.1039/D0CC01643H, Communication
Lixia Zhang, Zhenhua Li, Zhijun Chen
A curli fluorescent light-up probe called bromophenol blue, which binds to curli via recognizing CsgA.
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Synthesis of functionalized tetrahydropyrans via cascade cycloaddition involving silyloxyallyl cation intermediates

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Chem. Commun., 2020, 56,5034-5037
DOI: 10.1039/D0CC01796E, Communication
Fatimat O. Badmus, Joshua A. Malone, Frank R. Fronczek, Rendy Kartika
An expedient synthesis of highly substituted tetrahydrobenzofuran via an unsymmetrical silyloxyallyl cation is reported.
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Modulation of an intermediate layer between NiCoP and Ni foam substrate in a microwire array electrode for enhancing the hydrogen-evolution reaction

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Chem. Commun., 2020, 56,4990-4993
DOI: 10.1039/D0CC01488E, Communication
Dan Guo, Huayu Chen, Hanmin Tian, Shuxin Ouyang, Jianbo Wang, Jun Lv
A strategy involving modulating the intermediate layer of an electrode was developed to promote the electrocatalysis kinetics of the electrode and therefore enhance its performance.
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Ring-opening iodination and bromination of unstrained cycloalkanols through β-scission of alkoxy radicals

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Chem. Commun., 2020, 56,5002-5005
DOI: 10.1039/D0CC01720E, Communication
Jiang-Ling Shi, Yuankai Wang, Zixuan Wang, Bowen Dou, Jianbo Wang
Ring-opening iodination or bromination of unstrained cycloalkanols with NaI or NaBr and PhI(OAc)2 under visible light irradiation is developed.
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Highly selective hydrosilylation of equilibrating allylic azides

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Chem. Commun., 2020, 56,5038-5041
DOI: 10.1039/D0CC01316A, Communication
Ruzhang Liu, Zhen Wei, Juan Wang, Yongmei Liu, Huaiguo Xue
Pt-catalyzed hydrosilylation of equilibrating allylic azides provides 3-azidopropansilanes with high chemoselectivity, regioselectivity, and excellent functional group tolerance.
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A multipedal DNA walker for amplified detection of tumor exosomes

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Chem. Commun., 2020, 56,4982-4985
DOI: 10.1039/D0CC01817A, Communication
Peng Miao, Yuguo Tang
A novel electrochemical biosensor for exosomes is proposed based on a multipedal DNA walking strategy. A limit of detection down to 6/μL is obtained with excellent selectivity.
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Catalytic asymmetric synthesis of diazabicyclo[3.1.0]hexanes by 1,3-dipolar cycloaddition of azomethine ylides with azirines

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Chem. Commun., 2020, 56,5050-5053
DOI: 10.1039/D0CC01061H, Communication
Alba Molina, Sergio Díaz-Tendero, Javier Adrio, Juan C. Carretero
A practical CuI/(R)-Fesulphos catalyzed 1,3-dipolar cycloaddition of azomethine ylides with azirines has been developed to produce highly valuable enantioenriched diazabicyclo[3.1.0]hexanes.
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Al centre-powered graphitic nanozyme with high catalytic efficiency for pH-independent chemodynamic therapy of cancer

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01331E, Communication
Jun Li, Ke Yi, Yanli Lei, Zhihe Qing, Zhen Zou, Yuedong Zhang, Haiyan Sun, Ronghua Yang
In this work, an Al centre-powered graphitic nanozyme (Fe/Al-GNE) was developed for chemodynamic cancer therapy, which afforded pH-independent catalytic activity and high reaction kinetics.
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Improving the structural and cyclic stabilities of P2-type Na0.67MnO2 cathode material via Cu and Ti co-substitution for sodium ion batteries

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC01442G, Communication
Xueping Zhang, Feilong Qiu, Kezhu Jiang, Ping He, Min Han, Shaohua Guo, Haoshen Zhou
An air-stable Na0.67Mn0.7Cu0.15Ti0.15O2 (NMCT) has been synthesized using a solid-state method. And it showed the excellent performance as a cathode material for sodium ion batteries.
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Facile construction of double network cross-linked luminescent supramolecular elastomer from hydrosilylation and pillar[5]arene host–guest recognition

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02214D, Communication
Rong Fu, Junying Zhang, Shaojie Liu, Xing-Dong XU, Shengyu Feng
Reticulated copolymer hosts pillar[5]arene crosslinked with poly(dimethylsiloxane) (PDMS) were synthesized for the facile construction of double network crosslinked elastomer upon noncovalently cross-linking with tetraphenyethylene (TPE)-based tetratopic guests through host-guest interactions....
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Control of microenvironment around enzymes by hydrogels

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC01332C, Communication
Yuichiro Kobayashi, Kenji Kohara, Yusuke Kiuchi, Hiroki Onoda, Osami Shoji, Hiroyasu Yamaguchi
We prepared enzyme immobilized hydrogels and investigated the effects of the cross-linking density and polymer properties on their oxidation reaction rate. The oxidation rate of enzyme immobilized hydrogels increased as...
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Is breaking of a hydrogen bond enough to lead to drug resistance?

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02164D, Communication
María José Dávila-Rodríguez, Thales Souza Freire, Erik Lindahl, Ignez Caracelli, Júlio Zukerman-Schpector, Ran Friedman
Drug resistance is a serious problem in cancer, viral, bacterial, fungal and parasitic diseases. Examination of crystal structures of protein-drug complexes is often not enough to explain why a certain...
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Efficient generation of sulfate radicals in Fe (II)/S (IV) system induced by WS2 nanosheets and examined by its intrinsic chemiluminescence

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC01999B, Communication
Tong Sun, Yingying Su, Houjing Liu, Hongjie Song, Yi Lv
In this study, more 〖SO〗_4^( ∙-) and strong intrinsic chemiluminescence (CL) can be achieved through activating sulphite (〖SO〗_3^( 2-)) with ferrous ions (Fe2+) on the WS2 nanosheets with the thickness...
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Rh(III)-catalyzed sequential ortho- C–H oxidative arylation/cyclization of sulfoxonium ylides with quinones toward 2-hydroxy-dibenzo[b,d]pyran-6-ones

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC00176G, Communication
Yaqun Dong, Jin-Tao Yu, Song Sun, Jiang Cheng
A rhodium(III)-catalyzed ortho- C−H functionalization of sulfoxonium ylides followed by intramolecular annulation reactions with quinones is described, where the carbonyl in sulfoxonium ylides served as a chelation group. This protocol...
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Superstructural diversity in salt-cocrystals: higher-order hydrogen-bonded assemblies formed using U-shaped dications and with assistance of π(-)−π stacking

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02671A, Communication
Shweta P. Yelgaonkar, Daniyal Kiani, Jonas Baltrusaitis, Len R MacGillivray
Salt cocrystals with components that assemble by hydrogen bonds and aromatic anion-molecule stacks (π(−)−π stacks) are reported. U-shaped bipyridines and an isocoumarin carboxylic acid self-assemble to form 5-, 6-, and...
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Engineering of Decameric D-fructose-6-phosphate Aldolase A by Combinatorial Modulation of Inter- and Intra-subunit Interactions

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02437F, Communication
Xiaohong Yang, Lian Wu, Aipeng Li, Lidan Ye, Jiahai Zhou, Hongwei Yu
Combinatorial modulation of inter- and intra-subunit interactions on decameric D-fructose-6-phosphate aldolase A (FSAA) generated a triple-site variant I31T/Q59T/I195Q FSAA with 27 to 278-fold activity improvement towards target heteroaromatic aldehydes. X-ray...
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Integration of ultra-high-pressure liquid chromatography-tandem mass spectrometry with machine learning for identifying fatty acid metabolite biomarkers of ischemic stroke

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02329A, Communication
Lijian Zhang, Fei Ma, Ao Qi, Lulu Liu, Junjie Zhang, Simin Xu, Qisheng Zhong, Yusen Chen, Chun-yang Zhang, Chun Cai
We report for the first time the integration of ultra-high-pressure liquid chromatography-tandem mass spectrometry with machine learning for identifying fatty acid metabolite biomarkers of ischemic stroke. Especially, we develop an...
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Rotation of a helical coordination polymer by mechanical grinding

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Chem. Commun., 2020, Advance Article
DOI: 10.1039/D0CC02158J, Communication
Bibhuti Bhusan Rath, Goutam Kumar Kole, Samuel Alexander Morris, Jagadese J. Vittal
Mechanical grinding causes anisotropic cell volume expansion, which facilitates the misaligned arms containing olefin functional groups in the neighbouring strands of the photo-inert helical coordination polymer to align to undergo [2+2] cycloaddition reaction.
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Single molecule magnet behaviour in a square planar S = 1/2 Co(II) complex and spin-state assignment of multiple relaxation modes

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC01854F, Communication
Indrani Bhowmick, David Washburn Shaffer, Jenny Y Yang, Matthew Shores
We report the first example of field-induced single molecule magnet (SMM) behaviour in a square-planar S = ½ Co(II) pincer complex [(PNNNP)CoBr]Br (2). The related five-coordinate complexes [(PCNCP)CoBr2] (1) and...
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Helicity of a polyacetylene directed by molecular recognition of biscalixarene and fullerene

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Chem. Commun., 2020, Accepted Manuscript
DOI: 10.1039/D0CC02506B, Communication
Takehiro Hirao, Yoshiki Iwabe, Naoyuki Hisano, Takeharu HAINO
Chiral biscalixarenes and a C60-appended polyphenylacetylene have been synthesized. The chiral biscalixarene encapsulated the C60 unit of the phenylpolyacetylene, which induced the preferred helicity of the polyacetylene.
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Save the pixel : the art of simple web design / Ben Hunt

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Hunt, Ben (Ben R.)


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The language of advertising [videorecording]

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The enigma of web interfaces : cultural aspects of web site design / by Linda Lim Mei Luan

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Lim, Linda Mei Luan


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Sams teach yourself Microsoft Expression web 4 in 24 hours / Morten Rand-Hendriksen

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Rand-Hendriksen, Morten


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NoSQL distilled : a brief guide to the emerging world of polyglot persistence / Pramod J. Sadalage, Martin Fowler

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Sadalage, Pramod J


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Five hundred years of printing / S.H. Steinberg

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Steinberg, S. H. (Sigfrid Henry), 1899-1969


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