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Quality by Design (QbD) approach for the development of a rapid UHPLC method for simultaneous determination of aglycone and glycoside forms of isoflavones in dietary supplements

Anal. Methods, 2020, 12,2082-2092
DOI: 10.1039/C9AY02778E, Paper
Kornelija Lasić, Ana Mornar, Biljana Nigović
Systematic development of a UHPLC method by QbD approach as performed for simultaneous determination of aglycone (genistein, daidzein, biochanin A and formononetin) and glycoside (genistin, daidzin, sissotrin, ononin) forms of isoflavones.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Discrimination between fresh, chilled, and frozen/thawed chicken based on its skin's spectrochemical and optical properties

Anal. Methods, 2020, 12,2093-2101
DOI: 10.1039/D0AY00324G, Paper
Omnia Hamdy, Zienab Abdel-Salam, Mohamed Abdel-Harith
Monitoring of the spectrochemical and optical properties of biomaterials has been widely utilized in many biomedical applications for both diagnosis and therapy.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
To cite this article before page numbers are assigned, use the DOI form of citation above.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00334D, Paper
Hong-Lin Ding, Yan-Qing Pu, Da-Ying Ye, Zi-Yue Dong, Man Yang, Cheng-Wei Lü, Yue An
The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications are shown.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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One-step synthesis of mitochondrion-targeted fluorescence carbon dots and fluorescent detection of silver ions

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00622J, Paper
Yue Hou, Hanxiao Liu, Zhanxian Li, Hongyan Zhang, Liuhe Wei, Mingming Yu
Silver ions (Ag+) are the most representative harmful ions found in water pollution and widely used in many industries, excessive ingestion of Ag+ in the human body may interact with...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Sample treatment based on molecularly imprinted polymers for the analysis of veterinary drugs in food samples: a review

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00533A, Critical Review
Israel Samuel Ibarra, J. M. Miranda, Irma Perez, Aldo C Jardinez, Gabriela Islas
The use of veterinary drugs in medical treatments and in the livestock industry is a recurrent practice. In subtherapeutic doses during prolonged times act to growth promoters. Residues of these...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
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Facile dispersive solid-phase extraction based on humic acid for the determination of aflatoxins in various edible oils

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00534G, Paper
Ping Liu, Yan-Hua Liao, Hao-Bo Zheng, Yang Tang
Aflatoxins (AFs), as the secondary metabolites produced by some toxigenic fungi of Aspergillus species, are well known to be extremely harmful to humans and animals because of their high toxicity, mutagenicity, carcinogenicity, and teratogenicity.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Droplet image analysis with user-friendly freeware CellProfiler

Anal. Methods, 2020, 12,2287-2294
DOI: 10.1039/D0AY00031K, Technical Note
Simona Bartkova, Marko Vendelin, Immanuel Sanka, Pille Pata, Ott Scheler
We show how to use free open-source CellProfiler for droplet microfluidic image analysis.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
The content of this RSS Feed (c) The Royal Society of Chemistry




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LC-MS in combination with DMBA derivatization for sialic acid speciation and distribution analysis in fish tissues

Anal. Methods, 2020, 12,2221-2227
DOI: 10.1039/D0AY00100G, Paper
Junjie Du, Qiwei Zhang, Jianjun Li, Qi Zheng
For sialic acid speciation analysis, DMBA provides superior chromatographic separation efficiency and comparable MS/MS spectra with DMB.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Development and validation of a real-time microelectrochemical sensor for clinical monitoring of tissue oxygenation/perfusion

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00206B, Paper
Gama Theophile Gnahoré, Jack L. Kelly, Saidhbhe L. O'Riordan, Fiachra B. Bolger, Michelle M. Doran, Michelle Sands, John P. Lowry
Oxygen is critically important to tissue viability and there is increasing demand for its reliable real-time clinical monitoring in order to prevent, diagnose and treat several pathological disorders, including hypoxia, stroke and reperfusion injury.
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ELISA as an effective tool to determine spatial and seasonal occurrence of emerging contaminants in the aquatic environment

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00426J, Paper
Carla Patrícia Silva, Tânia Carvalho, Rudolf J. Schneider, Valdemar I. Esteves, Diana L. D. Lima
Monitoring emerging contaminants is essential as they represent a risk to the aquatic environment. ELISA is a promising method for their quantification mostly because it allows controlling their concentration levels through large screening campaigns.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Dispersive micro-solid phase extraction based on graphene/polydopamine composite for the extraction of pyrethroids in water samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00562B, Paper
Qinqin Xu, Kexin Qiao, Chen Yan, Zikai Liu, Runhua Lu, Wenfeng Zhou
In this study, a simple, rapid, precise, and environmentally friendly microextraction named dispersive micro-solid phase extraction based on graphene/polydopamine composite as sorbent was investigated for the analysis of four pyrethroids...
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The application of antibody – aptamer hybrid biosensors in the clinical diagnostics and environmental analysis

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00678E, Critical Review
Marta Jarczewska, Elzbieta Malinowska
The growing number of various diseases and the increase of environmental contamination are the causes for elaboration of novel methods for their detection. The possibility of application of affinity-based biosensors...
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Digital Reference Section (DRS) Virtual Programs: New blog post invites readers to "Sample a Taste of History This Thanksgiving"

Find a new and historic recipe for a dish to put on your Thanksgiving table in What Mrs. Fisher Knows About Old Southern Cooking. This cookbook, published in 1881, is highlighted in a recent post on the Library of Congress Blog. Abby Fisher perfected her culinary skills as an enslaved cook on a South Carolina plantation but went on to establish a successful catering business in San Francisco and publish a compilation of her recipes—one of the first by an African-American. Learn more about this remarkable woman and, this Thanksgiving, sample a taste of history!

Click here to go to the Library of Congress Blog post, "Sample a Taste of History This Thanksgiving!"




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May 30 Webinar: Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

Reminder!!

Please join us for our May topical webinar:

Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

May 2019 marks the 200th anniversary of the birth of poet Walt Whitman, who revolutionized the style and content of American poetry with his 1855 publication of Leaves of Grass. Whitman was also a journalist, printer, publisher, orator, and prose writer.

The Library of Congress holds the largest group of Whitman-related special collection materials in the world, including printed materials, rare books, photographs, and manuscripts. In this webinar program, Manuscript Division historian Barbara Bair highlights the content and research use of three digitized Whitman manuscript collections as well as programs celebrating Whitman’s birthday at the Library of Congress.

Date: Thursday, May 30
Time
: 1:00 pm – 2:00 pm EDT
Registration (required): Please register via Eventbrite.

This program will be held in real time via webinar software, which allows participants from around the country and the world to join us. Confirmation and log-on instructions will be sent via email. Please read the Library of Congress Comment and Posting Policy.

ADA: Request ADA accommodations five days in advance at (202) 707-6362 or ada@loc.gov. Registration for the program is also required.

Questions? Ask A Librarian!

 




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Perils of Perestroika : viewpoints from the Soviet press, 1989-1991 / edited by Isaac J. Tarasulo.

Wilmington, Del. : SR Books, 1992




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A history of ancient Moab from the Ninth to First centuries BCE [electronic resource] / by Burton MacDonald.

Atlanta : SBL Press, [2020]




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The Oxford handbook of Roman Egypt [electronic resource] / edited by Christina Riggs.

Oxford : Oxford University Press, 2012.




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Recharting the Black Atlantic [electronic resource] : modern cultures, local communities, global connections / edited by Annalisa Oboe and Anna Scacchi

New York : Routledge, 2008




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GSTN Helpdesk handles over 56,000 taxpayer issues in one month of lockdown

GST Network Helpdesk on Sunday said it has handled over 56,000 taxpayer issues in one month since the nationwide lockdown was imposed on March 25.




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I-T dept, GSTN, CBIC caution people against phishing emails promising refunds

Separately GST Network, the company handling the technology backbone for Goods and Services Tax, cautioned against a fraud website onlinefilingindia.in asking taxpayers not to reveal personal and bank details.




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Govt to gain Rs 1.6 lakh cr this fiscal from record excise duty hike on petrol, diesel

The cash-strapped government will gain close to Rs 1.6 lakh crore in additional revenues this fiscal from a record increase in excise duty on petrol and diesel, that will help make up for revenue it lost in a slowing economy and shutting down of businesses due to coronavirus lockdown.




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Toll collections to see 13% drop due to 57-day coronavirus lockdown: CRISIL Research

With the nationwide lockdown to fight the COVID-19 pandemic restricting inter- and intra-state traffic to essential services, toll collections from build-operate-transfer (BOT) highway projects, and remittances from publicly funded projects would decline sharply in the near term, Crisil report said.




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Investors in FPIs and PE funds go back on payment commitment amid Covid-19 uncertainty

Several sovereign wealth funds, pension funds, university endowments, limited partners, corporate investors and high net worth individuals have reached out to FPIs and PE fund managers in the last few weeks to convey their decision to partially or fully defer their commitments, people in the know said.




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Record excise duty hike unlikely to help bridge fiscal gap: Report

Following the record hike in excise duty on petrol and diesel, the total incidence of taxation on auto fuels jumped to 70 per cent of the retail price. But the retail prices are not impacted as the hike completely wipes out the fall in crude prices.




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Covid alters India's borrowing plan, target now raised to Rs 12L cr

Govt will borrow Rs 6L cr from the market via gilts through the remaining part of the first half of the year.




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Statistical Analysis of Network Data with R [electronic resource] / by Eric D. Kolaczyk, Gábor Csárdi

New York, NY : Springer New York : Imprint: Springer, 2014




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Stochastic Processes and Applications [electronic resource] : Diffusion Processes, the Fokker-Planck and Langevin Equations / by Grigorios A. Pavliotis

New York, NY : Springer New York : Imprint: Springer, 2014




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Statistical Methods for Ranking Data [electronic resource] / by Mayer Alvo, Philip L.H. Yu

New York, NY : Springer New York : Imprint: Springer, 2014




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R for Cloud Computing [electronic resource] : An Approach for Data Scientists / by A Ohri

New York, NY : Springer New York : Imprint: Springer, 2014




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Topics in Statistical Simulation [electronic resource] : Research Papers from the 7th International Workshop on Statistical Simulation / edited by V.B. Melas, Stefania Mignani, Paola Monari, Luigi Salmaso

New York, NY : Springer New York : Imprint: Springer, 2014




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Longitudinal Categorical Data Analysis [electronic resource] / by Brajendra C. Sutradhar

New York, NY : Springer New York : Imprint: Springer, 2014




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Analysis and Geometry of Markov Diffusion Operators [electronic resource] / by Dominique Bakry, Ivan Gentil, Michel Ledoux

Cham : Springer International Publishing : Imprint: Springer, 2014




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German-Japanese Interchange of Data Analysis Results [electronic resource] / edited by Wolfgang Gaul, Andreas Geyer-Schulz, Yasumasa Baba, Akinori Okada

Cham : Springer International Publishing : Imprint: Springer, 2014




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The Contribution of Young Researchers to Bayesian Statistics [electronic resource] : Proceedings of BAYSM2013 / edited by Ettore Lanzarone, Francesca Ieva

Cham : Springer International Publishing : Imprint: Springer, 2014




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Foundations of Applied Statistical Methods [electronic resource] / by Hang Lee

Cham : Springer International Publishing : Imprint: Springer, 2014




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Contemporary Developments in Statistical Theory [electronic resource] : A Festschrift for Hira Lal Koul / edited by Soumendra Lahiri, Anton Schick, Ashis SenGupta, T.N. Sriram

Cham : Springer International Publishing : Imprint: Springer, 2014




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A Chronicle of Permutation Statistical Methods [electronic resource] : 1920–2000, and Beyond / by Kenneth J. Berry, Janis E. Johnston, Paul W. Mielke Jr

Cham : Springer International Publishing : Imprint: Springer, 2014




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Excel 2010 for Engineering Statistics [electronic resource] : A Guide to Solving Practical Problems / by Thomas J. Quirk

Cham : Springer International Publishing : Imprint: Springer, 2014




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Modern Stochastics and Applications [electronic resource] / edited by Volodymyr Korolyuk, Nikolaos Limnios, Yuliya Mishura, Lyudmyla Sakhno, Georgiy Shevchenko

Cham : Springer International Publishing : Imprint: Springer, 2014




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Statistical Theory and Inference [electronic resource] / by David J. Olive

Cham : Springer International Publishing : Imprint: Springer, 2014




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New Advances in Statistical Modeling and Applications [electronic resource] / edited by António Pacheco, Rui Santos, Maria do Rosário Oliveira, Carlos Daniel Paulino

Cham : Springer International Publishing : Imprint: Springer, 2014




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Person-Centered Methods [electronic resource] : Configural Frequency Analysis (CFA) and Other Methods for the Analysis of Contingency Tables / by Mark Stemmler

Cham : Springer International Publishing : Imprint: Springer, 2014