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[ASAP] Nontraditional Application of the Photo-Fenton Process: A Novel Strategy for Molecular Construction Using Formamide and Flow Chemistry

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Published On :: Mon, 13 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00057


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[ASAP] Reductive Amination Bicarbonate Quench: Gas-Evolving Waste Stream Near-Miss Investigation

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Published On :: Thu, 16 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00085


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[ASAP] Investigating Process Variables and Additive Selection To Optimize Polymorphic Control of Carbamazepine in a CO<sub>2</sub> Antisolvent Crystallization Process

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Published On :: Wed, 22 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00545


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[ASAP] Photo-oxidation of Cyclopentadiene Using Continuous Processing: Application to the Synthesis of (1<italic toggle="yes">R</italic>,4<italic toggle="yes">S</italic>)-4-Hydroxycyclopent-2-en-1-yl Acetate

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Published On :: Wed, 22 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00066


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[ASAP] Efficient Kinetic Data Acquisition and Model Prediction: Continuous Flow Microreactors, Inline Fourier Transform Infrared Spectroscopy, and Self-Modeling Curve Resolution

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Published On :: Mon, 27 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00037


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[ASAP] Improved Synthesis of 6-Chloro-5-methylpyridin-2-amine: A Key Intermediate for Making Lumacaftor

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Published On :: Tue, 28 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00556


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[ASAP] <italic toggle="yes">N</italic>-Acyl-5,5-Dimethylhydantoins: Mild Acyl-Transfer Reagents for the Synthesis of Ketones Using Pd–PEPPSI or Pd/Phosphine Catalysts

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Published On :: Tue, 28 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00054


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[ASAP] Drug Loading and Dissolution Properties of Dalcetrapib–Montmorillonite Nanocomposite Microparticles

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Published On :: Wed, 29 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00460


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[ASAP] Bromine–Lithium Exchange on a <italic toggle="yes">gem</italic>-Dibromoalkene, Part 2: Comparative Performance of Flow Micromixers

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Published On :: Thu, 30 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00203


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[ASAP] Upscaling Photoredox Cross-Coupling Reactions in Batch Using Immersion-Well Reactors

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Published On :: Thu, 30 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00070


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[ASAP] Continuous Process for Preparing the Difluoromethylating Reagent [(DMPU)<sub>2</sub>Zn(CF<sub>2</sub>H)<sub>2</sub>] and Improved Synthesis of the ICHF<sub>2</sub> Precursor

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Published On :: Tue, 05 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00089


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[ASAP] Development and Production of an Enantioselective Tetrahydroisoquinoline Synthesis Enabled by Continuous Cryogenic Lithium–Halogen Exchange

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Published On :: Tue, 05 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00141


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[ASAP] Some Items of Interest to Process R&D Chemists and Engineers

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Published On :: Tue, 05 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00197


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[ASAP] <sc>d</sc>-Serine as a Key Building Block: Enzymatic Process Development and Smart Applications within the Cascade Enzymatic Concept

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Published On :: Thu, 07 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00024


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[ASAP] Correction to “Application of Crabtree/Pfaltz-type Iridium Complexes for the Catalyzed Asymmetric Hydrogenation of an Agrochemical Building Block”

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Published On :: Fri, 08 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00206


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[ASAP] Catalyst-Free Cyclization- and Curtius Rearrangement-Induced Functional Group Transformation: An Improved Synthetic Strategy of First-in-Class ATX Inhibitor Ziritaxestat (GLPG-1690)

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Published On :: Fri, 08 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00511


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Atomic-scale engineering of metal–oxide interfaces for advanced catalysis using atomic layer deposition

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00304B, Perspective
Lina Cao, Junling Lu
Two main routes to optimization of metal–oxide interfaces: reducing metal particle size and oxide overcoating.
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Enhancing aqueous pollutants photodegradation via Fermi level matched Z-scheme BiOI/Pt/g-C3N4 photocatalyst: unobstructed photogenerated charge behavior and degradation pathway exploration

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00429D, Paper
Jingjing Jiang, Yueyu Song, Xingyue Wang, Tianren Li, Mingyu Li, Yanhong Lin, Tengfeng Xie, Shuangshi Dong
Z-scheme photocatalytic system was widely requisited to solve water pollution problem. However, the degradation mechanism for pollutants with Z-scheme photocatalyst has been ambiguous. In this work, an efficient all solid-state...
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Superior adsorption capability and excellent photocatalytic activity derived from the ferroelectric external screening effect in Bi3TiNbO9 single-crystal nanosheets

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/C9CY02513H, Paper
Xiaofeng Yin, Yingjie Sun, Xiaojun Wu, Xiaoning Li, Huan Liu, Wen Gu, Wei Zou, Liuyang Zhu, Zhengping Fu, Yalin Lu
A new strategy based on the ferroelectric external screening effect was used to enhance dye adsorption and degradation activity.
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Oxidation of lignocellulosic platform molecules to value-added chemicals using heterogeneous catalytic technologies

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00240B, Minireview
Pedro L. Arias, Juan A. Cecilia, Iñaki Gandarias, José Iglesias, Manuel López Granados, Rafael Mariscal, Gabriel Morales, Ramón Moreno-Tost, Pedro Maireles-Torres
This minireview gives an overview about heterogeneous catalytic technologies for the oxidation of key platform molecules (glucose, 5-hydroxymethylfurfural, furfural and levulinic acid) into valuable chemicals.
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Recent advances and prospects of inkjet printing in heterogeneous catalysis

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00040J, Minireview
Open Access
Hesam Maleki, Volfango Bertola
This review provides an insight into inkjet printing technology in the context of heterogeneous catalysis.
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Enhancing the methane low-temperature conversion on the Zn/ZSM-5 in the presence of methanol by regulating methanol-to-aromatics reaction pathway

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00449A, Paper
Zhixiang Xi, Bingjie Zhou, Yue Yu, Binbo Jiang, Zhengliang Huang, Zuwei Liao, Jingdai Wang, Yao Yang, Jingyuan Sun, Yongrong Yang
Co-reaction method provides efficient strategy for methane conversion in mild condition, which is of urgent importance of direct valorization of natural gas to liquid hydrocarbons. However, vague mechanism and neglect...
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Development of an engineered thermostable amine dehydrogenase for the synthesis of structurally diverse chiral amines

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Catal. Sci. Technol., 2020, 10,2353-2358
DOI: 10.1039/D0CY00071J, Paper
Lei Liu, Dong-Hao Wang, Fei-Fei Chen, Zhi-Jun Zhang, Qi Chen, Jian-He Xu, Zhi-Long Wang, Gao-Wei Zheng
Structurally diverse chiral amines and amino alcohols were synthesized using an engineered thermostable amine dehydrogenase, demonstrating its extensive synthesis potential.
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Fine-tuning of the substrate binding mode to enhance the catalytic efficiency of an ortho-haloacetophenone-specific carbonyl reductase

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Catal. Sci. Technol., 2020, 10,2462-2472
DOI: 10.1039/C9CY02335F, Paper
Aipeng Li, Xue Li, Wei Pang, Qing Tian, Ting Wang, Lianbing Zhang
Fine-tuning of the substrate binding mode was successfully applied for enhancing the catalytic efficiency of an ortho-haloacetophenone-specific carbonyl reductase.
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Microemulsion solventing-out co-precipitation strategy for fabricating highly active Cu–ZnO/Al2O3 dual site catalysts for reverse water gas shift

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Catal. Sci. Technol., 2020, 10,2343-2352
DOI: 10.1039/C9CY02608H, Paper
Ziheng Zhen, Wenxiang Tang, Wei (Willy) Chu, Tao Zhang, Li Lv, Shengwei Tang
A new strategy for the preparation of dual site catalysts is introduced, which combines microemulsion technology and anti-solvent extraction technology.
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Path of electron transfer created in S-doped NH2-UiO-66 bridged ZnIn2S4/MoS2 nanosheet heterostructure for boosting photocatalytic hydrogen evolution

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Catal. Sci. Technol., 2020, 10,2531-2539
DOI: 10.1039/D0CY00127A, Paper
Qi Ran, Zebin Yu, Ronghua Jiang, Lun Qian, Yanping Hou, Fei Yang, Fengyuan Li, Mingjie Li, Qianqian Sun, Heqing Zhang
This work introduces the synthesis of ZnIn2S4/NH2-UiO-66/MoS2 sheet heterostructure photocatalysts and their application to photocatalytic hydrogen evolution.
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Hourglass-type polyoxometalate-based crystalline materials as efficient cooperating photocatalysts for the reduction of Cr(VI) and oxidation of dyes

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Catal. Sci. Technol., 2020, 10,2593-2601
DOI: 10.1039/D0CY00208A, Paper
Xuerui Tian, Yaqi Zhang, Yuanyuan Ma, Qing Zhao, Zhangang Han
Hourglass-type polyoxometalate-based crystalline materials exhibit efficient photocatalytic activities towards simultaneous photocatalytic Cr(VI) reduction and organic MB oxidation.
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Hydroxyl groups attached to Co2+ on the surface of Co3O4: a promising structure for propane catalytic oxidation

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Catal. Sci. Technol., 2020, 10,2573-2582
DOI: 10.1039/D0CY00265H, Paper
Kun Chen, Wenzhi Li, Zean Zhou, Qifu Huang, Yang Liu, Qiuyan Duan
Co3O4 catalysts with three specific morphologies (nanocubes, nanosheets, and nanooctahedra) were prepared using simple preparation methods and tested for catalytic combustion of propane under the same reaction conditions.
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Mechanism of selective and complete oxidation in La2O3-catalyzed oxidative coupling of methane

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Catal. Sci. Technol., 2020, 10,2602-2614
DOI: 10.1039/D0CY00141D, Paper
Shibin Wang, Shenggang Li, David A. Dixon
The catalytic mechanism and reaction network of oxidative coupling of methane over La2O3 are thoroughly investigated by density functional theory calculations.
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980 nm NIR light driven overall water splitting over a combined CdS–RGO–NaYF4–Yb3+/Er3+ photocatalyst

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Catal. Sci. Technol., 2020, 10,2389-2397
DOI: 10.1039/D0CY00256A, Paper
Wei Gao, Yuqi Wu, Gongxuan Lu
Infrared light (NIR) accounts for more than 50% of the energy donated by the Sun to the Earth, but most of this type of energy is not utilized in photocatalytic reactions.
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Single-step benzene hydroxylation by cobalt(II) catalysts via a cobalt(III)-hydroperoxo intermediate

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Catal. Sci. Technol., 2020, 10,2540-2548
DOI: 10.1039/C9CY02601K, Paper
Karunanithi Anandababu, Sethuraman Muthuramalingam, Marappan Velusamy, Ramasamy Mayilmurugan
Cobalt(II) complexes reported as efficient and selective catalysts for single-step phenol formation from benzene using H2O2. The catalysis proceeds likely via cobalt(III)-hydroperoxo species.
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New findings and current controversies in the reaction of ruthenium red and ammonium cerium(IV) nitrate: focus on the precipitated compound

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Catal. Sci. Technol., 2020, 10,2491-2502
DOI: 10.1039/C9CY02499A, Paper
Bahram Sarvi, Seyedeh Maedeh Hosseini, Bahareh Deljoo, Abdelhamid El-Sawy, Alireza Shirazi Amin, Mark Aindow, Steven L. Suib, Mohammad Mahdi Najafpour
During water-oxidation reaction in the presence of RuR and CAN, a heterogeneous nano-sized Ru-Ce compound is detected, which is formed by the interaction of [(NH3)5RuORu(NH3)4ORu(NH3)5],6+/7+ nitrate ions, and the products of the reduction of CAN.
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Effects of Ni loading on the physicochemical properties of NiOx/CeO2 catalysts and catalytic activity for NO reduction by CO

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Catal. Sci. Technol., 2020, 10,2359-2368
DOI: 10.1039/C9CY02619C, Paper
Shuhao Zhang, Jaeha Lee, Do Heui Kim, Taejin Kim
The NO reduction by CO reaction was investigated using NiOx/CeO2 catalysts with different Ni loadings. Surface NiOx controls the catalytic activity which was related to the molecular structure and reducibility of the catalysts.
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Alumina grafted SBA-15 sustainable bifunctional catalysts for direct cross-coupling of benzylic alcohols to diarylmethanes

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Catal. Sci. Technol., 2020, 10,2583-2592
DOI: 10.1039/D0CY00471E, Paper
Chandran Rajendran, Govindaswamy Satishkumar, Charlotte Lang, Eric M. Gaigneaux
AlSBA-15 catalysts possessing Brønsted acid and Lewis acid–base bifunctionalities catalyze the direct arylation of benzyl alcohols to diarylmethanes with an 85% product yield through C–O bond activation.
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Kinetic study of the methane dry (CO2) reforming reaction over the Ce0.70La0.20Ni0.10O2−δ catalyst

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Catal. Sci. Technol., 2020, 10,2652-2662
DOI: 10.1039/C9CY02192B, Paper
Lidia Pino, Cristina Italiano, Massimo Laganà, Antonio Vita, Vincenzo Recupero
The kinetic behaviour of the Ce0.70La0.20Ni0.10O2−δ catalyst during the methane dry reforming reaction was investigated in a fixed bed reactor in the temperature range of 923–1023 K with the partial pressure of CH4 and CO2 ranging between 5 and 50 kPa.
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Construction of heterostructure based on hierarchical Bi2MoO6 and g-C3N4 with ease for impressive performance in photoelectrocatalytic water splitting and supercapacitor

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Catal. Sci. Technol., 2020, 10,2427-2442
DOI: 10.1039/D0CY00211A, Paper
C. Murugan, M. Karnan, M. Sathish, A. Pandikumar
This work demonstrates the formation of g-C3N4/Bi2MoO6 heterostructure for water splitting and supercapacitor; which shows highest PEC efficiency and symmetric device delivered a energy density and power density of 47 W h kg−1 and 4.5 kW kg−1.
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Highly-efficient Ru/Al–SBA-15 catalysts with strong Lewis acid sites for the water-assisted hydrogenation of p-phthalic acid

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Catal. Sci. Technol., 2020, 10,2443-2451
DOI: 10.1039/D0CY00047G, Paper
Cong Mao, Jingwei Zheng, Babasaheb M. Matsagar, Ranjith Kumar Kankala, Tansir Ahamad, Yucheng Yang, Kevin C.-W. Wu, Xueqin Zhang
A Ru/Al–SBA-15 catalyst with excess Lewis acid sites displayed excellent efficiency (100%), high cis-isomer selectivity (84%), and exceptional stability towards hydrogenation of p-phthalic acid in water.
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Carbon deposits during catalytic combustion of toluene on Pd–Pt-based catalysts

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Catal. Sci. Technol., 2020, 10,2452-2461
DOI: 10.1039/D0CY00101E, Paper
Yu Yang, Gang Wang, Peng Zheng, Falu Dang, Jiannian Han
Carbon is easily deposited on a catalyst during the catalytic combustion of toluene, resulting in catalyst deactivation.
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Gold-catalyzed domino cyclization enabling construction of diverse fused azaspiro tetracyclic scaffolds: a cascade catalysis mechanism due to a substrate and counterion

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Catal. Sci. Technol., 2020, 10,2415-2426
DOI: 10.1039/D0CY00120A, Paper
Yunhe Li, Xiang Zhao
The detailed mechanism and origins of gold-catalyzed domino cyclization to diverse fused azaspiro tetracyclic scaffolds by cooperative dual catalysis and cascade catalysis are systematically studied.
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Integrated adsorption and photocatalytic degradation of VOCs using a TiO2/diatomite composite: effects of relative humidity and reaction atmosphere

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Catal. Sci. Technol., 2020, 10,2378-2388
DOI: 10.1039/D0CY00168F, Paper
Guangxin Zhang, Arman Peyravi, Zaher Hashisho, Zhiming Sun, Yangyu Liu, Shuilin Zheng, Lexuan Zhong
The optimal relative humidity condition for VOC degradation is related to the length of the carbon chain of VOCs.
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Loop engineering of aryl sulfotransferase B for improving catalytic performance in regioselective sulfation

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Catal. Sci. Technol., 2020, 10,2369-2377
DOI: 10.1039/D0CY00063A, Paper
Yu Ji, Shohana Islam, Haiyang Cui, Gaurao V. Dhoke, Mehdi D. Davari, Alan M. Mertens, Ulrich Schwaneberg
Loop engineering of aryl sulfotransferase B improves catalytic performance in regioselective sulfation.
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Adjustable anchoring of Ni/Co cations by oxygen-containing functional groups on functionalized graphite paper and accelerated mass/electron transfer for overall water splitting

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Catal. Sci. Technol., 2020, 10,2627-2643
DOI: 10.1039/D0CY00181C, Paper
Yiyi Huang, Lei Sun, Zebin Yu, Ronghua Jiang, Jun Huang, Yanping Hou, Fei Yang, Boge Zhang, Runzhi Zhang, Yalan Zhang
NCS–NCO/FGP0.44 with a cellular network of porous nanosheets and close-contact heterointerface reveals accelerated interfacial mass/electron transportation for overall water splitting.
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Synthesis and molecular structure of model silica-supported tungsten oxide catalysts for oxidative coupling of methane (OCM)

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00289E, Paper
Daniyal Kiani, Sagar Sourav, Israel E. Wachs, Jonas Baltrusaitis
Catalysts with only dispersed phase Na–WO4 sites where Na/W < 2 are slightly less active but significantly more C2 selective than the traditional Na2WO4/SiO2 catalysts that contain a crystalline phase where Na/W = 2.
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Enhancing hydrogen evolution reaction through modulating electronic structure of self-supported NiFe LDH

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00315H, Paper
Xiao-Peng Li, Wen-Kai Han, Kang Xiao, Ting Ouyang, Nan Li, Feng Peng, Zhao-Qing Liu
NiFe-layered double hydroxide (NiFe LDH), as an efficient oxygen evolution reaction (OER) electrocatalyst, has emerged as a promising electrocatalyst for catalyzing overall water splitting in alkaline electrolyte.
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Outstanding Reviewers for Catalysis Science & Technology in 2019

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Catal. Sci. Technol., 2020, 10,2328-2328
DOI: 10.1039/D0CY90032J, Editorial

We would like to take this opportunity to highlight the Outstanding Reviewers for Catalysis Science & Technology in 2019, as selected by the editorial team for their significant contribution to the journal.
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Mechanistic insights into the oxidation of copper(I) species during NH3–SCR over Cu-CHA zeolites: A DFT study

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00379D, Paper
Chong Liu, Hiroe Kubota, Takashi Toyao, Zen Maeno, Ken-ichi Shimizu
Selective catalytic reduction of nitrogen oxides using ammonia (NH3–SCR) over Cu-exchanged zeolites proceeds via reduction of Cu(II) to Cu(I) and subsequent reoxidation of Cu(I) to Cu(II). Although the mechanism of...
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Selenium-catalyzed oxidation of alkenes: insight into the mechanisms and developing trend

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00400F, Perspective
Hongen Cao, Rongrong Qian, Lei Yu
Recent progresses of the selenium-catalyzed oxidation of alkenes are summarized at the mechanism level. It may be beneficial for designing novel selenium-containing catalysts and alkene oxidation protocols for the next phase of studies.
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Carbon nanotube/PTFE as a hybrid platform for lipase B from Candida antarctica in transformation of α-angelica lactone into alkyl levulinates

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00545B, Paper
Anna Szelwicka, Anna Kolanowska, Piotr Latos, Sebastian Jurczyk, Slawomir Boncel, Anna Chrobok
A highly active biocatalyst based on a hybrid platform was designed for the conversion of α-angelica lactone to alkyl levulinates.
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Origin of CO2 as the main carbon source in syngas-to-methanol process over Cu: theoretical evidence from a combined DFT and microkinetic modeling study

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00602E, Paper
Dongyang Xu, Panpan Wu, Bo Yang
A theoretical study combining DFT and microkinetic modeling provides evidence that CO2 is the main carbon source in methanol synthesis from syngas (CO, CO2 and H2) over Cu.
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Heterogeneous iron-containing nanocatalysts – promising systems for selective hydrogenation and hydrogenolysis

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00086H, Minireview
Anastasiya A. Shesterkina, Leonid M. Kustov, Anna A. Strekalova, Vladimir B. Kazansky
Bimetallic catalytic systems Fe–Me (Pt, Pd, Cu) demonstrate synergy in the activity/selectivity pattern in reactions involving hydrogen: selective hydrogenation of CC bonds, NO2 and carbonyl groups and hydrogenolysis of C–O bonds.
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