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A sensitive HPLC-FL method to simultaneously determine febuxostat and diclofenac in rat plasma: assessment of metabolic drug interactions in vitro and in vivo

Anal. Methods, 2020, 12,2166-2175
DOI: 10.1039/D0AY00471E, Paper
Dong-Gyun Han, Kyu-Sang Kim, Seong-Wook Seo, Young Mee Baek, Yunjin Jung, Dae-Duk Kim, In-Soo Yoon
We developed a sensitive, simple and validated HPLC-FL method for simultaneous determination of FEB and DIC in rat plasma. The method requires a relatively small volume of sample, has simple sample preparation and excellent sensitivity.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
The content of this RSS Feed (c) The Royal Society of Chemistry




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The influence of lateral flake size in graphene/graphite paste electrodes: an electroanalytical investigation

Anal. Methods, 2020, 12,2133-2142
DOI: 10.1039/D0AY00169D, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Alejandro García-Miranda Ferrari, Hadil M. Elbardisy, Valentine Silva, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks, Dale A. C. Brownson
We report the electroanalytical properties of graphene and graphite paste electrodes comprising varying lateral flake sizes when applied for sensing relevant biomolecules and prominent drugs of abuse.
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The characterization of self-assembled nanostructures in whole blood

Anal. Methods, 2020, 12,2068-2081
DOI: 10.1039/D0AY00170H, Tutorial Review
Mark Pitman, Jessica Larsen
This tutorial describes methods of characterizing nanomaterials in whole blood, and the associated benefits and shortcomings of each technique.
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In situ imaging of intracellular human telomerase RNA with molecular beacon-functionalized gold nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00461H, Paper
Tao Xie, Ziyan Fan, Ruilong Zhang, Xiaohe Tian, Guangmei Han, Zhengjie Liu, Zhongping Zhang
We develop molecular beacon-functionalized gold nanoparticles for in situ human telomerase RNA imaging in live cells.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Rh(III) hydroxocomplexes speciation using HPLC-ESI-MS

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00363H, Paper
Victoria V Volchek, Semen Nikolaevich Berdyugin, Olga Vasil`evna Shuvaeva, Dmitriy Sheven, Danila Vasilchenko, Sergey Korenev
A mixture of rhodium(III) hydroxocomplexes formed during the polycondensation process in alkaline media has been fully characterized by the hyphenated high performance liquid chromatography with electrospray ionization mass spectrometry (HPLC-ESI-MS)....
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Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00334D, Paper
Hong-Lin Ding, Yan-Qing Pu, Da-Ying Ye, Zi-Yue Dong, Man Yang, Cheng-Wei Lü, Yue An
The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications are shown.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Solid-phase microextraction using a β-ketoenamine-linked covalent organic framework coating for efficient enrichment of synthetic musks in water samples

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02755F, Paper
Lian Wen, Peng Wu, Lei-Lei Wang, Li-Zong Chen, Ming-Lin Wang, Xia Wang, Jin-Ming Lin, Ru-Song Zhao
This study indicated the promising applicability of the TpPa-1 as a solid-phase microextraction fiber coating for reliably detecting synthetic musks at trace levels from environmental samples.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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One-step synthesis of mitochondrion-targeted fluorescence carbon dots and fluorescent detection of silver ions

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00622J, Paper
Yue Hou, Hanxiao Liu, Zhanxian Li, Hongyan Zhang, Liuhe Wei, Mingming Yu
Silver ions (Ag+) are the most representative harmful ions found in water pollution and widely used in many industries, excessive ingestion of Ag+ in the human body may interact with...
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Quantification of Anthracene after dermal absorption test via APCI-Tandem Mass Spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00486C, Paper
Xinyi Sui, Julio E Teran, Chengcheng Feng, Killian Wustrow, Caroline J. Smith , Nelson R Vinueza
An analytical method for the detection and quantification of anthracene from dermal samples was developed by using Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry (APCI-MS/MS). The anthracene samples were obtained from...
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A high-throughput plasmonic tongue using an aggregation assay and nonspecific interactions: classification of taste profiles in maple syrup

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY01942A, Paper
Simon Forest, Trevor Théorêt, Julien Coutu, Jean-Francois Masson
A simple colorimetric test detects off-flavour profiles of maple syrups in minutes, which are detectable by the naked eye.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Sample treatment based on molecularly imprinted polymers for the analysis of veterinary drugs in food samples: a review

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00533A, Critical Review
Israel Samuel Ibarra, J. M. Miranda, Irma Perez, Aldo C Jardinez, Gabriela Islas
The use of veterinary drugs in medical treatments and in the livestock industry is a recurrent practice. In subtherapeutic doses during prolonged times act to growth promoters. Residues of these...
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Effects of harvesting and extraction methods on metabolite recovery from adherently growing mammalian cells

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02753J, Paper
Yun Luo, Ningbo Geng, Baoqin Zhang, Jiping Chen, Haijun Zhang
We compare the efficiencies of different cell harvesting methods and metabolite extraction methods in sample preparation procedures and provide a cell sample processing protocol which focuses on maximizing metabolite recovery ranging from polar to lipidic ones.
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Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
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Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
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Adsorptive removal of Hg2+ from environmental water samples using thioglycerol-intercalated magnetic layered double hydroxides

Anal. Methods, 2020, 12,2279-2286
DOI: 10.1039/D0AY00448K, Paper
Ali Esrafili, Mahnaz Ghambarian, Mohammad Tajik, Mahroo Baharfar
Herein, the removal of Hg2+ from environmental water samples was carried out using a novel nanoadsorbent based on magnetite nanoparticles coated by a thioglycerol-intercalated layered double hydroxide.
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LC-MS in combination with DMBA derivatization for sialic acid speciation and distribution analysis in fish tissues

Anal. Methods, 2020, 12,2221-2227
DOI: 10.1039/D0AY00100G, Paper
Junjie Du, Qiwei Zhang, Jianjun Li, Qi Zheng
For sialic acid speciation analysis, DMBA provides superior chromatographic separation efficiency and comparable MS/MS spectra with DMB.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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A sensitive and selective fluorescent probe for the detection of endogenous peroxynitrite (ONOO-) in live cells

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00012D, Paper
Yaru Sun, Baoli Dong, Yaru Lu, Wenhui Song, Abdul Hadi Mehmood, Weiying Lin
Peroxynitrite (ONOO−) is one of reactive oxygen species, and plays a vital role in many physiological and pathological processes. Given that the ONOO− level is closely related with many serious...
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Dispersive micro-solid phase extraction based on graphene/polydopamine composite for the extraction of pyrethroids in water samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00562B, Paper
Qinqin Xu, Kexin Qiao, Chen Yan, Zikai Liu, Runhua Lu, Wenfeng Zhou
In this study, a simple, rapid, precise, and environmentally friendly microextraction named dispersive micro-solid phase extraction based on graphene/polydopamine composite as sorbent was investigated for the analysis of four pyrethroids...
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Fabrication of an electrochemical sensor based on metal-organic framework ZIF-8 for quantitation of silver ion: optimizing experimental conditions by central composite design (CCD)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00843E, Paper
Farzaneh Hashemi , Ali Reza Zanganeh, Farid Naeimi , Maryam Tayebani
The ZIF-8 was synthesized and carbon paste electrode (CPE) modified with this metal-organic framework utilized for quantitation of silver(Ι) by differential pulse anodic stripping voltammetry (DPASV) technique. The prepared ZIF-8...
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Digital Reference Section (DRS) Virtual Programs: New blog post invites readers to "Sample a Taste of History This Thanksgiving"

Find a new and historic recipe for a dish to put on your Thanksgiving table in What Mrs. Fisher Knows About Old Southern Cooking. This cookbook, published in 1881, is highlighted in a recent post on the Library of Congress Blog. Abby Fisher perfected her culinary skills as an enslaved cook on a South Carolina plantation but went on to establish a successful catering business in San Francisco and publish a compilation of her recipes—one of the first by an African-American. Learn more about this remarkable woman and, this Thanksgiving, sample a taste of history!

Click here to go to the Library of Congress Blog post, "Sample a Taste of History This Thanksgiving!"




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April 3 Webinar: Caught in the Web? Online Tools for Business Research

Please join us for our April topical webinar:

Caught in the Web? Online Tools for Business Research

With so many options available, identifying the best ways to meet your research needs online can be a challenge. Please join our business librarians for an overview of freely available tools for business research, for beginning and intermediate-level users. Topics discussed will include: types of business information, effective use of online search engines, the importance of the deep web, identifying reliable sources of business information, and more. By the end of this program participants will be able to successfully search a research topic online, navigate selected Internet sources, and discover resources and services offered through the Library of Congress Business Reference Section.

Date: Wednesday, April 3
Time: 12:00 noon – 1:00 pm EDT
Registration: Please register via Eventbrite

How to Attend:

Web discussions are held in real time via webinar software, which allows participants from around the country and the world to join us. Registration is required. Confirmation and log on instructions will be sent via email. Please read the Library of Congress Comment and Posting Policy.

Technical requirements: Participants must have access to an Internet-connected computer or device with speakers or headphones. There is also a telephone option for listening to audio.

ADA: Request ADA accommodations five days in advance at (202) 707-6362 or ada@loc.gov. Registration for the program is also required.

Questions? Ask A Librarian.




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Perils of Perestroika : viewpoints from the Soviet press, 1989-1991 / edited by Isaac J. Tarasulo.

Wilmington, Del. : SR Books, 1992




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The Canada-US border in the 21st century [electronic resource] : trade, immigration and security in the age of Trump / John B. Sutcliffe and William P. Anderson.

Abingdon, Oxon : Routledge, 2019.




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North American borders in comparative perspective [electronic resource] / edited by Guadalupe Correa-Cabrera and Victor Konrad.

Tucson : University of Arizona Press, 2020.




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A history of ancient Moab from the Ninth to First centuries BCE [electronic resource] / by Burton MacDonald.

Atlanta : SBL Press, [2020]




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Between Rome and Persia [electronic resource] : the middle Euphrates, Mesopotamia, and Palmyra under Roman control / Peter M. Edwell

London ; New York : Routledge, 2008




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The Oxford handbook of ancient Anatolia, 10,000-323 B.C.E. [electronic resource] / edited by Sharon R. Steadman and Gregory McMahon.

New York ; Oxford : Oxford University Press, 2011.




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The Oxford handbook of Anglo-Saxon archaeology [electronic resource] / edited by Helena Hamerow, David A. Hinton and Sally Crawford.

Oxford : Oxford University Press, 2011.




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The Oxford handbook of Roman Egypt [electronic resource] / edited by Christina Riggs.

Oxford : Oxford University Press, 2012.




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A Faustian foreign policy from Woodrow Wilson to George W. Bush [electronic resource]: dreams of perfectibility / Joan Hoff

Cambridge ; New York : Cambridge University Press, 2008




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Egyptian mummies and modern science [electronic resource] / edited by Rosalie David

Cambridge ; New York : Cambridge University Press, 2008




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Recharting the Black Atlantic [electronic resource] : modern cultures, local communities, global connections / edited by Annalisa Oboe and Anna Scacchi

New York : Routledge, 2008




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Asian-European relations [electronic resource] : building blocks for global governance? / edited by Jürgen Rüland [and others]

London ; New York : Routledge, 2008




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The United States and Iran [electronic resource] : sanctions, wars and the policy of dual containment / Sasan Fayazmanesh

London ; New York : Routledge, 2008




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Covid-19 Factoid: Gap between daily new cases and recoveries widening

The world is adding over 70,000 cases everyday while the daily recoveries are still sub-15,000 on an average in the last three days.




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Covid-19 Factoid: Pain and recovery as cases set to cross 1.5 mn mark

Germany, where 40 per cent of all infected persons are recovering, is doing the best by that metric among the five worst-affected nations




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Covid-19 Factoid: Just 3 states account for half of new India cases in Apr

While North America and Europe account for the bulk of all coronavirus cases globally, half of new cases reported in India have come from Delhi, Maharashtra and Tamil Nadu alone




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Covid-19 factoid: Alarm bells ring as India adds 1,500 cases in a day

Country's death toll consistently rising too, taking just two days to add the last 50 fatalities to the total.




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Business activities significantly hit; recovery may take over a year: Survey

A CII survey indicates that the country may experience a protracted slowdown in economic activity.




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GSTN Helpdesk handles over 56,000 taxpayer issues in one month of lockdown

GST Network Helpdesk on Sunday said it has handled over 56,000 taxpayer issues in one month since the nationwide lockdown was imposed on March 25.




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Nabard refinances close to Rs 13,000 crore to state co-op banks and RRBs to assit farmers deal on-going lockdown

The loan has been disbursed under a refinance scheme by Nabard from its own resources and was given this week. "An amount of Rs 12,767 crore has been disbursed this week to StCBs and RRBs across the country in a bid to augment their resources during the ongoing lockdown conditions for extending credit to farmers," Nabard said.




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Govt to gain Rs 1.6 lakh cr this fiscal from record excise duty hike on petrol, diesel

The cash-strapped government will gain close to Rs 1.6 lakh crore in additional revenues this fiscal from a record increase in excise duty on petrol and diesel, that will help make up for revenue it lost in a slowing economy and shutting down of businesses due to coronavirus lockdown.