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The influence of lateral flake size in graphene/graphite paste electrodes: an electroanalytical investigation

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Anal. Methods, 2020, 12,2133-2142
DOI: 10.1039/D0AY00169D, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Alejandro García-Miranda Ferrari, Hadil M. Elbardisy, Valentine Silva, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks, Dale A. C. Brownson
We report the electroanalytical properties of graphene and graphite paste electrodes comprising varying lateral flake sizes when applied for sensing relevant biomolecules and prominent drugs of abuse.
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The characterization of self-assembled nanostructures in whole blood

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Anal. Methods, 2020, 12,2068-2081
DOI: 10.1039/D0AY00170H, Tutorial Review
Mark Pitman, Jessica Larsen
This tutorial describes methods of characterizing nanomaterials in whole blood, and the associated benefits and shortcomings of each technique.
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In situ imaging of intracellular human telomerase RNA with molecular beacon-functionalized gold nanoparticles

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00461H, Paper
Tao Xie, Ziyan Fan, Ruilong Zhang, Xiaohe Tian, Guangmei Han, Zhengjie Liu, Zhongping Zhang
We develop molecular beacon-functionalized gold nanoparticles for in situ human telomerase RNA imaging in live cells.
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Correction: Towards simultaneous quantification of protease inhibitors and inflammatory biomarkers in serum for people living with HIV

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Anal. Methods, 2020, 12,2196-2196
DOI: 10.1039/D0AY90050H, Correction
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Pengyi Wang, Charles S. Venuto, Raymond Cha, Benjamin L. Miller
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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
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Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
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Plasticizer-free and pH-independent ion-selective optode films based on a solvatochromic dye

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00439A, Communication
Xuewei Wang, Yang Zhou, Vanessa Decker, Mark E. Meyerhoff, Meng Sun, Yu Cui
A layer of a solvatochromic dye, an ionophore, and an ion-exchanger deposited on a Nylon membrane enables highly selective colorimetric and fluorometric ion sensing. This new platform does not suffer...
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
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Confirmation of brand identification in infant formulas by using near-infrared spectroscopy fingerprints

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00375A, Paper
Shuyi Chang, Chengcheng Yin, Sha Liang, Mei Lu, Ping Wang, Zhicheng Li
The NIR spectra of 12 batches of each stage of Brand A infant formulas.
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Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
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The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00334D, Paper
Hong-Lin Ding, Yan-Qing Pu, Da-Ying Ye, Zi-Yue Dong, Man Yang, Cheng-Wei Lü, Yue An
The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications are shown.
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Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
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Solid-phase microextraction using a β-ketoenamine-linked covalent organic framework coating for efficient enrichment of synthetic musks in water samples

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02755F, Paper
Lian Wen, Peng Wu, Lei-Lei Wang, Li-Zong Chen, Ming-Lin Wang, Xia Wang, Jin-Ming Lin, Ru-Song Zhao
This study indicated the promising applicability of the TpPa-1 as a solid-phase microextraction fiber coating for reliably detecting synthetic musks at trace levels from environmental samples.
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One-step synthesis of mitochondrion-targeted fluorescence carbon dots and fluorescent detection of silver ions

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00622J, Paper
Yue Hou, Hanxiao Liu, Zhanxian Li, Hongyan Zhang, Liuhe Wei, Mingming Yu
Silver ions (Ag+) are the most representative harmful ions found in water pollution and widely used in many industries, excessive ingestion of Ag+ in the human body may interact with...
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Quantification of Anthracene after dermal absorption test via APCI-Tandem Mass Spectrometry

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00486C, Paper
Xinyi Sui, Julio E Teran, Chengcheng Feng, Killian Wustrow, Caroline J. Smith , Nelson R Vinueza
An analytical method for the detection and quantification of anthracene from dermal samples was developed by using Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry (APCI-MS/MS). The anthracene samples were obtained from...
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A high-throughput plasmonic tongue using an aggregation assay and nonspecific interactions: classification of taste profiles in maple syrup

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY01942A, Paper
Simon Forest, Trevor Théorêt, Julien Coutu, Jean-Francois Masson
A simple colorimetric test detects off-flavour profiles of maple syrups in minutes, which are detectable by the naked eye.
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Sample treatment based on molecularly imprinted polymers for the analysis of veterinary drugs in food samples: a review

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00533A, Critical Review
Israel Samuel Ibarra, J. M. Miranda, Irma Perez, Aldo C Jardinez, Gabriela Islas
The use of veterinary drugs in medical treatments and in the livestock industry is a recurrent practice. In subtherapeutic doses during prolonged times act to growth promoters. Residues of these...
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Effects of harvesting and extraction methods on metabolite recovery from adherently growing mammalian cells

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02753J, Paper
Yun Luo, Ningbo Geng, Baoqin Zhang, Jiping Chen, Haijun Zhang
We compare the efficiencies of different cell harvesting methods and metabolite extraction methods in sample preparation procedures and provide a cell sample processing protocol which focuses on maximizing metabolite recovery ranging from polar to lipidic ones.
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Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
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Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
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Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
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A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

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Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
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Droplet image analysis with user-friendly freeware CellProfiler

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Anal. Methods, 2020, 12,2287-2294
DOI: 10.1039/D0AY00031K, Technical Note
Simona Bartkova, Marko Vendelin, Immanuel Sanka, Pille Pata, Ott Scheler
We show how to use free open-source CellProfiler for droplet microfluidic image analysis.
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Detection of organophosphorus compounds using a surface acoustic wave array sensor based on supramolecular self-assembling imprinted films

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Anal. Methods, 2020, 12,2206-2214
DOI: 10.1039/D0AY00211A, Paper
Yong Pan, Tengxiao Guo, Genwei Zhang, Junchao Yang, Liu Yang, Bingqing Cao
In this study, diisopropyl methylphosphonate (DIMP), tributyl phosphate (TBP), and dimethyl methylphosphonate (DMMP) were selected as organophosphorus chemical warfare agent (CWA) simulants.
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Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

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Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
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LC-MS in combination with DMBA derivatization for sialic acid speciation and distribution analysis in fish tissues

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Anal. Methods, 2020, 12,2221-2227
DOI: 10.1039/D0AY00100G, Paper
Junjie Du, Qiwei Zhang, Jianjun Li, Qi Zheng
For sialic acid speciation analysis, DMBA provides superior chromatographic separation efficiency and comparable MS/MS spectra with DMB.
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Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

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Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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Selection and optimization of protein and carbohydrate assays for the characterization of marine biofouling

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Anal. Methods, 2020, 12,2228-2236
DOI: 10.1039/D0AY00272K, Paper
Chloe Richards, Nicole O'Connor, Diveena Jose, Alan Barrett, Fiona Regan
Biofilms comprise a set of microorganisms attached to a surface through extracellular polymeric substances (EPS). Development of reliable analytical assays are valuable in determining the rate of biofilm attachment on surfaces.
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Simultaneous aptasensor assay of ochratoxin A and adenosine triphosphate in beer based on Fe3O4 and SiO2 nanoparticle as carriers

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Anal. Methods, 2020, 12,2253-2259
DOI: 10.1039/D0AY00311E, Paper
Xiluan Yan, Mengmeng Jiang, Yuting Jian, Jing Luo, Xinxin Xue, Xin Chen, Xiangjuan Zheng, Fanrong Ai
In this work, a chemiluminescence (CL) method based on dual aptasensors using Fe3O4 and SiO2 nanoparticles (NPs) as carriers is developed for the simultaneous detection of ochratoxin A (OTA) and adenosine triphosphate (ATP) in beer.
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Ion chromatography for monitoring [NTf2]− anion contaminants in pure and saline water

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Anal. Methods, 2020, 12,2244-2252
DOI: 10.1039/D0AY00337A, Paper
Coby J. Clarke, Liem Bui-Le, Jason Hallett
An optimized ion chromatography method for quantifying highly polarizable [NTf2]− anions in high salinity wastewater is presented.
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Detection of radium at the attogram per gram level in copper by inductively coupled plasma mass spectrometry after cation-exchange chromatography

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Anal. Methods, 2020, 12,2272-2278
DOI: 10.1039/D0AY00512F, Paper
Mélodie Bonin, Dominic Larivière, Pavel P. Povinec
In this study, a new method was developed for the separation and isolation of radium from metallic copper.
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Development and validation of a real-time microelectrochemical sensor for clinical monitoring of tissue oxygenation/perfusion

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00206B, Paper
Gama Theophile Gnahoré, Jack L. Kelly, Saidhbhe L. O'Riordan, Fiachra B. Bolger, Michelle M. Doran, Michelle Sands, John P. Lowry
Oxygen is critically important to tissue viability and there is increasing demand for its reliable real-time clinical monitoring in order to prevent, diagnose and treat several pathological disorders, including hypoxia, stroke and reperfusion injury.
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A sensitive and selective fluorescent probe for the detection of endogenous peroxynitrite (ONOO-) in live cells

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00012D, Paper
Yaru Sun, Baoli Dong, Yaru Lu, Wenhui Song, Abdul Hadi Mehmood, Weiying Lin
Peroxynitrite (ONOO−) is one of reactive oxygen species, and plays a vital role in many physiological and pathological processes. Given that the ONOO− level is closely related with many serious...
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A simple paper-based approach for arsenic determination in water using hydride generation coupled with mercaptosuccinic-acid capped CdTe quantum dots

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00273A, Paper
Oraphan Thepmanee, Kanlaya Prapainop Katewongsa, Obnithi Nooppha, Nuanlaor Ratanawimarnwong, Weena Siangproh, Orawon Chailapakul, Kriangsak Songsrirote
This research aims to develop a simple paper-based device for arsenic detection in water samples where a hydride generation technique coupled with mercaptosuccinic acid-capped CdTe quantum dots (MSA-CdTe QDs) as...
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ELISA as an effective tool to determine spatial and seasonal occurrence of emerging contaminants in the aquatic environment

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Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00426J, Paper
Carla Patrícia Silva, Tânia Carvalho, Rudolf J. Schneider, Valdemar I. Esteves, Diana L. D. Lima
Monitoring emerging contaminants is essential as they represent a risk to the aquatic environment. ELISA is a promising method for their quantification mostly because it allows controlling their concentration levels through large screening campaigns.
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The application of antibody – aptamer hybrid biosensors in the clinical diagnostics and environmental analysis

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00678E, Critical Review
Marta Jarczewska, Elzbieta Malinowska
The growing number of various diseases and the increase of environmental contamination are the causes for elaboration of novel methods for their detection. The possibility of application of affinity-based biosensors...
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A flower-like Ag coated with molecularly imprinted polymers as surface-enhanced Raman scattering substrate for sensitive and selective detection of glibenclamide

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00575D, Paper
Xiaohui Ren, Xin Li
The flower-like Ag, was formed by nanosheets self-assembly, as SERS active substrate was utilized for preparation of flower-like Ag@molecularly imprinted polymers (MIPs) surface-enhanced Raman scattering (SERS) sensor. Based on the...
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Rapid and colorimetric detection of nucleic acids based on entropy-driven circuit and DNAzyme mediated autocatalytic reaction

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00341G, Paper
Hongli Shi, Jianyuan Dai, fang Wang, Yushun Xia, Dan Xiao, Cuisong Zhou
In this work, a novel, rapid and enzyme-free colorimetric biosensor for nucleic acids detection has been developed based on entropy-driven circuit (EDC) and DNAzyme mediated autocatalytic reaction. Upon sensing of...
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Fabrication of an electrochemical sensor based on metal-organic framework ZIF-8 for quantitation of silver ion: optimizing experimental conditions by central composite design (CCD)

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Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00843E, Paper
Farzaneh Hashemi , Ali Reza Zanganeh, Farid Naeimi , Maryam Tayebani
The ZIF-8 was synthesized and carbon paste electrode (CPE) modified with this metal-organic framework utilized for quantitation of silver(Ι) by differential pulse anodic stripping voltammetry (DPASV) technique. The prepared ZIF-8...
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Digital Reference Section (DRS) Virtual Programs: New blog post invites readers to "Sample a Taste of History This Thanksgiving"

By blogs.loc.gov
Published On :: Wed, 21 Nov 2018 10:00:27 -0600

Find a new and historic recipe for a dish to put on your Thanksgiving table in What Mrs. Fisher Knows About Old Southern Cooking. This cookbook, published in 1881, is highlighted in a recent post on the Library of Congress Blog. Abby Fisher perfected her culinary skills as an enslaved cook on a South Carolina plantation but went on to establish a successful catering business in San Francisco and publish a compilation of her recipes—one of the first by an African-American. Learn more about this remarkable woman and, this Thanksgiving, sample a taste of history!

Click here to go to the Library of Congress Blog post, "Sample a Taste of History This Thanksgiving!"


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January 15 Intro to loc.gov

By www.loc.gov
Published On :: Wed, 02 Jan 2019 10:00:22 -0600

Make the most of the Library's online collections: photographs, maps, sound recordings, films, legal and historical documents, and more. Join the Digital Reference Section's next free one-hour webinar for an interactive orientation to loc.gov.

Title: Introducing loc.gov: Orientation and Research Strategies
Date: Tuesday, January 15
Time: 11:00 am - 12:00 noon EST

Registration (required): Please register via Eventbrite.

Orientations are held in real time via webinar software, which allows participants from around the country and the world to join us. Confirmation and log-on instructions will be sent via email. Please read the Library of Congress Comment and Posting Policy.

ADA: Request ADA accommodations five days in advance at (202) 707-6362 or ada@loc.gov. Registration for the program is also required.

Questions? Ask A Librarian!


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May 30 Webinar: Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

By www.loc.gov
Published On :: Wed, 22 May 2019 10:54:59 -0500

Reminder!!

Please join us for our May topical webinar:

Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

May 2019 marks the 200th anniversary of the birth of poet Walt Whitman, who revolutionized the style and content of American poetry with his 1855 publication of Leaves of Grass. Whitman was also a journalist, printer, publisher, orator, and prose writer.

The Library of Congress holds the largest group of Whitman-related special collection materials in the world, including printed materials, rare books, photographs, and manuscripts. In this webinar program, Manuscript Division historian Barbara Bair highlights the content and research use of three digitized Whitman manuscript collections as well as programs celebrating Whitman’s birthday at the Library of Congress.

Date: Thursday, May 30
Time: 1:00 pm – 2:00 pm EDT
Registration (required): Please register via Eventbrite.

This program will be held in real time via webinar software, which allows participants from around the country and the world to join us. Confirmation and log-on instructions will be sent via email. Please read the Library of Congress Comment and Posting Policy.

ADA: Request ADA accommodations five days in advance at (202) 707-6362 or ada@loc.gov. Registration for the program is also required.

Questions? Ask A Librarian!

 


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The Canada-US border in the 21st century [electronic resource] : trade, immigration and security in the age of Trump / John B. Sutcliffe and William P. Anderson.

By darius.uleth.ca
Published On ::

Abingdon, Oxon : Routledge, 2019.


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North American borders in comparative perspective [electronic resource] / edited by Guadalupe Correa-Cabrera and Victor Konrad.

By darius.uleth.ca
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Tucson : University of Arizona Press, 2020.


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A history of ancient Moab from the Ninth to First centuries BCE [electronic resource] / by Burton MacDonald.

By darius.uleth.ca
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Atlanta : SBL Press, [2020]


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Between Rome and Persia [electronic resource] : the middle Euphrates, Mesopotamia, and Palmyra under Roman control / Peter M. Edwell

By darius.uleth.ca
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London ; New York : Routledge, 2008


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The Oxford handbook of ancient Anatolia, 10,000-323 B.C.E. [electronic resource] / edited by Sharon R. Steadman and Gregory McMahon.

By darius.uleth.ca
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New York ; Oxford : Oxford University Press, 2011.


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The Oxford handbook of Anglo-Saxon archaeology [electronic resource] / edited by Helena Hamerow, David A. Hinton and Sally Crawford.

By darius.uleth.ca
Published On ::

Oxford : Oxford University Press, 2011.


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The Oxford handbook of Roman Egypt [electronic resource] / edited by Christina Riggs.

By darius.uleth.ca
Published On ::

Oxford : Oxford University Press, 2012.


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A Faustian foreign policy from Woodrow Wilson to George W. Bush [electronic resource]: dreams of perfectibility / Joan Hoff

By darius.uleth.ca
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Cambridge ; New York : Cambridge University Press, 2008


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