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Measurement of uranium in a glass matrix based on spatial confinement using fiber-optic laser-induced breakdown spectroscopy

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J. Anal. At. Spectrom., 2024, 39,2716-2727
DOI: 10.1039/D4JA00237G, Paper
Xinyu Guo, Jian Wu, Jinghui Li, Mingxin Shi, Xinxin Zhu, Ying Zhou, Di Wu, Ziyuan Song, Sijun Huang, Xingwen Li
The storage and management of nuclear waste materials require the detection of uranium, but traditional analytical methods are unsuitable for radioactive environments.
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High-precision, mass dependent Si isotope measurements via the critical mixture double-spiking technique

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J. Anal. At. Spectrom., 2024, 39,2799-2808
DOI: 10.1039/D4JA00152D, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Xiao-Ning Liu, Martijn Klaver, Remco C. Hin, Christopher D. Coath, Hong Chin Ng, Tim Elliott
We developed critical mixture double-spiking Si isotope measurement, achieving an enhanced long-term reproducibility of ±0.03‰ (δ30Si, 2 s.d.), which is ∼4 times better than the current methods' long-term reproducibility over ±0.1‰ (δ30Si, 2 s.d.).
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Bimodal data fusion of LIBS spectroscopy and plasma acoustic emission signals: improving the accuracy of machining process identification for low roughness samples

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J. Anal. At. Spectrom., 2024, 39,2737-2747
DOI: 10.1039/D4JA00225C, Paper
Shilei Xiong, Minchao Cui, Nan Yang, Guangyuan Shi, Yuxin Pi, Yuyang Mu, Yuntao Zhang, Yue Zhao
The fusion of LIBS spectral data with PAES data improves machining process classification identification accuracy.
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Development and application of reference and routine analytical methods providing SI-traceable results for the determination of technology-critical elements in PCB from WEEE

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J. Anal. At. Spectrom., 2024, 39,2809-2823
DOI: 10.1039/D4JA00235K, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Giancarlo D'Agostino, Marcus Oelze, Jochen Vogl, Jean-Philippe Ghestem, Nicolas Lafaurie, Ole Klein, Daniel Pröfrock, Marco Di Luzio, Luigi Bergamaschi, Radojko Jaćimović, Caroline Oster, Johanna Irrgeher, Shaun T. Lancaster, Anna Walch, Anita Röthke, Lena Michaliszyn, Axel Pramann, Olaf Rienitz, Timo Sara-Aho, Oktay Cankur, Derya Kutan, Johanna Noireaux
Development and test of five reference analytical methods and six routine analytical methods providing SI-traceable results of twenty technology-critical elements in end-of-life PCB materials.
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A simplified instrumental protocol for trace Nd and Hf isotope measurements (<10 ng) using a MC-ICP-MS and an Apex Omega de-solvating system

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J. Anal. At. Spectrom., 2024, 39,2694-2702
DOI: 10.1039/D4JA00276H, Technical Note
Ting Zhou, Liang Qi, Sheng-hua Liu, Bo Zhou
Accurate and precise Nd and Hf isotope measurements of samples with low contents by simple adjustments of an Apex Omega membrane de-solvating system.
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A novel in situ methodology for U–Pb, (U–Th)/He, and fission track triple dating

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J. Anal. At. Spectrom., 2024, 39,2856-2869
DOI: 10.1039/D4JA00257A, Paper
Jie Hu, Zhiwu Li, Jinxi Li, Shugen Liu, Ganqing Xu, Chaoqun Yang, Kui Tong, Yin Li
For the first time, this paper introduces a general workflow for in situ U–Pb, (U–Th)/He, and fission track triple dating on a single grain.
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Optimization of informative variables selection for quantitative analysis of heavy metal (Cu) contaminated Tegillarca granosa using laser-induced breakdown spectroscopy

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J. Anal. At. Spectrom., 2024, 39,2824-2831
DOI: 10.1039/D4JA00084F, Paper
Xudong Huang, Xiaojing Chen, Guangzao Huang, Zhonghao Xie, Wen Shi, Shujat Ali, Leiming Yuan, Xi Chen
The KMRCD algorithm successfully selected 50 informative variables from the 1520 variables in the LIBS spectra.
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Evaluation and calibration of matrix effects during SIMS silicon isotope analysis in silicate glasses

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J. Anal. At. Spectrom., 2024, 39,2832-2840
DOI: 10.1039/D4JA00253A, Paper
Liu-Yang Chen, Yu Liu, Di Zhang, Guo-Qiang Tang, Qiu-Li Li
A matrix effect calibration model during SIMS silicon isotope analysis based on the contents of Si, Ca, Al and Mg (SCAM model) in silicate glasses.
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Sodium nanoferrite-based solid phase extraction: a green method for the simultaneous determination of cadmium, copper, and lead

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J. Anal. At. Spectrom., 2024, 39,2884-2892
DOI: 10.1039/D4JA00210E, Paper
Saima Perveen, Aysen Hol, Jameel Ahmed Baig, Syed Tufail Hussain Sherazi, Khalil Akhtar, Sajjad Hussain, Fahad Abbasi
A solid phase extraction (SPE) methodology utilizing sodium ferrite nanoparticles (Na2Fe4O7-NPs; SF-NPs) is presented for the simultaneous determination of heavy metals (HMs) via flame atomic absorption spectrometry (FAAS).
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First demonstration of in situ Lu–Hf dating using LA-ICP-MS/MS applied to monazite

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J. Anal. At. Spectrom., 2024, 39,2703-2715
DOI: 10.1039/D4JA00258J, Technical Note
Shitou Wu, Junlong Niu, Yueheng Yang, Hao Wang, Jinhui Yang, Fuyuan Wu
Monazite is a LREE-rich accessory mineral in various igneous and metamorphic rocks; therefore, monazite geochronology has the potential to answer a range of important geological questions.
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Efficient preconcentration of ultra-trace rhenium from geological materials via induced adsorption for accurate isotope analysis

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J. Anal. At. Spectrom., 2024, 39,2748-2755
DOI: 10.1039/D4JA00295D, Paper
Yumeng Liu, Tianyu Chen, Tao Li, Weiqiang Li, Qingquan Hong, Jiubin Chen
Preconcentration via induced adsorption achieves the quantitative recovery of Re and facilitates Re isotope analysis.
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Data fusion of spectral and acoustic signals in LIBS to improve the measurement accuracy of carbon emissions at varying gas temperatures

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J. Anal. At. Spectrom., 2024, 39,2756-2766
DOI: 10.1039/D4JA00287C, Paper
Shu Chai, Jie Ren, Suming Jiang, Aochen Li, Ziqing Zhao, Haimeng Peng, Qiwen Zhang, Wendong Wu
A novel mid-level data fusion method integrating spectral and acoustic signals of laser-induced plasmas was proposed to improve the measurement accuracy of carbon concentrations in flue gas at varying gas temperatures.
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Mg separation from samples with very high Ca/Mg ratios for Mg isotope analysis

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J. Anal. At. Spectrom., 2024, 39,2767-2773
DOI: 10.1039/D4JA00266K, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Niklas Keller, Michael Tatzel
We present an efficient method to separate Mg from samples with high Ca/Mg matrices for the analysis of Mg isotope ratios. By utilising the automated sample purification system prepFAST, the labour is substantially minimised.
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A single-column and efficient procedure for separating Fe and Mg from geological materials for isotopic analyses using MC-ICP-MS

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J. Anal. At. Spectrom., 2024, 39,2783-2790
DOI: 10.1039/D4JA00272E, Paper
Guanhong Zhu, Zhenmin Ge, Le Zhang, Gangjian Wei, Jinlong Ma
We developed a single-column and efficient procedure for separating Fe and Mg from geological materials for isotope measurements.
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Accurate determination of ultra-trace REEs in seawater using a membrane desolvation Q-ICP-MS coupled with an online automatic separation system

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J. Anal. At. Spectrom., 2024, 39,2870-2883
DOI: 10.1039/D4JA00240G, Paper
Ji-Hao Zhu, Feng-You Chu, Feng Liang, Xian-Ying Luo, Qiang Liu, Quan-Hui Xu, Wei Yu, Yong-Chun Li, Jiang-Gu Lu, Yun-Xiu Li, Yan-Hui Dong, Huai-Ming Li, Jun Zhao, Cai Zhang
A highly precise method, based on a traditional Q-ICP-MS coupled with an online automatic separation system and membrane desolvation sample introduction device, was developed for accurate determination of ultra-trace REEs in seawater samples.
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Research on a bimodal fusion detection method for surface defects of metal AM components based on LIBS

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J. Anal. At. Spectrom., 2024, 39,2917-2928
DOI: 10.1039/D4JA00159A, Paper
Xiaomei Lin, Jiangfei Yang, Yutao Huang, Jingjun Lin, Changjin Che
A bimodal fusion method using Laser-Induced Breakdown Spectroscopy (LIBS) is proposed to identify surface defects in metal additive manufacturing (AM) samples. This method integrates LIBS spectra with plasma image data to enhance defect detection.
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Assessment of the metal grain size of 12Cr1MoV steel by LIBS coupled with acoustic wave information

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00285G, Paper
Feiqiang Tang, Meirong Dong, Junbin Cai, Zhichun Li, Kaiqing Chen, Weijie Li, Shunchun Yao, Jidong Lu
A modelling scheme that integrates spectral and acoustic data was put forth as a means of enhancing the precision of grain size detection in 12Cr1MoV steel.
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Assessing the performance of handheld LIBS for predicting soil organic carbon and texture in European soils

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J. Anal. At. Spectrom., 2024, 39,2903-2916
DOI: 10.1039/D4JA00292J, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Alex Wangeci, Maria Knadel, Olga De Pascale, Mogens H. Greve, Giorgio S. Senesi
Evaluating the performance of handheld LIBS for determination of soil properties across a continental scale.
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Atomic spectrometry update: review of advances in the analysis of metals, chemicals and materials

By pubs.rsc.org
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J. Anal. At. Spectrom., 2024, 39,2617-2693
DOI: 10.1039/D4JA90052A, Atomic Spectrometry Update
Eduardo Bolea-Fernandez, Robert Clough, Andy Fisher, Bridget Gibson, Ben Russell
This review covers advances in the analysis of advanced materials, metals, fuels and lubricants, nanostructures, ceramics, refractories, chemicals, catalysts and nuclear materials by a range of techniques including ICP-MS, non-destructive surface ablation and X-ray.
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Evaluation of miniaturized ultrasonic nebulization for high-efficiency sampling in characterization of silver nanoparticles by single particle inductively coupled plasma mass spectrometry

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J. Anal. At. Spectrom., 2024, 39,2791-2798
DOI: 10.1039/D4JA00320A, Paper
Junhang Dong, Zhenli Zhu, Lujie Li, Pengju Xing, Shuyang Li, Lei Ouyang, Xing Liu, Wei Guo, Hongtao Zheng, Rong Qian
Miniaturized ultrasonic nebulization (MUN) provides high sampling efficiency for single particle inductive coupled plasma mass spectrometry (sp-ICPMS).
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Hydrophobicity induced graphene oxide based dispersive micro solid phase extraction of strontium from seawater and groundwater prior to GFAAS determination

By pubs.rsc.org
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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D3JA00445G, Paper
Maria Sebastian, Saikrishna Devulapally, Sk. Jayabun, Noorbasha Nagula Meeravali, Shekhar Raparthi, A. C. Sahayam
A novel graphene oxide (GO) mediated dispersive micro solid phase extraction method is developed for the extraction of ultratrace level strontium (Sr) from seawater and ground water. This method involves...
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A new concept for correction of instrumental isotopic fractionation in MC-ICP-MS using a pair of monoisotopic elements: a critical evaluation

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00117F, Paper
Open Access
Andrii Tupys, Klaudia Tetfejer, Ludwik Halicz, Ewa Bulska, Jakub Karasiński
In this research work, we investigated the possibility of using mixtures of monoisotopic elements (93Nb/89Y, 165Ho/159Tb and 209Bi/197Au) as calibrators for accurate determination of isotope ratios by multicollector mass spectrometry (MC-ICP-MS).
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INSIGHTS INTO THE ROLE OF TRANSITION AND NOBLE METALS MEDIATING PHOTOCHEMICAL VAPOR GENERATION

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00261J, Tutorial Review
Open Access
Ralph E Sturgeon, Enea Pagliano, Gisele Simone Lopes, Renato Neto, Jane Kelly Sousa Brito
Abstract The recent expansion of the suite of elements amenable to photochemical vapor generation (PVG) is primarily linked to the addition of mg/L concentrations of selected transition metals (TMs) to...
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Chemical analysis of Chang’e-5 lunar soil using LA–ICP–MS in highly diluted fused glass discs

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00329B, Technical Note
Shi-Tou Wu, Ding-Shuai Xue, Yue-Heng Yang, Hao Wang, Chunlai Li, Fu-Yuan Wu
The bulk chemical compositions of extraterrestrial material can provide critical information on the evolution and magmatism of planetary bodies. However, accurate measurements are challenging, because these samples, particularly returned samples,...
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A single-stage purification method for the precise determination of zirconium isotopic composition in geological samples by double spike MC-ICP-MS

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00332B, Paper
Lanping Feng, Chen Wang, Yan Han, Wen Zhang, Jing-Liang Guo, Lian Zhou, Zhaochu Hu
A simple, fast and efficient column separation method for extracting Zr from geological sample matrices using DGA resin.
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A simple method for elemental analysis of liquids in sprayed microdroplets by laser-induced breakdown spectroscopy

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00192C, Paper
Jun Feng, Yihui Yan, Yuzhu Liu, Jozef Lengyel
The study shows that paper spray and laser-induced breakdown spectroscopy (PS-LIBS) analyze trace elements in aqueous solutions, addressing challenges in bulk analysis. Its efficiency highlights its potential for in situ liquid sample analysis.
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Robust determination of low Ti contents in zircon using LA–ICP–MS/MS with NH3 reaction gas

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00304G, Paper
Junlong Niu, Shitou Wu, Yueheng Yang, Hao Wang, Chao Huang, Lei Xu, Liewen Xie
Compared with the single quadrupole (SQ) mode, Triple Quadrupole (TQ) method is more robust for determining low Ti contents in zircon at high spatial resolutions (laser spot size <20 μm), making it useful for the analysis of complex zircon grains.
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Determination of boron isotopic compositions in five fractions of soil boron: traces of the environmental behavior of boron in soil

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00286E, Paper
Xuejun Chen, Qingcai Xu, Li Yan, Xiaodong Hao, Xiaochen Guan, Xiaopeng Han, Aide Sun, Zhiqun Chen, Lihua Liu, Zihao Zhu
A stepwise extraction method established for boron isotope measurement of five fractions in soil boron showed their feathered isotopic signals.
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Fast analysis of metal components in coal dust using spark emission spectroscopy

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00322E, Paper
Jialin Li, Jing Huang, Lina Zheng, Shakila Naz, Xutong Liu
We present a fast method based on spark emission spectroscopy to quantify metal components such as Al, Si, Fe, Ca, and Ti in airborne coal dust.
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A miniaturized microplasma excitation source coupled with photochemically induced volatile species generation as a cost-effective tool for in situ mercury pollution analyses

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00306C, Technical Note
Open Access
Tymoteusz Klis, Pawel Pohl, Anna Dzimitrowicz, Piotr Jamroz
A portable, miniaturized atmospheric microplasma discharge system coupled with the photochemical vapour generation was developed for the sensitive Hg determination in water samples using OES.
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Investigation of direct simultaneous uranium isotopic determination and age dating of micrometer-sized uranium particles by laser ablation – multi-collector ICPMS

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00280F, Paper
Anne-Claire Humbert, Fabien Pointurier, Amélie Hubert
The proposed method offers to the analytical community an alternative technique for uranium particle aged dating more widely available than LG SIMS. Moreover, working on μm-sized particles reduces issues with laser-induced fractionation.
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A Gaussian Spot Overlap Ablation Model for Prediction of Aluminium Alloy Spectral Peak Intensity in High Pulse Repetition Frequency LIBS

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00298A, Paper
Dongming Qu, Bohao Su, Zhongshu Bai, Biye Liu, Xueying Jin, Guanyu Chen, Yuting Fu, Tingwen Gu, Guang Yang, Qingkai Li
The use of microjoule high pulse repetition frequency (PRF) lasers as excitation sources is an important direction in the miniaturisation of laser-induced breakdown spectroscopy (LIBS) instruments. However, high PRF LIBS...
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Magneto-electrical fusion enhancement of LIBS signal: A case of Al and Fe emission lines’ characteristic analysis in soil

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00223G, Paper
Zihan Yang, Mengyu Pang, Jincheng Ma, Yanru Zhao, Keqiang Yu, Y. He
Soil is a vital resource for human survival. In particular, aluminum (Al) and iron (Fe) metal elements in soil play significant roles in stabilizing soil organic matter. Therefore, the rapid...
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Sensitive and Rapid Determination of Iodine/Calcium Ratio in Carbonate Rock Samples by ICP-MS Based on Solution Cathode Glow Discharge Sampling

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00264D, Paper
Xuan Wang, Xing Liu, Lanlan Jin, Zhenli Zhu, Junhang Dong, Pengju Xing, Linjie Chen, Yuanhui Geng, Jingwen Zhang, Hao Tong, Hongtao Zheng, Min Zhang, Shenghong Hu
The iodine-to-calcium ratio (I/Ca) in carbonate rocks has been extensively used to indicate marine oxidation states. However, the low-iodine and high-calcium characteristics of carbonate samples pose challenges in achieving rapid...
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High-precision MC-ICP-MS measurements of Cd isotopes using a novel double spike method without Sn isobaric interference

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00357H, Paper
Jin Li, Suohan Tang, Xiangkun Zhu, Jianxiong Ma, Zhi-Yong Zhu, Bin Yan
Previous studies have reported that even low concentrations of Sn can lead to biased Cd isotopic measurements using MC-ICP-MS. In this paper, we propose a novel method of Cd isotopic...
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Laser-Induced Breakdown Spectroscopy (LIBS): calibration challenges, combination with other techniques, and spectral analysis using data science

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00250D, Critical Review
Dennis Ferreira, Diego Victor De Babos, Mauro Henrique Lima-Filho, Heloisa Froehlick Castello, Alejandro C. Olivieri, Fabiola Manhas Verbi Pereira, Edenir Rodrigues Pereira-Filho
Laser-Induced Breakdown Spectroscopy (LIBS) is a versatile and powerful analytical technique widely used for rapid, in-situ elemental analysis across various fields, from industrial quality control to planetary exploration. This review...
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Fundamental studies of laser ablation ICPMS using a nitrogen plasma source and helium, argon and nitrogen as carrier gas

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00327F, Paper
Open Access
Dylan Käser, Ralf Kägi, Bodo Hattendorf, Detlef Günther
Nitrogen as alternative carrier gas for LA-ICPMS showed similar sensitivities and quantification capabilities as using helium in combination with a N2 plasma. The role of the gas and of the ablation cell design on the aerosol structure was studied.
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Applying standard addition to determine antimony isotopes in low-Sb samples using HG-MC-ICP-MS

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J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00333K, Paper
Honggang Zhu, Jian-Ming Zhu, Decan Tan, Zhuo Lu, Hongfei Liao, Yiwei Ma
The δ123Sb value of BCR-2 obtained by the standard addition (SA) method.
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External electric field assisted laser-induced plasma and bubble dynamics for optimizing Mn2O3 nanoparticles as UV emitters.

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00163J, Paper
Sanchia M. Kharpanbuh, Arpita Nath
To gain a deeper understanding of how the size of the nanoparticles synthesized by Electric Field-Assisted Laser Ablation in Liquids (EFLAL) changes with the applied electric field, we use Laser-Induced...
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SPCal - An open source, easy-to-use processing platform for ICP-TOFMS based single event data

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J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00241E, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Thomas Edward Lockwood, Lukas Schlatt, David Clases
Single particle inductively coupled plasma – mass spectrometry (SP ICP-MS) has evolved into one of the most powerful techniques for the bottom-up characterisation of nanoparticle suspensions. The latest generations of...
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Six reasons why people buy luxury homes

By www.thehindu.com
Published On :: Fri, 24 Apr 2015 16:32:31 +0530

Anil Pharande tells us what drives the demand for über luxury homes in India


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Trends in residential realty

By www.thehindu.com
Published On :: Fri, 08 May 2015 20:56:03 +0530

Sanjay Chugh writes on the renewed momentum in Chennai's residential market.


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Your choicest designs are just a click away

By www.thehindu.com
Published On :: Fri, 08 May 2015 21:35:50 +0530

Modular kitchen, wardrobes, cabinets, wall entertainment units, and even fixed furniture, you name it, the long list of wood work to suit your taste and wallet is just a few clicks away


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Six attributes of a good neighbourhood

By www.thehindu.com
Published On :: Fri, 22 May 2015 16:48:22 +0530

Kishor Pate writes on factors that determine the value of your property


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The fight for more FSI

By www.thehindu.com
Published On :: Fri, 29 May 2015 15:30:30 +0530

Chennai requires a higher Floor Space Index to make housing affordable, reduce costs and raise building flexibility, say developers.


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Financing affordable housing projects

By www.thehindu.com
Published On :: Fri, 05 Jun 2015 15:46:07 +0530

IFC, Tata Housing to collaborate and build 16,800 homes in the venture


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Renewed momentum in residential realty

By www.thehindu.com
Published On :: Fri, 05 Jun 2015 16:00:23 +0530

Sanjay Chugh writes on the factors contributing to the growth of Chennai’s realty sector


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FSI: Point Counterpoint

By www.thehindu.com
Published On :: Fri, 05 Jun 2015 16:09:30 +0530

Increasing the FSI need not be the only solution to make housing affordable, argues A. Venkatasubramanian


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Making life easier for landlords

By www.thehindu.com
Published On :: Fri, 17 Jul 2015 13:09:51 +0530

The Draft Model Tenancy Act 2015 is all set to encourage the rental market, as it promises to safeguard the interests of both landlords and tenants.


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Housing, simplified

By www.thehindu.com
Published On :: Fri, 02 Oct 2015 21:24:25 +0530

In a scenario where prices are beyond one’s affordability, the proposal of the Labour Ministry, under whom the EPFO is functioning, to provide housing finance is noteworthy


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