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A safe and new strategy for N-arylation of 2,4-thiazolidinediones via microwave irradiation using base catalyst K2CO3 in DMF

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React. Chem. Eng., 2024, 9,842-848
DOI: 10.1039/D3RE00641G, Paper
Ragini C. Patil, Nita M. Khiratkar, Sumeer Ahmed, Joazaizulfazli Jamalis, Aso Hameed Hasan, Malika Berredjem, Sarkar M. A. Kawsar, Ajmal R. Bhat
Green efforts as an alternative to existing conventional methods for providing new tools, knowledge and design of organic synthesis, will contribute to the economy and protecting the environment and health.
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Encapsulation of TixFeyLamOz nanoparticles into NH2-MIL-125(Ti) to fabricate a promising photocatalyst for the C–N coupling reaction

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React. Chem. Eng., 2024, 9,849-860
DOI: 10.1039/D3RE00457K, Paper
Yahya Absalan, Mohammad Rafsanjani Dehghazi, Reza Samavati, Kambiz Souri, Mostafa Gholizadeh
An array of organic compounds and natural products can be synthesized through carbon–nitrogen coupling reactions.
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Machine-learning assisted optimisation during heterogeneous photocatalytic degradation utilising a static mixer under continuous flow

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React. Chem. Eng., 2024, 9,872-882
DOI: 10.1039/D3RE00570D, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Thomas M. Kohl, Yan Zuo, Benjamin W. Muir, Christian H. Hornung, Anastasios Polyzos, Yutong Zhu, Xingdong Wang, David L. J. Alexander
Machine-learning assisted optimisation of a continuous photodegradation reaction, using a TiO2 coated catalytic static mixer successfully accounting for catalyst degradation.
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Green synthesis of surfactant-free mesoporous silica with strong hydrophilicity via metal salt modifications for moisture adsorption

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React. Chem. Eng., 2024, 9,816-824
DOI: 10.1039/D3RE00513E, Paper
Pariyawalee Sangteantong, Kunpirom Chainarong, Waleeporn Donphai, Metta Chareonpanich
In this work, the green synthesis of mesoporous silica (MPS) was carried out using low-cost sodium silicate as a precursor.
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Understanding the effects of forced and bubble-induced convection in transport-limited organic electrosynthesis

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React. Chem. Eng., 2024, 9,930-939
DOI: 10.1039/D3RE00579H, Paper
Casey K. Bloomquist, Melisa Dogan, James S. Harris, Benjamin D. Herzog, William J. Tenn III, Eray S. Aydil, Miguel A. Modestino
Insights from data-driven surrogate models reveal that the Sherwood number characterizes mass transport conditions independent of the convection method, offering design guidelines for scaling up organic electrosynthesis.
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Interaction of SO2 with a Cu–Mn oxide oxygen carrier during chemical looping with oxygen uncoupling

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React. Chem. Eng., 2024, 9,888-900
DOI: 10.1039/D3RE00498H, Paper
Turna Barua, Bihter Padak
During chemical looping combustion with oxygen uncoupling (CLOU) fuel-sulfur species impact the reactivity of Cu–Mn oxide oxygen carrier with CH4. SO2 oxidation to SO3 competes with fuel for available O2 and lowers CH4 conversion.
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Selective aerobic oxidative C–C bond cleavage using a high-entropy oxide-derived multimetallic catalyst

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React. Chem. Eng., 2024, 9,967-973
DOI: 10.1039/D3RE00525A, Paper
Shaoyuan Guo, Xinli Tong, Jipeng Wang, Hang Tang
A stable and efficient high entropy catalyst is developed for the selective oxidative C–C bond cleavage in the presence of O2.
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From microkinetic model to process: understanding the role of the boron nitride surface and gas phase chemistry in the oxidative dehydrogenation of propane

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React. Chem. Eng., 2024, 9,795-802
DOI: 10.1039/D3RE00600J, Paper
Unni Kurumbail, William P. McDermott, Edgard A. Lebrón-Rodríguez, Ive Hermans
In the oxidative dehydrogenation of propane over boron nitride, propylene selectivity is lost due to unselective gas-phase chemistry.
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At-line monitoring of hydrogen peroxide released from its photocatalytic and continuous synthesis

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React. Chem. Eng., 2024, 9,777-781
DOI: 10.1039/D3RE00659J, Communication
Open Access
Anders Ø. Tjell, Lars-Erik Meyer, Barbara Jud, Selin Kara, Torsten Mayr
Photocatalytic synthesis of H2O2 in a continuous operation set-up using nitrogen-doped carbon nanodots (N-CNDs) and simultaneous determination of generated H2O2.
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Digital Pareto-front mapping of homogeneous catalytic reactions

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React. Chem. Eng., 2024, 9,787-794
DOI: 10.1039/D3RE00673E, Communication
Open Access
Negin Orouji, Jeffrey A. Bennett, Sina Sadeghi, Milad Abolhasani
We present a digital framework for rapid multi-objective reaction space exploration and optimization of homogeneous catalytic reactions through autonomous experimentation and Bayesian optimization.
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Surface treatment of magnetite nanoparticle thin films with potassium phosphate for calcium phosphate precipitation

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React. Chem. Eng., 2024, 9,782-786
DOI: 10.1039/D4RE00048J, Communication
Reo Kimura, Kazuto Sugimoto, Iori Yamada, Motohiro Tagaya
The treatment of magnetite nanoparticle thin films with potassium phosphate and their surface reaction with simulated body fluid were in situ monitored by the QCM-D technique, which is suitable for the precipitation of calcium phosphate.
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Merging inline crystallization and pulsed flow operation to enable enantiospecific solid state photodecarbonylation

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00058G, Paper
Open Access
Bavo Vandekerckhove, Bart Ruttens, Bert Metten, Christian V. Stevens, Thomas S. A. Heugebaert
Photoelimination of α-chiral ketones in the solid state results in highly regio- and enantiospecific C–C bond formation. By combining inline crystallisation and pulsatile flow, the photochemistry of these slurries can now be run fully continuously.
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Comprehensive Study of Lumped Kinetic Models and Bio-Oil Characterization in Microwave-Assisted Pyrolysis of Sargassum sp.

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React. Chem. Eng., 2024, Accepted Manuscript
DOI: 10.1039/D3RE00674C, Paper
Teta Fathya Widawati, Muhammad Fuad Refki, Rochmadi Rochmadi, Arief Budiman
Indonesia, renowned for its tropical marine environments, boasts a rich diversity of macroalgae, with Sargassum being a major contributor. Currently, Sargassum's primary application revolves around alginate extraction, prompting a systematic...
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Selective hydrogenation of 5-hydroxymethylfurfural to 2,5-bis(hydroxymethyl)furan over Ni–Ga intermetallic catalysts and its kinetic studies

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00129J, Paper
Weixiao Sun, Fuzeyu Zhong, Xiaohu Ge, Wenyao Chen, Gang Qian, Yueqiang Cao, Xuezhi Duan, Xinggui Zhou, Jing Zhang
5-Hydroxymethylfurfural (HMF) has been listed as the “TOP 14” most important biomass-derived platform molecules, which can be converted into 2,5-bis(hydroxymethyl)furan (BHF) via selective hydrogenation of the carbonyl group on HMF.
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Novel TPMS carbon-based monolithic catalysts by three-dimensional printing for enhancement of nitrobenzene hydrogenation reaction

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00049H, Paper
Haoyang Wang, Haoran Tian, Qi Zhang, Li Zhang
Preparation of periodic curved surface, structured, carbon-based catalysts using a 3D printing method achieved good results in the hydrogenation of nitrobenzene to aniline in a packed-bed micro-reactor.
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Thermokinetic analyses of metal-sensitive reactions in a ceramic flow calorimeter

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00014E, Paper
Open Access
Soritz S., Sommitsch A., Irndorfer S., Brouczek D., Schwentenwein M., Priestley I. J. G., Iosub A. V., Krieger J. P., Gruber-Woelfler H.
A ceramic flow calorimeter for metal-sensitive reactions is characterized and used to obtain thermokinetic data on highly exothermic reactions.
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Catalytic degradation of pine sawdust over heterotopic Ca–Fe and HZSM-5 to produce aromatic hydrocarbons

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D3RE00572K, Paper
Huifen Kang, Xintong Guo, Mei An, Conghua Ma, Guozhang Chang, Qingjie Guo, Jingjing Ma
Up to 90.47% aromatic proportion and a 31.02 mg g−1 BTEX yield were obtained by heterogeneous catalysis of Ca–Fe and HZSM-5.
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Efficient aqueous-phase hydrogenation of m-xylylenediamine to 1,3-cyclohexandimethylamine over a highly active and stable ruthenium catalyst

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D3RE00712J, Paper
Jing Guo, Heng Shao, Le Gao, Wancheng Ma, Wei Zhang, Long Huang, Haibin Chu
The strong interaction between Ru and –NH2 in Ru/NH2–Al2O3 led to the formation of highly dispersed Ru and modification of its electronic properties, and consequently greatly enhanced its performance and stability.
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Automated kinetic model identification via cloud services using model-based design of experiments

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00047A, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Emmanuel Agunloye, Panagiotis Petsagkourakis, Muhammad Yusuf, Ricardo Labes, Thomas Chamberlain, Frans L. Muller, Richard A. Bourne, Federico Galvanin
Industry 4.0 has birthed a new era for the chemical manufacturing sector, transforming reactor design and integrating digital twin into process control.
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Photochemical organocatalytic heteroarylation of anilines and secondary alicyclic amines in continuous-flow

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00130C, Paper
Egor N. Boronin, Milena M. Svetlakova, Ilya I. Vorobyov, Yulia B. Malysheva, Yuri V. Polushtaytsev, Sergey N. Mensov, Andrey V. Vorotyntsev, Alexey Yu. Fedorov, Timothy Noël, Alexander V. Nyuchev
Photoorganocatalytic arylation of amines in continuous-flow enables scaling up including decreasing of both reaction time and catalyst loading.
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On a seamlessly replicable circular photoreactor for lab-scale continuous flow applications

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React. Chem. Eng., 2024, Accepted Manuscript
DOI: 10.1039/D4RE00109E, Paper
Yi-Hsuan Tsai, Martin Cattoen, Guillaume Masson, Gabrielle Christen, Lisa Traber, Morgan Donnard, Frederic R. Leroux, Guillaume Bentzinger, Sylvain Guizzetti, Jean-Christophe M. Monbaliu
A cost effective and replicable continuous flow circular photoreactor system is introduced. All body parts of the reactor are 3D-printed and the electronics are purchased from various mainstream suppliers. The...
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A sequential lumped kinetic modelling approach for the co-pyrolysis of plastic mixtures with a heavy refinery intermediate product in a tubular reactor

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00075G, Paper
Open Access
Sebastian-Mark Lorbach, Andreas E. Lechleitner, Teresa Schubert, Markus Lehner
A novel sequential approach for the lumped kinetic modelling of a plastic pyrolysis process in a tubular reactor.
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High-efficiency non-thermal plasma synthesis of imine macrocycles

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00061G, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Patrycja Roszkowska, Abbie M. Scholes, James L. Walsh, Timothy L. Easun, Anna G. Slater
Non-thermal plasma synthesis offers efficient access to imine macrocycles.
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Scaling-up continuous production of mesoporous silica particles at kg scale: design & operational strategies

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D3RE00707C, Paper
Rajashri B. Jundale, Jayesh R. Sonawane, Anil V. Palghadmal, Hemant Kumar Jaiswal, Hital S. Deore, Amol A. Kulkarni
This paper demonstrates a continuous flow pilot-scale production of highly porous mesoporous silica particles (MSPs) via a soft template based technique.
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Hydrothermal liquefaction of plastics: a survey of the effect of reaction conditions on the reaction efficiency

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D2RE00510G, Review Article
Open Access
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Matthijs Justin Boel, Hongqi Wang, Ahmad AL Farra, Laura Megido, José Manuel González-LaFuente, N. Raveendran Shiju
Plastic waste is a major global issue and hydrothermal liquefaction is a promising technique for the chemical recycling of waste plastics. This review summarises the effect of reaction conditions on the liquefaction efficiency.
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Correction: Applying quantum mechanics to deconvolute benchtop 1H NMR reaction data

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE90015D, Correction
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Jiayu Zhang, Tristan Maschmeyer, Ben Shapiro, Sunil Babu Paudel, Matthew C. Leclerc, Jason E. Hein
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Synthesis and kinetic study of 1,3,2-dioxathiolane 2,2-dioxide in microreactors

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React. Chem. Eng., 2024, Accepted Manuscript
DOI: 10.1039/D4RE00123K, Paper
Ting Wang, Junnan Wang, Chengxiang He, Zhongdong Wang, Yating Li, Chunying Zhu, Youguang Ma, Taotao Fu
1,3,2-dioxathiolane 2,2-dioxide (DTD) is an essential intermediate in organic synthesis and plays a vital role in improving the performance and service life of lithium-ion batteries. A large amount of heat...
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Generation of nitrogen by means of electrochemical oxygen depletion

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00104D, Paper
Open Access
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Dominik Sachse, Basil Noha Chelachottil, Andreas Glüsen, Martin Müller, Uwe Rau, Ralf Peters
Electrochemical oxygen reduction enables a high depletion of the oxygen content with very high Faraday efficiency at the same time.
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Efficient removal of dibutyl phthalate from aqueous solutions: recent advances in adsorption and oxidation approaches

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React. Chem. Eng., 2024, Advance Article
DOI: 10.1039/D4RE00055B, Review Article
Yaqi Wang, Jiawei Wu, Wenju Zhang, Linyun Zhong, Dan Zhang, Siqi Yan, Junyou Shi
Dibutyl phthalate (DBP), a recognized endocrine-disrupting contaminant, poses substantial environmental challenges due to its persistence, resistance to degradation, and potential for bioaccumulation.
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India Cements’ Q2 loss widens on falling cement prices despite eased cost pressures

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 16:22:18 +0530

India Cements reports a sharp increase in its net loss to ₹240 crore


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LatentView Analytics Q2FY25 net profit grows 17%

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 16:50:20 +0530

The acquisition of Decision Point Analytics has concluded and integration of the GTM and delivery teams is underway


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Ola Electric sees 5% y-o-y loss reduction to ₹495 crore for Q2FY25

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 18:46:40 +0530

Revenue for the quarter under review increased by 38.5 per cent y-o-y to ₹1,240 crore from ₹896 crore in the year-ago period


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SIS Ltd eyes strategic acquisitions in India

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 19:19:36 +0530

Plans listing of cash logistics joint venture


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Create SECI-like entity for efficient long-term procurement of green hydrogen: TERI

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 19:35:48 +0530

The policy think tank also recommends creating an SPV for each industrial segment for development of pilot plants


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Lupin aims to be part of ‘first wave of generics’ on GLP-1 products: Nilesh Gupta

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 19:52:26 +0530

GLP-1 products going off patent in some markets includes popular Type-2 diabetes and weight-loss drug Ozempic


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Ashok Leyland expands to Southeast Asia, expects domestic market recovery in H2

By www.thehindubusinessline.com
Published On :: Fri, 08 Nov 2024 20:25:25 +0530

EV Arm Switch Mobility set for EBITDA break-even this fiscal


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ITC’s snack brand Bingo! Inks five-year partnership to promote Pickleball in India

By www.thehindubusinessline.com
Published On :: Mon, 11 Nov 2024 15:53:52 +0530

This partnership, starts with the Bingo! World Pickleball Championship (WPC)


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Domestic tractor sales hit historic high in festive October, H2 outlook remains robust

By www.thehindubusinessline.com
Published On :: Mon, 11 Nov 2024 18:18:55 +0530

Total tractor sales in the domestic market grew by 23%per cent to 144,675 units in October 2024


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L&T Technology Services to acquire Silicon Valley-based Intelliswift

By www.thehindubusinessline.com
Published On :: Mon, 11 Nov 2024 22:16:04 +0530

LTTS claims the acquisition will deepen its offerings across software product development, platform engineering, digital integration, data, and AI


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Bharat Dynamics partners with Russia’s Rosoboronexport for air defence systems

By www.thehindubusinessline.com
Published On :: Tue, 12 Nov 2024 07:18:03 +0530

The agreement, sed during the 5th India-Russia Inter-Governmental Commission meeting in Goa, aims to diversify India’s air defence capabilities


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ABCs of organic home gardening

By www.thehindu.com
Published On :: Fri, 31 Jan 2014 18:23:02 +0530

How do we tackle pests without synthetic pesticides? How can we get a huge haul of vegetables without resorting to chemical fertilisers? A workshop series teaches us organic gardening step-by-step


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Nature, nurture and niches in cities

By www.thehindu.com
Published On :: Fri, 02 May 2014 21:34:02 +0530

Even if you can’t go to the wild and soak in diverse ecosystems look around and you will find them right here in our city, says Pauline Deborah R.


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Pave it aesthetically

By www.thehindu.com
Published On :: Fri, 10 Apr 2015 20:33:57 +0530

Concrete, stone, burnt brick, clay… you have multiple options when designing pathways in a garden.


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Structure it geometrically

By www.thehindu.com
Published On :: Fri, 08 May 2015 21:48:37 +0530

Design patterns and angles should flow naturally, and create smooth symmetrical finishes, says Nandhini Sundar


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Time to lift restrictions on planting sandalwood?

By www.thehindu.com
Published On :: Fri, 05 Jun 2015 15:49:12 +0530

Hema Vijay writes on the benefits of growing this fragrant tree at home


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Raising organic gardens at home

By www.thehindu.com
Published On :: Fri, 30 Oct 2015 14:19:55 +0530

More people are now raising organic kitchen gardens with resources and guidance available even online


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Why does India lag behind in automatic cars?

By www.thehindubusinessline.com
Published On :: Wed, 08 May 2013 17:51:21 +0530


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Microencapsulation of broccoli sulforaphane using whey and pea protein: in vitro dynamic gastrointestinal digestion and intestinal absorption by Caco-2-HT29-MTX-E12 cells

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Published On ::

Food Funct., 2024, Advance Article
DOI: 10.1039/D4FO03446E, Paper
Open Access
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Ali Ali Redha, Luciana Torquati, John R. Bows, Michael J. Gidley, Daniel Cozzolino
Sulforaphane-rich extract was prepared from broccoli. The extract was encapsulated with whey and pea protein isolates by freeze-drying. The products were characterised and assessed for in vitro bioaccessibility and bioavailability.
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Pentadecanoic acid (C15:0, PA) induces mild maternal glucose intolerance and promotes the growth of the offspring partly through up-regulating liver PPARα and MAPK signaling pathways

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Published On ::

Food Funct., 2024, Advance Article
DOI: 10.1039/D4FO03970J, Paper
Jun Wang, Shiqi Zheng, Ziying Li, Yimei Tang, Yanhua Huang, Junwen Wang, Rui Li, Jie Peng
1% PA can induce a mild decrease in the maternal glucose tolerance and lipolysis mainly by activated MAPK and PPARα signaling.
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