CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00370K, Paper

Corrado Di Nicola, Alessia Tombesi, Marco Moroni, Rebecca Vismara, Fabio Marchetti, Riccardo Pettinari, Luca Nardo, Guglielmo Vesco, Simona Galli, Silvia Casassa, Luciano Pandolfo, Claudio Pettinari
Enlarging the family of CPs with the {Cu(μ-pz)₂} building unit: synthesis, thermal behaviour, crystal structure and spectroscopic properties of [Cu(μ-4-Xpz)₂(μ-DMF)]_n (4-Xpz = 4-Xpyrazolate, X = H, Cl, Br, I) and the non-solvated counterparts.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00416B, Communication

Takumi Kusakawa, Takayuki Goto, Akiko Hori
Expanded π-conjugated coordination complexes, [M(L²)₂] (M = Cu²⁺, Pd²⁺, Pt²⁺; L² = dinaphthoylmethanido⁻), were prepared and their unique electron contributions and electrophile/nucleophile characteristics were found due to the supramolecular associations.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00317D, Paper

Zhen-Li Yang, Jian Qin, Jun- Qing Yang , Jianguo Zhang
Research on novel energetic coordination polymers (ECPs) is becoming increasingly important for energetic materials, numerous ECPs were reported and found to be potential energetic materials. In this study, 4,5-dicarboxylic-1,2,3-triazolean was...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00255K, Paper

Yunhao Zang, Jinying Wang, Jianfeng Gu, Jiangying Qu, Feng Gao
Herein, a mesoporogen-free, and steam-assisted route is proposed to synthesize highly crystalline hierarchical HZSM-5 using Stöber silica spheres as the precursor. The effect of crystallization time on the morphology and...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00269K, Paper

Selma Piranej, Michael A. W. Shelhart Sayers, Gregory J. Deye, Sergey N. Maximoff, Jonathan P. Hopwood, Haejun Park, Jean G. Slavsky, Jacob Ciszek
Reactivity trends for molecular solids cannot be explained exclusively through topochemical phenomenon (i.e. diffusivity, reaction cavities) or electronic structure of the molecules. As an example of this class, Diels-Alder reactions...
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00294A, Paper

Chih-Tung Yang, Xiang-Kai Yang, Ji-Hong Hu, Wei-Te Lee, Tsun-Ren Chen, Chih-Chieh Wang, Jhy-Der Chen
Two extended metal chains based on linear tetracopper units are reported, in which the bromide complex undergoes reversible structural transformation and luminescence change.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00489H, Highlight

Zhonghua Pan, chenglong deng, zhi wang , Jin-Qing Lin, Geng-Geng Luo, Di Sun
Silver clusters with atomic precision have garnered immense attention owing to their aesthetic structures and fascinating properties. Assembly of silver clusters involves organizing positively charged silver ions into an intricate...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00430H, Paper

Hai-Huan Yu, Jia-Qi Chi, Zhong-Min Su, Xiao Li, Jing Sun, Chen Zhou, Xiao-Li Hu, Qun Liu
The existence of Cr2O72- anions, excessive Fe3+ cations in water and picric acid in seawater have irreversible harm to human health and aquatic organism. Herein, a water-stable terbium metal-organic framework...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00347F, Paper

Yu Feng, Erwei Du, Shijing Gong, Ke Yu, Xiaofan Chen, Ziqiang Zhu
The MoS2@VS2 micro-nano composite was synthesized via a two-step hydrothermal method. The field emission properties of MoS2@VS2 micro-nano composite were investigated for the first time. The finger-like VS2 has a...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00360C, Paper

Xiufang Li, Qunmei Fan, Qiang Zhang, Shuqin Yan, Renchuan You
Thermal annealing strongly impacts the crystallization of proteins. Despite the fundamental importance for the crystallization of silk fibroin, the underlying crystallization kinetics of silk fibroin in freezing state has not...
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00168F, Paper

Shubhangi Kakkar, K. Renuka Devi, Michael Svärd, Åke Rasmuson
Nucleation behaviour of salicylamide in different solvents was determined and compared with salicylic acid, attempting to progress the rationalization of the influence of the solvent and solute on crystal nucleation of organic compounds in solution.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE90057E, Correction

Open Access

  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.

Chenglan Zhao, Yuqian Jiang, Shunfei Liang, Fang Gao, Li Xie, Lingyun Chen
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00526F, Paper

Shuang Zhao, Baiqi Shao, Yang Feng, Senwen Yuan, Langping Dong, Liang Zhang, Hongpeng You
A novel synthesis strategy of porous/hollow YVO₄ submicro-ellipsoids with multicolor emissions has been developed based on the high structural matching of LYH and YVO₄.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00297F, Paper

Zhihui Hu, Zhi Chen, Juntong Huang, Mingge Yan, Meng Zhang, Lei Zhang, Xibao Li, Zhijun Feng
3C-SiC nanowires with nanosheets were synthesized via a direct reaction of Si vapor (from solid silicon) and SiO vapor (from silicon and silicon dioxide) with graphene nanosheets at 1500 °C without any additional metal catalyst.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00026D, Paper

Open Access

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Thai T. H. Nguyen, Robert B. Hammond, Ioanna D. Styliari, Darragh Murnane, Kevin J. Roberts
A detailed inter-molecular (synthonic) analysis of terbutaline sulfate, an ionic addition salt for inhalation drug formulation, is related to its crystal morphology, the surface chemistry of the habit faces and hence to its crystal surface energy.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/C9CE01884K, Communication

Shuangliang Cheng, Rachel E. Hunneke, Mengkun Tian, Eric Lukosi, Mariya Zhuravleva, Charles L. Melcher, Yuntao Wu
We developed novel LiCl–CeCl₃ eutectic scintillators that are capable of detecting thermal neutrons.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00084A, Paper

Yang Wang, Mengjia Luo, pei Zhao, Xiangli Che, Yunzhen Cao, Fu Qiang Huang
A new mid-infrared nonlinear optical oxyselenide, Sr₄Pb_1.5Sb₅O₅Se₈, was successfully synthesized by traditional solid-state reaction. It crystallizes in the noncentrosymmetric space group Cm (No. 8) of the monoclinic system. The crystal...
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE90053B, Editorial

We would like to take this opportunity to highlight the Outstanding Reviewers for CrystEngComm in 2019, as selected by the editorial team for their significant contribution to the journal.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00204F, Paper

Zhi-Ping Shi, Guo-Bin Ren, Ming-Hui Qi, Zhong Li, Xiaoyong Xu
Based on reported isomorphism of Azoxystrobin (AZO) solvates, five novel AZO solvates, including dimethyl succinate solvate (AZO-DMS), ethyl butyrate solvate (AZO-EB), thiophene solvate (AZO-TP), furan solvate (AZO-FN), and 1,2-diethoxyethane solvate...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00386G, Paper

Jinxin Huang, Zongqi Wang, Bing Teng, Hong Liu, Xixi Zheng, Shaohua Ji
A series of K(D_xH_1-x)₂PO₄ (DKDP) crystals with different saturating temperature and deuteration levels were grown by point-seed rapid growth method. The correlation between deuterium segregation coefficient and temperature and deuterium...
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00311E, Paper

Lei Gao, Yunhui Hao, Xiunan Zhang, Xin Huang, Ting Wang, Hongxun Hao
Photomechanical motions of the polymorphs of trans-4,4'-azopyridine are distinct under the influence of different molecular packing and intermolecular interactions.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00214C, Paper

João P. P. Copetti, Paulo R. S. Salbego, Tainára Orlando, Jéssica M. L. Rosa, Gabriela F. Fiss, João P. G. de Oliveira, Mário L. A. A. Vasconcellos, Nilo Zanatta, Helio G. Bonacorso, Marcos A. P. Martins
The crystallization mechanisms of a series of fourteen 7-chloro-4-substituted-quinolines were proposed based on a retrocrystallization approach using the supramolecular cluster as demarcation.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00644K, Communication

Kazuyuki Maeda, Kentaro Wakui, Kyosuke Arakawa, Atsushi Kondo
Topotactic pillaring of lamellar aluminophosphate (ALPO) layers with zinc cations is used to prepare microporous zincoaluminophosphate (ZnAPO) with AFY-type framework for the first time. This approach should be promising for...
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00417K, Paper

Weidong Hou, Jia Yang, Haiming Xu, Dongya Li, Zhongwei Zou, Dongsheng Xia
Nymphaea-like BiOCl with oxygen vacancies (OVs) was successfully prepared by adjusting the pH of the precursor and using aspartic acid as surfactant. The as-fabricated samples were investigated by XRD, SEM,...
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CrystEngComm, 2020, 22,2904-2913
DOI: 10.1039/C9CE01157A, Paper

Edurne S. Larrea, Roberto Fernández de Luis, Arkaitz Fidalgo-Marijuan, Eva M. Maya, Marta Iglesias, Maria I. Arriortua
The versatility of CuBTC (HKUST-1) MOF materials to be functionalized to improve their catalytic activity performance was evaluated. CuBTC@IL catalysts are selective for the cycloaddition of CO₂ to epoxides, giving rise to value-added products.
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CrystEngComm, 2020, 22,2970-2977
DOI: 10.1039/D0CE00251H, Paper

Prasanata Kumar Bhaumik, Abhisek Banerjee, Tamal Dutta, Sudipta Chatterjee, Antonio Frontera, Shouvik Chattopadhyay
The ethoxy groups have a dual effect in hindering the attack of the pseudo-halides on the nickel(II) centre and also in stabilizing the complex by intra-molecular interactions.
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CrystEngComm, 2020, 22,3059-3069
DOI: 10.1039/D0CE00310G, Paper

Smriti Thakur, Sanjay K. Mandal
Morphology transformation and dimensionality change as a result of dilution and post-synthetic annealing are reported.
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CrystEngComm, 2020, 22,2978-2989
DOI: 10.1039/D0CE00106F, Paper

Utsav Garg, Yasser Azim, Aranya Kar, Chullikkattil P. Pradeep
Revisit of acid–aminopyrimidine synthons to explore the robustness in presence of linear hetrotetramer and heterotrimer synthon.
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CrystEngComm, 2020, 22,2914-2918
DOI: 10.1039/D0CE00244E, Paper

Shengliang Zhong, Honghong Zou, Yanhua Ji, Chenghui Zeng, Lei Wang, Yanhong Chen, Hualan Xu
Coordination polymer superstructures connected by a flange union with a good geometry were fabricated. Assembly, disassembly and reassembly process happened during the formation.
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CrystEngComm, 2020, 22,2919-2925
DOI: 10.1039/D0CE00067A, Paper

Kohei Yoshiyama, Masae Mori, Manabu Hagiwara, Shinobu Fujihara
The effect of the size and morphology of piezoelectric BiFeO₃ particles on the performance of BiFeO₃–PDMS composite generators is revealed.
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CrystEngComm, 2020, 22,2945-2952
DOI: 10.1039/D0CE00185F, Paper

Jiacheng Yao, Min Zhang, Hongfei Yin, Muhammad Arif, Xiaoheng Liu
Fabrication of rose-like WO₃ by chemical bath method.
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CrystEngComm, 2020, 22,2990-2997
DOI: 10.1039/D0CE00112K, Paper

Yan-Kai Li, Yu-Ge Wang, Cui-Liu Fu, You-Liang Zhu, Zhan-Wei Li, Zhao-Yan Sun
The crystallization transformation from form II to form I in PB-1/CNT materials is mainly influenced by the lamellar thickness.
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CrystEngComm, 2020, 22,3033-3041
DOI: 10.1039/D0CE00224K, Paper

Chunyan Dong, Yan Zhou, Na Ta, Wenjie Shen
Ceria nanocubes of 10–20 nm were hydrothermally synthesized, involving Ce(OH)₃ rods and small-sized CeO₂ polyhedra/cubes as building blocks.
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CrystEngComm, 2020, 22,2926-2932
DOI: 10.1039/D0CE00086H, Paper

Hualan Xu, Ran Liu, Yongmei Zhu, Jinjiang Li, Changfeng Wan, Hang Zhang, Chuying Ouyang, Shengliang Zhong
Scandium-based coordination polymer octahedrons with concaved surfaces have been fabricated. The formation mechanism was also investigated. Sc₂O₃ octahedrons were obtained after simple calcination in a N₂ atmosphere.
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CrystEngComm, 2020, 22,3070-3078
DOI: 10.1039/D0CE00075B, Paper

Yucheng Hao, Yang Pan, Yuan Lin, Linbo He, Guangjie Ge, Yu Ruan, Haida Zhou, Yang Xue, Kisan Koirala
Three novel highly porous aluminophosphates were synthesized through mild hydrothermal methods. Interestingly, among them, α-NaAlPO₄(OH) is polar and exhibits moderate nonlinear optical properties with a short cutoff edge.
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CrystEngComm, 2020, 22,2953-2963
DOI: 10.1039/D0CE00268B, Paper

Chenglan Zhao, Yuqian Jiang, Shunfei Liang, Fang Gao, Li Xie, Lingyun Chen
2D porous nickel oxalate thin sheets constructed by ultrathin nanosheets were first synthesized by using a simple hydrothermal method. The resulting porous thin sheets exhibited superior supercapacitor performance.
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CrystEngComm, 2020, 22,2884-2888
DOI: 10.1039/D0CE00305K, Communication

Mei-li Qi, Shengkun Yao, Xiao-Cun Liu, Xiaoning Wang, Fengkun Cui
Well-defined carbonated hydroxyapatite microspheres assembled from nanosheets were synthesized by a Na₂EDTA-assisted hydrothermal homogeneous precipitation route.
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CrystEngComm, 2020, 22,2933-2944
DOI: 10.1039/D0CE00275E, Paper

Anna Goldman, Beatriz Gil-Hernández, Simon Millan, Serkan Gökpinar, Christian Heering, Ishtvan Boldog, Christoph Janiak
The prototypal [M₂(EtBCP)₂(DABCO)_0.5] MOFs, compliant with isoreticular expansion in two-dimensions, show flexibility manifested by a two-step CO₂ adsorption isotherm, which might be associated to the “lever-action” of the metal-phosphonate moieties.
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CrystEngComm, 2020, 22,3042-3058
DOI: 10.1039/D0CE00157K, Paper

Xiangyang Li, Jianjun Ding, Pujing Chen, Kang Zheng, Lin Chen, Xingyou Tian
The interface distribution function is composed mainly of the self-interference item of the first interface F₁₁, the interference term of the first and the second interfaces F₁₂, and the interference term of the first and the third interfaces F₁₃.
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CrystEngComm, 2020, 22,2900-2903
DOI: 10.1039/D0CE00296H, Communication

Oksana Danylyuk, Volodymyr Sashuk
Crystallization-driven self-assembly of three macrocyclic members of the cucurbit[n]uril family is explained by the cumulative effect of multiple C–H⋯O hydrogen bonds.
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CrystEngComm, 2020, 22,2895-2899
DOI: 10.1039/D0CE00379D, Communication

Andrey V. Gavrikov, Andrey B. Ilyukhin, Pavel S. Koroteev
Uncommon SCSC transformation when desolvation induces subtle changes within a mononuclear complex, namely a stepwise change in the binding of a particular ligand.
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CrystEngComm, 2020, 22,2889-2894
DOI: 10.1039/D0CE00397B, Communication

Open Access

  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.

Peng Yang, Buthainah Alshankiti, Niveen M. Khashab
Intrinsically porous molecular building blocks are used for the rational design and construction of molecular-level controlled porous materials.
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CrystEngComm, 2020, 22,3020-3032
DOI: 10.1039/D0CE00343C, Paper

Christian A. Juillerat, Vladislav V. Klepov, Mark D. Smith, Hans-Conrad zur Loye
The flux synthesis of a uranium gallophosphate and a uranium gallate, Cs₄[UO₂Ga₂(PO₄)₄] and Cs₂UO₂Ga₂O₅, and 4 uranium phosphates, [Rb₂Rb_3.93Cl_0.93][(UO₂)₅(PO₄)₅], Rb₁₁[(UO₂)₈(PO₄)₉], Rb_7.6[(UO₂)₈O_8.6F_0.4(PO₄)₂], and Rb₆[(UO₂)₅O₂(PO₄)₄], is reported.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00341G, Paper

Yue Qi, Ou Sun, Yanyan Zhou, Yuan Yao, Zhenyu Cheng, Ting Gao, Hongfeng Li
Due to the effect of the combination of the rigid structure and synergistic interactions of two ligands on energy transfer, the Cd–Ln complexes show excellent NIR luminescence properties with the QYs reaching 0.34% for Nd³⁺ and 2.13% for Yb³⁺.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00253D, Paper

Yini Mao, Li Jiang, Pengfei Xian, Qiongfen Fu, Shanshan Hu, Jun Yang
Pure hexagonal phase KSc(MoO₄)₂ crystals with a hexagonal block shape were successfully synthesized via a one-step hydrothermal method.
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CrystEngComm, 2020, 22,2964-2969
DOI: 10.1039/D0CE00221F, Paper

Masahide Tominaga, Kosuke Mizuno, Haruka Yamamoto, Tadashi Hyodo, Kentaro Yamaguchi
Crystallization of a diimide-based macrocycle having adamantane parts and several cyclic ethers in chloroform provided inclusion crystals, where both guests were cooperatively accommodated within inner spaces between the macrocycles.
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CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00359J, Communication

Zhenfeng Zhang
An X-shaped CN⋯CO interaction, which plays a critical role in dictating the molecule conformation and crystal packing patterns, has been found to occur on the polar surface of (cyanoacetyl)hydrazones, and is rationalized by density functional theory calculations.
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CrystEngComm, 2020, 22,2998-3004
DOI: 10.1039/D0CE00039F, Paper

Ruirui Wang, Haili Wang, Juan Wang, Feifei Bai, Yue Ma, Licun Li, Qinglun Wang, Bin Zhao, Peng Cheng
For the isomorphic tetranuclear 3d–4f compounds constructed by [M(CN)₆]³⁻ linking Ln^III-Schiff-base units, the diamagnetic Co^III ions in the system could suppress QTM effectively and obtain a field-induced SMMs behavior.
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CrystEngComm, 2020, 22,3005-3019
DOI: 10.1039/D0CE00125B, Paper

Ipsita Mondal, Tanmoy Basak, Snehasis Banerjee, Shouvik Chattopadhyay
A reduced Schiff base used as a fluorescence chemo-sensor for selective detection of zinc(II). Strong fluorescence behaviors of two zinc(II) complexes are correlated with the presence of a rigid hydrogen-bonded network in their solid state structure.
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CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00435A, Paper

Pengpeng Lei, Ran An, Chengyu Li, Jing Feng, Hongjie Zhang
Bismuth-based nanoparticles, especially NaBiF4, have attracted extensive attention as hosts of lanthanides (Ln3+) ions and other luminescent ions in recent years. However, controllable synthesis of NaBiF4 nanoparticles remains a challenge....
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