de

Chiral separations with crosslinked cellulose derivatives attached onto hybrid silica monolith particles via thiol-ene click reaction

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00772B, Paper
Yuhong Zhou, Qian Liang, Zhilun Zhang, Zhaodi Wang, Mingxian Huang
Hybrid silica monolith containing vinyl groups was synthesized by a sol-gel method and then ground and treated, yielding silica particles with 3-5 μm in particles size and 10-20 nm in...
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de

A novel hybrid micro extraction for sensitive determination of 17β-Estradiol in water samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00581A, Paper
Shivender Singh Saini
A novel and green hybrid of pipette tip micro solid phase extraction (PT-µSPE) and supported liquid extraction (SLE) has been tailored and established for efficient and sensitive determination of 17β-Estradiol...
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de

Targeted profiling of amino acid metabolome in serum by a liquid chromatography-mass spectrometry method: application to identify potential markers for diet-induced hyperlipidemia

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00305K, Paper
Xiao-fan Wang, You-xi Zhang, Hai-ying Ma
Targeted profiling of amino acid metabolome in serum by LC-MS: application to identify potential markers for diet-induced hyperlipidemia.
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de

Derivatization and rapid GC—MS screening of chlorides relevant to the Chemical Weapons Convention in organic liquid samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00263A, Paper
Open Access
Marja-Leena Kuitunen, Jorgelina Cecilia Altamirano, Peter Siegenthaler, Terhi Hannele Taure, Vesa Mauri Antero Häkkinen, Paula Vanninen
A simple derivatization technique was developed for the analysis of seven Schedule 3 chemicals and one Schedule 2 chemical listed in the Chemical Weapons Conventions (CWC). Phosgene, phosphorus oxychloride, phosphorus...
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de

Improving the determination of celecoxib in body fluids and pharmaceuticals using a new selective and thermosensitive molecularly imprinted poly(vinylidene fluoride) membrane

Anal. Methods, 2020, 12,2185-2195
DOI: 10.1039/D0AY00237B, Paper
Negin Yazdanian, Behrouz Akbari-Adergani, Maryam Kazemipour, Homayon Ahmad Panahi, Mehran Javanbakht
Molecularly imprinted membranes that demonstrated high selectivity for celecoxib were synthesized using N-vinylcaprolactam and 2-hydroxyethyl methacrylate.
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de

Versatile additively manufactured (3D printed) wall-jet flow cell for high performance liquid chromatography-amperometric analysis: application to the detection and quantification of new psychoactive substances (NBOMes)

Anal. Methods, 2020, 12,2152-2165
DOI: 10.1039/D0AY00500B, Paper
Open Access
Hadil M. Elbardisy, Eduardo M. Richter, Robert D. Crapnell, Michael P. Down, Peter G. Gough, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks
Additive manufacturing is an emerging technology of vast applicability, receiving significant interest in a plethora of industrial and research domains as it allows the translation of designs produced via computer software, into 3D printed objects.
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de

Quality by Design (QbD) approach for the development of a rapid UHPLC method for simultaneous determination of aglycone and glycoside forms of isoflavones in dietary supplements

Anal. Methods, 2020, 12,2082-2092
DOI: 10.1039/C9AY02778E, Paper
Kornelija Lasić, Ana Mornar, Biljana Nigović
Systematic development of a UHPLC method by QbD approach as performed for simultaneous determination of aglycone (genistein, daidzein, biochanin A and formononetin) and glycoside (genistin, daidzin, sissotrin, ononin) forms of isoflavones.
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de

High cytotoxic activity of ZnO@leucovorin nanocomposite based materials against an MCF-7 cell model

Anal. Methods, 2020, 12,2176-2184
DOI: 10.1039/D0AY00498G, Paper
Mohamed Fathi Sanad, Esraa Samy Abu Serea, Shereen Magdy Bazid, Shimaa Nabih, Md Ariful Ahsan, Ahmed Esmail Shalan
In the current work, we design a multifunctional hybrid nanocomposite for treating MCF-7 cell lines, which act as a model for breast cancer cells, to overcome the serious side-effects of chemotherapy treatment pathways.
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de

A sensitive HPLC-FL method to simultaneously determine febuxostat and diclofenac in rat plasma: assessment of metabolic drug interactions in vitro and in vivo

Anal. Methods, 2020, 12,2166-2175
DOI: 10.1039/D0AY00471E, Paper
Dong-Gyun Han, Kyu-Sang Kim, Seong-Wook Seo, Young Mee Baek, Yunjin Jung, Dae-Duk Kim, In-Soo Yoon
We developed a sensitive, simple and validated HPLC-FL method for simultaneous determination of FEB and DIC in rat plasma. The method requires a relatively small volume of sample, has simple sample preparation and excellent sensitivity.
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de

Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
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de

The influence of lateral flake size in graphene/graphite paste electrodes: an electroanalytical investigation

Anal. Methods, 2020, 12,2133-2142
DOI: 10.1039/D0AY00169D, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Alejandro García-Miranda Ferrari, Hadil M. Elbardisy, Valentine Silva, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks, Dale A. C. Brownson
We report the electroanalytical properties of graphene and graphite paste electrodes comprising varying lateral flake sizes when applied for sensing relevant biomolecules and prominent drugs of abuse.
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de

Development of a paper-immobilized yeast biosensor for the detection of physiological concentrations of doxycycline in technology-limited settings

Anal. Methods, 2020, 12,2123-2132
DOI: 10.1039/D0AY00001A, Paper
Rachel A. Miller, Galen Brown, Elsa Barron, Jamie L. Luther, Marya Lieberman, Holly V. Goodson
To combat pharmaceutical counterfeiting in low- and middle-income countries (LMIC), there is a need for improved low-cost, portable methods that monitor pharmaceutical concentrations relevant to dosage forms and physiological fluids.
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de

Aptamer-based fluorometric determination of chloramphenicol by controlling the activity of hemin as a peroxidase mimetic

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00389A, Paper
Ling-Chen Wang, Cheng-Yi Hong, Zheng-Zhong Lin, Xiao-Mei Chen, Zhi-Yong Huang
A method for the aptamer-based determination of chloramphenicol (CAP) was developed by exploiting the peroxidase mimicking activity of hemin.
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de

Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
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de

Electrochemical determination of paracetamol in a pharmaceutical dose by adsorptive voltammetry with a carbon paste/La2O3 microcomposite

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00442A, Paper
Edgar Nagles, Mario Ceroni, John Hurtado-Murillo, John Hurtado Belalcazar
This paper presents a new application for microcomposites based on carbon paste (CP) and La2O3 (LaOX). This simple and versatile microcomposite (LaOX/CPE) was applied toward the determination of paracetamol (PCM)...
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de

Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
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de

Plasticizer-free and pH-independent ion-selective optode films based on a solvatochromic dye

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00439A, Communication
Xuewei Wang, Yang Zhou, Vanessa Decker, Mark E. Meyerhoff, Meng Sun, Yu Cui
A layer of a solvatochromic dye, an ionophore, and an ion-exchanger deposited on a Nylon membrane enables highly selective colorimetric and fluorometric ion sensing. This new platform does not suffer...
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de

Confirmation of brand identification in infant formulas by using near-infrared spectroscopy fingerprints

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00375A, Paper
Shuyi Chang, Chengcheng Yin, Sha Liang, Mei Lu, Ping Wang, Zhicheng Li
The NIR spectra of 12 batches of each stage of Brand A infant formulas.
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de

Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
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de

The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00334D, Paper
Hong-Lin Ding, Yan-Qing Pu, Da-Ying Ye, Zi-Yue Dong, Man Yang, Cheng-Wei Lü, Yue An
The design and synthesis of two imidazole fluorescent probes for the special recognition of HClO/NaHSO3 and their applications are shown.
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de

Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
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de

One-step synthesis of mitochondrion-targeted fluorescence carbon dots and fluorescent detection of silver ions

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00622J, Paper
Yue Hou, Hanxiao Liu, Zhanxian Li, Hongyan Zhang, Liuhe Wei, Mingming Yu
Silver ions (Ag+) are the most representative harmful ions found in water pollution and widely used in many industries, excessive ingestion of Ag+ in the human body may interact with...
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de

Quantification of Anthracene after dermal absorption test via APCI-Tandem Mass Spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00486C, Paper
Xinyi Sui, Julio E Teran, Chengcheng Feng, Killian Wustrow, Caroline J. Smith , Nelson R Vinueza
An analytical method for the detection and quantification of anthracene from dermal samples was developed by using Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry (APCI-MS/MS). The anthracene samples were obtained from...
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de

Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
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de

Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
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de

Facile dispersive solid-phase extraction based on humic acid for the determination of aflatoxins in various edible oils

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00534G, Paper
Ping Liu, Yan-Hua Liao, Hao-Bo Zheng, Yang Tang
Aflatoxins (AFs), as the secondary metabolites produced by some toxigenic fungi of Aspergillus species, are well known to be extremely harmful to humans and animals because of their high toxicity, mutagenicity, carcinogenicity, and teratogenicity.
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de

Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
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de

A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
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de

Detection of organophosphorus compounds using a surface acoustic wave array sensor based on supramolecular self-assembling imprinted films

Anal. Methods, 2020, 12,2206-2214
DOI: 10.1039/D0AY00211A, Paper
Yong Pan, Tengxiao Guo, Genwei Zhang, Junchao Yang, Liu Yang, Bingqing Cao
In this study, diisopropyl methylphosphonate (DIMP), tributyl phosphate (TBP), and dimethyl methylphosphonate (DMMP) were selected as organophosphorus chemical warfare agent (CWA) simulants.
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de

Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
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de

Adsorptive removal of Hg2+ from environmental water samples using thioglycerol-intercalated magnetic layered double hydroxides

Anal. Methods, 2020, 12,2279-2286
DOI: 10.1039/D0AY00448K, Paper
Ali Esrafili, Mahnaz Ghambarian, Mohammad Tajik, Mahroo Baharfar
Herein, the removal of Hg2+ from environmental water samples was carried out using a novel nanoadsorbent based on magnetite nanoparticles coated by a thioglycerol-intercalated layered double hydroxide.
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de

LC-MS in combination with DMBA derivatization for sialic acid speciation and distribution analysis in fish tissues

Anal. Methods, 2020, 12,2221-2227
DOI: 10.1039/D0AY00100G, Paper
Junjie Du, Qiwei Zhang, Jianjun Li, Qi Zheng
For sialic acid speciation analysis, DMBA provides superior chromatographic separation efficiency and comparable MS/MS spectra with DMB.
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de

Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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de

Simultaneous aptasensor assay of ochratoxin A and adenosine triphosphate in beer based on Fe3O4 and SiO2 nanoparticle as carriers

Anal. Methods, 2020, 12,2253-2259
DOI: 10.1039/D0AY00311E, Paper
Xiluan Yan, Mengmeng Jiang, Yuting Jian, Jing Luo, Xinxin Xue, Xin Chen, Xiangjuan Zheng, Fanrong Ai
In this work, a chemiluminescence (CL) method based on dual aptasensors using Fe3O4 and SiO2 nanoparticles (NPs) as carriers is developed for the simultaneous detection of ochratoxin A (OTA) and adenosine triphosphate (ATP) in beer.
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de

Detection of radium at the attogram per gram level in copper by inductively coupled plasma mass spectrometry after cation-exchange chromatography

Anal. Methods, 2020, 12,2272-2278
DOI: 10.1039/D0AY00512F, Paper
Mélodie Bonin, Dominic Larivière, Pavel P. Povinec
In this study, a new method was developed for the separation and isolation of radium from metallic copper.
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de

What’s novel in the new Eurachem guide on uncertainty from sampling?

Anal. Methods, 2020, 12,2295-2297
DOI: 10.1039/D0AY90051F, AMC Technical Brief
Analytical Methods Committee, AMCTB No. 96
This Technical Brief aims to explain how the new second edition of the Eurachem guide, Measurement uncertainty arising from sampling, differs significantly from the first edition that was published in 2007.
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de

Development and validation of a real-time microelectrochemical sensor for clinical monitoring of tissue oxygenation/perfusion

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00206B, Paper
Gama Theophile Gnahoré, Jack L. Kelly, Saidhbhe L. O'Riordan, Fiachra B. Bolger, Michelle M. Doran, Michelle Sands, John P. Lowry
Oxygen is critically important to tissue viability and there is increasing demand for its reliable real-time clinical monitoring in order to prevent, diagnose and treat several pathological disorders, including hypoxia, stroke and reperfusion injury.
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de

A sensitive and selective fluorescent probe for the detection of endogenous peroxynitrite (ONOO-) in live cells

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00012D, Paper
Yaru Sun, Baoli Dong, Yaru Lu, Wenhui Song, Abdul Hadi Mehmood, Weiying Lin
Peroxynitrite (ONOO−) is one of reactive oxygen species, and plays a vital role in many physiological and pathological processes. Given that the ONOO− level is closely related with many serious...
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de

A simple paper-based approach for arsenic determination in water using hydride generation coupled with mercaptosuccinic-acid capped CdTe quantum dots

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00273A, Paper
Oraphan Thepmanee, Kanlaya Prapainop Katewongsa, Obnithi Nooppha, Nuanlaor Ratanawimarnwong, Weena Siangproh, Orawon Chailapakul, Kriangsak Songsrirote
This research aims to develop a simple paper-based device for arsenic detection in water samples where a hydride generation technique coupled with mercaptosuccinic acid-capped CdTe quantum dots (MSA-CdTe QDs) as...
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de

ELISA as an effective tool to determine spatial and seasonal occurrence of emerging contaminants in the aquatic environment

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00426J, Paper
Carla Patrícia Silva, Tânia Carvalho, Rudolf J. Schneider, Valdemar I. Esteves, Diana L. D. Lima
Monitoring emerging contaminants is essential as they represent a risk to the aquatic environment. ELISA is a promising method for their quantification mostly because it allows controlling their concentration levels through large screening campaigns.
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de

A flower-like Ag coated with molecularly imprinted polymers as surface-enhanced Raman scattering substrate for sensitive and selective detection of glibenclamide

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00575D, Paper
Xiaohui Ren, Xin Li
The flower-like Ag, was formed by nanosheets self-assembly, as SERS active substrate was utilized for preparation of flower-like Ag@molecularly imprinted polymers (MIPs) surface-enhanced Raman scattering (SERS) sensor. Based on the...
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de

Rapid and colorimetric detection of nucleic acids based on entropy-driven circuit and DNAzyme mediated autocatalytic reaction

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00341G, Paper
Hongli Shi, Jianyuan Dai, fang Wang, Yushun Xia, Dan Xiao, Cuisong Zhou
In this work, a novel, rapid and enzyme-free colorimetric biosensor for nucleic acids detection has been developed based on entropy-driven circuit (EDC) and DNAzyme mediated autocatalytic reaction. Upon sensing of...
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de

Fabrication of an electrochemical sensor based on metal-organic framework ZIF-8 for quantitation of silver ion: optimizing experimental conditions by central composite design (CCD)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00843E, Paper
Farzaneh Hashemi , Ali Reza Zanganeh, Farid Naeimi , Maryam Tayebani
The ZIF-8 was synthesized and carbon paste electrode (CPE) modified with this metal-organic framework utilized for quantitation of silver(Ι) by differential pulse anodic stripping voltammetry (DPASV) technique. The prepared ZIF-8...
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de

Digital Reference Section (DRS) Virtual Programs: New blog post invites readers to "Sample a Taste of History This Thanksgiving"

Find a new and historic recipe for a dish to put on your Thanksgiving table in What Mrs. Fisher Knows About Old Southern Cooking. This cookbook, published in 1881, is highlighted in a recent post on the Library of Congress Blog. Abby Fisher perfected her culinary skills as an enslaved cook on a South Carolina plantation but went on to establish a successful catering business in San Francisco and publish a compilation of her recipes—one of the first by an African-American. Learn more about this remarkable woman and, this Thanksgiving, sample a taste of history!

Click here to go to the Library of Congress Blog post, "Sample a Taste of History This Thanksgiving!"




de

The Canada-US border in the 21st century [electronic resource] : trade, immigration and security in the age of Trump / John B. Sutcliffe and William P. Anderson.

Abingdon, Oxon : Routledge, 2019.




de

North American borders in comparative perspective [electronic resource] / edited by Guadalupe Correa-Cabrera and Victor Konrad.

Tucson : University of Arizona Press, 2020.




de

Between Rome and Persia [electronic resource] : the middle Euphrates, Mesopotamia, and Palmyra under Roman control / Peter M. Edwell

London ; New York : Routledge, 2008




de

Egyptian mummies and modern science [electronic resource] / edited by Rosalie David

Cambridge ; New York : Cambridge University Press, 2008




de

Recharting the Black Atlantic [electronic resource] : modern cultures, local communities, global connections / edited by Annalisa Oboe and Anna Scacchi

New York : Routledge, 2008




de

Covid-19 Factoid: Gap between daily new cases and recoveries widening

The world is adding over 70,000 cases everyday while the daily recoveries are still sub-15,000 on an average in the last three days.