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Sodium nanoferrite-based solid phase extraction: a green method for the simultaneous determination of cadmium, copper, and lead

J. Anal. At. Spectrom., 2024, 39,2884-2892
DOI: 10.1039/D4JA00210E, Paper
Saima Perveen, Aysen Hol, Jameel Ahmed Baig, Syed Tufail Hussain Sherazi, Khalil Akhtar, Sajjad Hussain, Fahad Abbasi
A solid phase extraction (SPE) methodology utilizing sodium ferrite nanoparticles (Na2Fe4O7-NPs; SF-NPs) is presented for the simultaneous determination of heavy metals (HMs) via flame atomic absorption spectrometry (FAAS).
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An ensemble model for rapid quantitative determination of vanadium (V) in petroleum coke by laser-induced breakdown spectroscopy

J. Anal. At. Spectrom., 2024, 39,2841-2855
DOI: 10.1039/D4JA00300D, Paper
Hongkun Du, Tengfei Sun, Shaoying Ke, Dongfeng Qi, Wei Zhang, Juan Wei, Bing Yang, Hongyu Zheng
Precise detection and analysis of trace elements in materials are critical for various industrial applications.
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Quantification of technetium-99 in wastewater by means of automated on-line extraction chromatography – anion-exchange chromatography – inductively coupled plasma-mass spectrometry

J. Anal. At. Spectrom., 2024, 39,2774-2782
DOI: 10.1039/D4JA00270A, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Maximilian Horstmann, C. Derrick Quarles, Steffen Happel, Michael Sperling, Andreas Faust, David Clases, Uwe Karst
Ultratrace concentrations of pertechnetate are determined by preconcentration on a dedicated resin and anion exchange chromatography with ICP-MS detection.
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Efficient preconcentration of ultra-trace rhenium from geological materials via induced adsorption for accurate isotope analysis

J. Anal. At. Spectrom., 2024, 39,2748-2755
DOI: 10.1039/D4JA00295D, Paper
Yumeng Liu, Tianyu Chen, Tao Li, Weiqiang Li, Qingquan Hong, Jiubin Chen
Preconcentration via induced adsorption achieves the quantitative recovery of Re and facilitates Re isotope analysis.
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Data fusion of spectral and acoustic signals in LIBS to improve the measurement accuracy of carbon emissions at varying gas temperatures

J. Anal. At. Spectrom., 2024, 39,2756-2766
DOI: 10.1039/D4JA00287C, Paper
Shu Chai, Jie Ren, Suming Jiang, Aochen Li, Ziqing Zhao, Haimeng Peng, Qiwen Zhang, Wendong Wu
A novel mid-level data fusion method integrating spectral and acoustic signals of laser-induced plasmas was proposed to improve the measurement accuracy of carbon concentrations in flue gas at varying gas temperatures.
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Self-absorption correction of NEXAFS spectra for intermediate sample thicknesses applied to organo-sulfur model compounds

J. Anal. At. Spectrom., 2024, 39,2893-2902
DOI: 10.1039/D4JA00232F, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Konstantin Skudler, Michael Walter, Michael Sommer, Matthias Müller
We present a self-absorption correction for NEXAFS which is valid for any sample thickness. The corrected spectrum is recovered in a forward calculation by fitting a model spectrum to experimental data of samples with ideally different thicknesses.
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A single-column and efficient procedure for separating Fe and Mg from geological materials for isotopic analyses using MC-ICP-MS

J. Anal. At. Spectrom., 2024, 39,2783-2790
DOI: 10.1039/D4JA00272E, Paper
Guanhong Zhu, Zhenmin Ge, Le Zhang, Gangjian Wei, Jinlong Ma
We developed a single-column and efficient procedure for separating Fe and Mg from geological materials for isotope measurements.
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Accurate determination of ultra-trace REEs in seawater using a membrane desolvation Q-ICP-MS coupled with an online automatic separation system

J. Anal. At. Spectrom., 2024, 39,2870-2883
DOI: 10.1039/D4JA00240G, Paper
Ji-Hao Zhu, Feng-You Chu, Feng Liang, Xian-Ying Luo, Qiang Liu, Quan-Hui Xu, Wei Yu, Yong-Chun Li, Jiang-Gu Lu, Yun-Xiu Li, Yan-Hui Dong, Huai-Ming Li, Jun Zhao, Cai Zhang
A highly precise method, based on a traditional Q-ICP-MS coupled with an online automatic separation system and membrane desolvation sample introduction device, was developed for accurate determination of ultra-trace REEs in seawater samples.
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Research on a bimodal fusion detection method for surface defects of metal AM components based on LIBS

J. Anal. At. Spectrom., 2024, 39,2917-2928
DOI: 10.1039/D4JA00159A, Paper
Xiaomei Lin, Jiangfei Yang, Yutao Huang, Jingjun Lin, Changjin Che
A bimodal fusion method using Laser-Induced Breakdown Spectroscopy (LIBS) is proposed to identify surface defects in metal additive manufacturing (AM) samples. This method integrates LIBS spectra with plasma image data to enhance defect detection.
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Assessment of the metal grain size of 12Cr1MoV steel by LIBS coupled with acoustic wave information

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00285G, Paper
Feiqiang Tang, Meirong Dong, Junbin Cai, Zhichun Li, Kaiqing Chen, Weijie Li, Shunchun Yao, Jidong Lu
A modelling scheme that integrates spectral and acoustic data was put forth as a means of enhancing the precision of grain size detection in 12Cr1MoV steel.
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Evaluation of miniaturized ultrasonic nebulization for high-efficiency sampling in characterization of silver nanoparticles by single particle inductively coupled plasma mass spectrometry

J. Anal. At. Spectrom., 2024, 39,2791-2798
DOI: 10.1039/D4JA00320A, Paper
Junhang Dong, Zhenli Zhu, Lujie Li, Pengju Xing, Shuyang Li, Lei Ouyang, Xing Liu, Wei Guo, Hongtao Zheng, Rong Qian
Miniaturized ultrasonic nebulization (MUN) provides high sampling efficiency for single particle inductive coupled plasma mass spectrometry (sp-ICPMS).
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A new concept for correction of instrumental isotopic fractionation in MC-ICP-MS using a pair of monoisotopic elements: a critical evaluation

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00117F, Paper
Open Access
Andrii Tupys, Klaudia Tetfejer, Ludwik Halicz, Ewa Bulska, Jakub Karasiński
In this research work, we investigated the possibility of using mixtures of monoisotopic elements (93Nb/89Y, 165Ho/159Tb and 209Bi/197Au) as calibrators for accurate determination of isotope ratios by multicollector mass spectrometry (MC-ICP-MS).
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Combined enhancement of fiber-optic laser-induced breakdown spectroscopy coupling spatial confinement and double-pulse irradiation

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00291A, Paper
Yan Qiu, Jinghui Li, Bowen Lu, Jian Wu, Xinyu Guo, Yuhua Hang, Yongdong Li, Xingwen Li
The mechanism of double-pulse laser irradiation under spatial confinement remains unclear due to complex plasma plume dynamics and multiple shock wave interactions.
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A single-stage purification method for the precise determination of zirconium isotopic composition in geological samples by double spike MC-ICP-MS

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00332B, Paper
Lanping Feng, Chen Wang, Yan Han, Wen Zhang, Jing-Liang Guo, Lian Zhou, Zhaochu Hu
A simple, fast and efficient column separation method for extracting Zr from geological sample matrices using DGA resin.
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A simple method for elemental analysis of liquids in sprayed microdroplets by laser-induced breakdown spectroscopy

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00192C, Paper
Jun Feng, Yihui Yan, Yuzhu Liu, Jozef Lengyel
The study shows that paper spray and laser-induced breakdown spectroscopy (PS-LIBS) analyze trace elements in aqueous solutions, addressing challenges in bulk analysis. Its efficiency highlights its potential for in situ liquid sample analysis.
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Robust determination of low Ti contents in zircon using LA–ICP–MS/MS with NH3 reaction gas

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00304G, Paper
Junlong Niu, Shitou Wu, Yueheng Yang, Hao Wang, Chao Huang, Lei Xu, Liewen Xie
Compared with the single quadrupole (SQ) mode, Triple Quadrupole (TQ) method is more robust for determining low Ti contents in zircon at high spatial resolutions (laser spot size <20 μm), making it useful for the analysis of complex zircon grains.
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Determination of boron isotopic compositions in five fractions of soil boron: traces of the environmental behavior of boron in soil

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00286E, Paper
Xuejun Chen, Qingcai Xu, Li Yan, Xiaodong Hao, Xiaochen Guan, Xiaopeng Han, Aide Sun, Zhiqun Chen, Lihua Liu, Zihao Zhu
A stepwise extraction method established for boron isotope measurement of five fractions in soil boron showed their feathered isotopic signals.
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Fast analysis of metal components in coal dust using spark emission spectroscopy

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00322E, Paper
Jialin Li, Jing Huang, Lina Zheng, Shakila Naz, Xutong Liu
We present a fast method based on spark emission spectroscopy to quantify metal components such as Al, Si, Fe, Ca, and Ti in airborne coal dust.
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A miniaturized microplasma excitation source coupled with photochemically induced volatile species generation as a cost-effective tool for in situ mercury pollution analyses

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00306C, Technical Note
Open Access
Tymoteusz Klis, Pawel Pohl, Anna Dzimitrowicz, Piotr Jamroz
A portable, miniaturized atmospheric microplasma discharge system coupled with the photochemical vapour generation was developed for the sensitive Hg determination in water samples using OES.
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Investigation of direct simultaneous uranium isotopic determination and age dating of micrometer-sized uranium particles by laser ablation – multi-collector ICPMS

J. Anal. At. Spectrom., 2024, Advance Article
DOI: 10.1039/D4JA00280F, Paper
Anne-Claire Humbert, Fabien Pointurier, Amélie Hubert
The proposed method offers to the analytical community an alternative technique for uranium particle aged dating more widely available than LG SIMS. Moreover, working on μm-sized particles reduces issues with laser-induced fractionation.
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Laser-Induced Breakdown Spectroscopy (LIBS): calibration challenges, combination with other techniques, and spectral analysis using data science

J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00250D, Critical Review
Dennis Ferreira, Diego Victor De Babos, Mauro Henrique Lima-Filho, Heloisa Froehlick Castello, Alejandro C. Olivieri, Fabiola Manhas Verbi Pereira, Edenir Rodrigues Pereira-Filho
Laser-Induced Breakdown Spectroscopy (LIBS) is a versatile and powerful analytical technique widely used for rapid, in-situ elemental analysis across various fields, from industrial quality control to planetary exploration. This review...
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Trace xenon detection in ambient helium by double-pulse laser-induced breakdown spectroscopy

J. Anal. At. Spectrom., 2024, Accepted Manuscript
DOI: 10.1039/D4JA00358F, Paper
Open Access
Londrea Garrett, Milos Burger, Yunu Lee, Hyeongbin Kim, Piyush Sabharwall, Sungyeol Choi, Igor Jovanovic
Safe operation of next-generation nuclear reactors is contingent on developing and effectively operating new diagnostics methods. For helium-cooled fast reactors, one important safety concern is the onset of fuel-cladding failure,...
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Boom in commercial realty

The commercial segment holds scope for both capital appreciation and regular income through monthly rentals.




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Calculating common maintenance charges

Your property-related legal queries answered by S.C. RAGHURAM, Partner, RANK Associates, a Chennai-based law firm




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FSI: Point Counterpoint

Increasing the FSI need not be the only solution to make housing affordable, argues A. Venkatasubramanian




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Community value in realty

Assess your new home’s community value and how it might impact its future valuation, says Sonal Sachdev.




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Creating cohesion out of fragmentation

Governments need to look at alternate methods of sourcing and developing land such as land pooling, says Rohan Sharma




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Will interest rates come down?

It is an anxious wait for the Budget and the fiscal new year.




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Calculating maintenance costs

Your property-related legal queries answered by S.C. RAGHURAM, Partner, RANK Associates, a Chennai-based law firm



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Waiting too long for a price correction?

Buyer indecisiveness is usually the result of confusion, not certainty




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Second US healthcare worker has Ebola




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Almonds could reduce belly fat: study




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China starts clinical trial to repair human spinal cord injury




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Gorilla origins of two AIDS virus lineages confirmed: Study

Previous research found that groups M and N of the HIV-1 virus originated in geographically distinct chimpanzee communities in southern Cameroon, but origins of groups O and P remained uncertain till now.




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Australian researchers discover new treatment for prostrate cancer




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India flooded with unsafe fixed dose combination drugs

Many unapproved FDC formulations contain banned, restricted, or never approved drugs




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Breakthrough in treating leucoderma




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First trial to use umbilical cord stem cells to cure HIV




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Quality control for AYUSH drugs




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Indians could face a higher risk of diabetes-induced lung ailments

High levels of insulin directly damage the lung structure, says global study.




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3D printing could help fix damaged cartilage in knees

A disruptive technology, says researcher




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Green Corridor paves the way for organ transport

13 km covered in just 14 minutes from Victoria Hospital to M.S. Ramaiah Hospital in Bengaluru




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Compound in turmeric may treat colon cancer: study

Researchers from Saint Louis University in the United States have said that curcumin, an active ingredient in the spice, holds promise in treating such cancers.




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Novel drug compound inhibits skin cancer in mice, finds study




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World’s smallest tape recorder built from bacteria

Mr. Wang and his team created the microscopic data recorder by taking advantage of CRISPR-Cas, an immune system in many species of bacteria.




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WHO pauses Covaxin supply via UN bodies




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Baby with ‘Tessier Facial Cleft’ gets complete face reconstruction in Bengaluru through crowdfunding

The baby from Ballari district in Karnataka has undergone three complex surgeries in Bengaluru through crowdfunding




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Compulsory rural service: Nearly 2,000 senior resident doctors in Karnataka await specialist counselling and posting

They say they wrote their exams in May and have been living with uncertainty for the last two months




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Kidwai institute to come up on PKTB campus in Mysuru

5 acres identified for establishing the cancer care centre next to Princess Krishnarajammanni Super Speciality Hospital on KRS Road




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Comprehensive Urban Primary Health Centre established in Bengaluru, opening to coincide with PM Narendra Modi’s birthday

Karnataka Government says that the comprehensive Urban Primary Health Centre (CUPHC) is the first of its kind in India, and is located at Palace Guttahalli, near Malleswaram